Returned lunar samples porphyrin analysis
Explore the source record for details and available documents.
Rho, J. H.↗
SEARCH · Search NASA
Results for “Sample Return”
Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.
Quote a phrase for an exact phrase match. Source license links do not imply unrestricted reuse.
Mars sample collection and preservation
The intensive exploration of Mars is a major step in the systematic exploration of the solar system. Mars, earth, and Venus provide valuable contrasts in planetary evolution. Mars exploration has progressed through the stages of exploration and is now ready for a sample-return mission. About 5 kg of intelligently selected samples will be returned from Mars. A variety of samples are wanted. This requires accurate landing in areas of high interest, surface mobility and analytical capability, a variety of sampling tools, and stringent preservation and isolation measures.
Blanchard, Douglas P.↗
Prompt Gamma Activation Analysis (PGAA): Technique of choice for nondestructive bulk analysis of returned comet samples
Prompt gamma activation analysis (PGAA) is a well-developed analytical technique. The technique involves irradiation of samples in an external neutron beam from a nuclear reactor, with simultaneous counting of gamma rays produced in the sample by neutron capture. Capture of neutrons leads to excited nuclei which decay immediately with the emission of energetic gamma rays to the ground state. PGAA has several advantages over other techniques for the analysis of cometary materials: (1) It is nondestructive; (2) It can be used to determine abundances of a wide variety of elements, including most major and minor elements (Na, Mg, Al, Si, P, K, Ca, Ti, Cr, Mn, Fe, Co, Ni), volatiles (H, C, N, F, Cl, S), and some trace elements (those with high neutron capture cross sections, including B, Cd, Nd, Sm, and Gd); and (3) It is a true bulk analysis technique. Recent developments should improve the technique's sensitivity and accuracy considerably.
Lindstrom, David J.↗
Curation of Frozen Samples
NASA's Johnson Space Center (JSC) and the Astromaterials Curator are charged by NPD 7100.10D with the curation of all of NASA s extraterrestrial samples, including those from future missions. This responsibility includes the development of new sample handling and preparation techniques; therefore, the Astromaterials Curator must begin developing procedures to preserve, prepare and ship samples at sub-freezing temperatures in order to enable future sample return missions. Such missions might include the return of future frozen samples from permanently-shadowed lunar craters, the nuclei of comets, the surface of Mars, etc. We are demonstrating the ability to curate samples under cold conditions by designing, installing and testing a cold curation glovebox. This glovebox will allow us to store, document, manipulate and subdivide frozen samples while quantifying and minimizing contamination throughout the curation process.
Fletcher, L. A.↗
Curation, Spacecraft Recovery and Preliminary Examination for the Stardust Mission: A Perspective from the Curatorial Facility
We briefly describe some of the challenges to the Stardust mission, curation and sample preliminary analysis, from the perspective of the Curation Office at the Johnson Space Center. Our goal is to inform persons planning future sample returns, so that they may learn from both our successes and challenges (and avoid some of our mistakes). The Curation office played a role in the mission from its inception, most critically assisting in the design and implementation of the spacecraft contamination control plan, and in planning and documenting the recovery of the spacecraft reentry capsule in Utah. A unique class 100 cleanroom was built to maintain the returned comet and interstellar samples in clean comfort, and to permit dissection and allocation of samples for analysis.
Zolensky, Michael↗
Simulation and Characterization of a Miniaturized Scanning Electron Microscope
A miniaturized Scanning Electron Microscope (mSEM) for in-situ lunar investigations is being developed at NASA Marshall Space Flight Center with colleagues from the University of Alabama in Huntsville (UAH), Advanced Research Systems (ARS), the University of Tennessee in Knoxville (UTK) and Case Western Reserve University (CWRU). This effort focuses on the characterization of individual components of the mSEM and simulation of the complete system. SEMs can provide information on the size, shape, morphology and chemical composition of lunar regolith. Understanding these basic properties will allow us to better estimate the challenges associated with In-Situ Resource Utilization and to improve our basic science knowledge of the lunar surface (either precluding the need for sample return or allowing differentiation of unique samples to be returned to Earth.) The main components of the mSEM prototype includes: a cold field emission electron gun (CFEG), focusing lens, deflection/scanning system and backscatter electron detector. Of these, the electron gun development is of particular importance as it dictates much of the design of the remaining components. A CFEG was chosen for use with the lunar mSEM as its emission does not depend on heating of the tungsten emitter (lower power), it offers a long operation lifetime, is orders of magnitude brighter than tungsten hairpin guns, has a small source size and exhibits low beam energy spread.
Gaskin, Jessica A.↗
The Laser Ablation Ion Funnel: Sampling for in situ Mass Spectrometry on Mars
A considerable investment has been made by NASA and other space agencies to develop instrumentation suitable for in situ analytical investigation of extra terrestrial bodies including various mass spectrometers (time-of-flight, quadrupole ion trap, quadrupole mass filters, etc.). However, the front-end sample handling that is needed to collect and prepare samples for interrogation by such instrumentation remains underdeveloped. Here we describe a novel approach tailored to the exploration of Mars where ions are created in the ambient atmosphere via laser ablation and then efficiently transported into a mass spectrometer for in situ analysis using an electrodynamic ion funnel. This concept would enable elemental and isotopic analysis of geological samples with the analysis of desorbed organic material a possibility as well. Such an instrument would be suitable for inclusion on all potential missions currently being considered such as the Mid-Range Rover, the Astrobiology Field Laboratory, and Mars Sample Return (i.e., as a sample pre-selection triage instrument), among others.
Johnson, Paul V.↗
Performance Evaluation of the Operational Air Quality Monitor for Water Testing Aboard the International Space Station
In the history of manned spaceflight, environmental monitoring has relied heavily on archival sampling. For short missions, this type of sample collection was sufficient; returned samples provided a snapshot of the presence of chemical and biological contaminants in the spacecraft air and water. However, with the construction of the International Space Station (ISS) and the subsequent extension of mission durations, soon to be up to one year, the need for enhanced, real-time environmental monitoring became more pressing. The past several years have seen the implementation of several real-time monitors aboard the ISS, complemented with reduced archival sampling. The station air is currently monitored for volatile organic compounds (VOCs) using gas chromatography-differential mobility spectrometry (Air Quality Monitor [AQM]). The water on ISS is analyzed to measure total organic carbon and biocide concentrations using the Total Organic Carbon Analyzer (TOCA) and the Colorimetric Water Quality Monitoring Kit (CWQMK), respectively. The current air and water monitors provide important data, but the number and size of the different instruments makes them impractical for future exploration missions. It is apparent that there is still a need for improvements in environmental monitoring capabilities. One such improvement could be realized by modifying a single instrument to analyze both air and water. As the AQM currently provides quantitative, compound-specific information for target compounds present in air samples, and many of the compounds are also targets for water quality monitoring, this instrument provides a logical starting point to evaluate the feasibility of this approach. In this presentation, we will discuss our recent studies aimed at determining an appropriate method for introducing VOCs from water samples into the gas phase and our current work, in which an electro-thermal vaporization unit has been interfaced with the AQM to analyze target analytes at the relevant concentrations at which they are routinely detected in archival water samples from the ISS.
Wallace, William T.↗
Selecting and Certifying a Landing Site for Moonrise in South Pole-Aitken Basin
MoonRise is a New Frontiers mission concept to land in the South Pole-Aitken (SPA) basin, collect samples, and return the samples to Earth for detailed mineral, chemical, petrologic, geochronologic, and physical properties analyses to address science questions relevant to the early evolution of the Solar System and the Moon. Science associated with this mission concept is described elsewhere; here we discuss selection of sites within SPA to address science objectives using recent scientific studies (orbital spectroscopy, gravity, topography), and the use of new data (LRO) to certify safe landing sites for a robotic sample return mission such as MoonRise.
Jolliff, B.↗
Returning Geological Samples from Mars
Mars Ascent Vehicle (MAV) Study: Design challenges associated with Mars; Remote; Temperature; Atmosphere; Radiation; Dust. Challenges unique to MAV: No vehicle has ever left the surface of Mars; Completely autonomous; Physical system extremely limited; Martian environment creates a number of issues with traditional propulsion systems.
Yaghoubi, Darius↗
Challenges of Returning Geological Samples from Mars
Explore the source record for details and available documents.
Industrial Engineering↗
Mars 2020: Mission, Science Objectives and Build
If all goes according to plan, in February 2021, NASA will land the Mars 2020 Rover on the surface of Mars. Mars 2020 is the latest in a series of unmanned Martian robotic rover missions that are part of NASA’s Mars Exploration Program, a long-term effort of robotic exploration of the planet. The mission seeks to address high-priority goals for Mars exploration, including answering questions about the potential for past life on Mars. Mars 2020 will look for evidence of habitable conditions on Mars in the ancient past, as well as look for signs of past microbial life itself. The mission also seeks to understanding the geological history and evolution of the planet, and to prepare for future robotic and human exploration. The Mars 2020 spacecraft and rover borrow heavily from the Mars Science Laboratory (MSL) mission and Curiosity rover which landed on Mars in 2012. This reliance on proven technology helps reduce mission risk and cost. Mars 2020 does contain new technology, including a drill for coring samples from Martian rock and soil and a Sample Caching System for gathering, storing and preserving samples for possible future return to Earth. In this paper, we will review the primary goals of the Mars 2020 Mission and look at the reasons for choosing Jezero Crater as the landing site. We will discuss the design and build of the Mars 2020 Spacecraft system and its similarities and differences with Mars Science Laboratory and the Curiosity Rover. We will also review the Mars 2020 Scientific Instrument Suite and their goals. Finally, we will review the Return Sample Contamination Control requirements and the design choices that were made to facilitate meeting these requirements.
Soares, Carlos E.↗
Method Development for In Situ Microbiome Profiling of the Water Recovery System’s Wastewater Tank Onboard the International Space Station
A distinctive microbial community has inhabited the wastewater tank within the International Space Station Water Recovery System (WRS) for over 14 years and experienced the stressors associated with the microgravity environment. The WRS generates potable water for the crew from urine distillate, humidity condensate, Sabatier product water, and the occasional off-loading of ground-supplied water. The reservoir for these products, the wastewater tank, does not have a means of microbial control. While samples are occasionally collected for analysis, the time between sample collection and the return to Earth, as well as the lack of preservation, results in a skewed depiction of the microbiome. Routinely observed from these returned samples are high counts (105 – 106 colony forming units per mL) and two prevailing genera, Burkholderia and Ralstonia. The wastewater tank likely contains a more diverse microbiome, as a higher diversity of bacteria and fungus has been noted upstream and downstream of the tank. To characterize the microbial profile of the tank, analysis needs to occur at the time of sample collection. Toward this goal, a method for in situ analysis based on nanopore sequencing was developed. The filter-to-sequencer method evolved from previous work that has been validated onboard the ISS (BEST payload and the BioMole Crew Health Care Systems Facility). The method, including filtration, DNA extraction, purification, amplification, library preparation, and nanopore sequencing will be described. Additionally, data collected with this method from both ISS and terrestrial samples will be detailed. The consumables needed to support in situ analysis of the tank are set to the launch to the ISS in the spring of 2023. This investigation will allow for the first accurate characterization of the microbiome of the tank providing insight for crew health, planetary protection, and has the potential to enable engineering controls for future space station water systems.
Sarah Stahl-Rommel↗
Insights From Routine Microbiological Monitoring of Air in Astromaterials Curation Cleanrooms
NASA maintains nine separate cleanrooms at the Johnson Space Center to curate and preserve astromaterials samples. Routine microbial monitoring of the surfaces in these cleanrooms began in 20181. Until recently, materials compatibility requirements prevented monitoring airborne biological particles in all but one of these cleanrooms. New astromaterials collections from carbon rich asteroids are more susceptible to biological degradation than previous collections. Therefore, it is important to monitor the bioburden in the air and on surfaces in these labs. Establishing a comprehensive microbial monitoring program will help inform the monitoring and curation plans for Mars sample return which will include samples that are extremely biologically sensitive. In April of 2022 we began routinely collecting air samples in seven of the nine curation cleanrooms (Meteorite ISO 7 equivalent, Lunar ISO 6 equivalent, Stardust, Hayabusa2, OSIRIS-REx ISO 5 equivalent, and Genesis ISO 4 equivalent) using a sampling device that collects airborne biological particles on an electret filter instead conventional sampler that collect cells in a liquid media or onto organic rich Petri dishes. Electret is a generic term for electrostatically charged media. The charge on these materials increases particle trapping when compared to non-charged filters of similar thickness. N95 respirators also use electret filters. This dry sample collection method allows us to meet materials requirements for all the curation labs and reduces the risk of inadvertently introducing contamination as part of our monitoring effort. This method also allows us to preserve a portion of each sample for DNA extraction and next generation sequencing. DNA sequencing helps us to characterize the portion of the cleanroom microbiome that we cannot culture. We will present the results of our first 8 months of monitoring, compare these results to particle counts in the labs and to measurements made directly onto Petri dishes when possible. We will also make recommendations for modifications to the sampling method to improve sampling efficiency and preserve diversity.
A. B. Regberg↗
Organic Matter in "Quick-Look" Returned Bennu samples Revealed by Coordinated UV Fluorescence, SEM-EDX and Two-Step Laser Mass Spectrometry
Explore the source record for details and available documents.
Bennu↗
FROSTE: Frozen Return of Samples to Earth
Explore the source record for details and available documents.
regolith↗
In situ propellant production - A new potential for round-trip spacecraft
In situ propellant production (ISPP) greatly reduces the Earth escape requirements for some roundtrip missions, particularly Mars Sample Return. ISPP systems are described which produce oxygen or oxygen and methane from available atmospheric and surface materials. With ISPP, a 1 kg sample can be returned direct from Mars using a single Shuttle launch. Mars entry can be either direct or from orbit. Comet and asteroid sample return is also accomplished within a single Shuttle launch. Launch requirements for round-trip missions to Ganymede and Callisto are reduced by 15 to 40%.
Stancati, M. L.↗