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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 1,279 records · Page 71
All sourcesNASA NTRSDOE OSTI
NASA NTRS2019

First Results from Laser-Based Spectral Characterization of Landsat 9 Operational Land Imager-2

Landsat 9 will continue the Landsat data record into its fifth decade with launch scheduled for December 2020. The two instruments on Landsat 9 are Thermal Infrared Sensor-2 (TIRS-2) and Operational Land Imager-2 (OLI-2). OLI-2 is a nine-channel pushbroom imager with a 15-degree field of view that will have a 16-day measurement cadence from its nominal 705-km orbit altitude. A key aspect of the data that will be produced by OLI-2 is its spectral fidelity which enables countless science applications. The prelaunch test campaign for spectral characterization of OLI-2 was substantially improved relative to the methodology used for OLI: the full spectral response of every detector was characterized with greater accuracy, sampling, and precision. This paper will describe how this was accomplished with a tunable laser-based light source called Goddard Laser for Absolute Measurement of Radiance (GLAMR).

tunable laser↗
NASA NTRS2021

Full Aerothermal Characterization of the NASA Glenn Research Center 9- by 15-Foot Low-Speed Wind Tunnel (2019 Test)

Following completion of the 9- by 15-Foot Low Speed Wind Tunnel acoustic improvement modification project, a characterization of the flow field throughout the 9- by 15-foot test section was conducted in 2019. The acoustic improvement modifications project included several large-scale tunnel loop modifications and reconstruction of the 9- by 15-Foot Low Speed Wind Tunnel test section and diffuser to decrease the noise floor in the test section. Data were collected at three cross-sectional planes in the 9- by 15-ft test section using a 15-foot traversing calibration rake and a set of eight boundary layer rakes. The data from the characterization test were used to generate calibration relationships for facility operation and understand the flow quality in the new test section, including uniformity, flow angularity, turbulence intensity, and boundary layer characteristics. Additionally, the subsonic quick check rake was used to baseline the check calibration data set for the new test section.

Wind↗
NASA NTRS2022

Characterization of Infrared Optical Motion Tracking System in NASA's Simulated Lunar Operations (SLOPE) Laboratory

This work characterizes the accuracy of a 16 camera OptiTrack motion tracking system installed in NASA Glenn Research Center's Simulated Lunar Operations (SLOPE) laboratory. The position of a rigid body mounted on a motorized linear stage is compared to its position reported by the motion tracking system as it travels through the facility's 777m$^3$ capture volume of interest. Experiments show that the mean error reported by the motion tracking system for the aggregate capture volume is in-line with independent measurements collected using the motion stage. Error within regions of the capture volume exceed the mean error reported by the motion tracking system, likely due to occlusion, and suggests that additional cameras should be used to increase measurement accuracy in these regions. Overall, results show that error values reported by the motion tracking system are representative of the measurement error in a collected data set and validates the system's use for characterizing the mobility and tractive performance of robots, rovers, and other vehicles for planetary exploration.

Motion capture↗
NASA NTRS2024

Structural Characterization of a TriTruss Module

The TriTruss is a novel structural module developed by researchers at NASA Langley Research Center (LaRC) that can be used in space to assemble large support structures for a variety of applications. One such application is the metering truss or primary mirror backbone support structure of an In-Space Assembled Telescope (iSAT). For the iSAT application, the TriTruss will be supporting mirror segments, payloads, and instruments, all of which require the TriTruss to have a high stiffness. Structural characterization from testing and analysis is needed to ensure the integrity of the struts that make up a TriTruss module is maintained when subjected to loads representative of the application. The test setup and loads applied to the TriTruss module as well as the analytical methods used to predict the response of the structure under conditions representative of those implemented during testing will be discussed. Also, the results obtained from testing and analysis will be summarized. The goal for the characterization study was to achieve a correlation within 10% between the test data and the analysis. Overall, the correlation varied for the struts with a few struts still having a larger error margin after further studies were conducted to improve the correlation through additional analysis.

Characterization↗
NASA NTRS2025

Influence of Actuator Movement Rate During Acquisition of Inlet Characterization Data

This report considers using a process to acquire performance data for supersonic mixed-compression inlets that is faster and less costly than the previous process. In the previous process for acquiring data during wind tunnel experiments, actuators for backpressuring an inlet moved in discrete increments, paused for dynamics to dampen, measured data for 5 s, recorded the data, and then reduced the data to graphic plots of pressure recovery versus mass capture ratio. This discrete data acquisition procedure was methodical, reliable, and accurate. However, acquiring data to characterize the inlet consumed significant wind-on time. Wind tunnel operation was costly when considering maintenance, energy, and human resources (operators and research team); therefore, the price for each data point was high. This report presents a quicker method to obtain all measurements, one which can also be used in blowdown wind tunnels. This approach, identified as the dynamic inlet characteristic data acquisition procedure, uses in situ dynamic high-speed pressure sensors to measure pressure signals. The backpressuring actuator moves continuously, and measurements from high-speed pressure sensors are recorded as the actuator progresses to and past the incremental points. Despite its advantages, the approach raised the following questions: (1) Will the new process be as accurate as the previous process? and (2) Are there any hidden costs? These concerns are addressed in this report. This report reviews a study that was undertaken to compare wind tunnel experiment data taken using the previous discrete data acquisition procedure with data recorded using the dynamic inlet characterization data acquisition procedure. In this report, the wind tunnel experiment and the study objectives are described. The processes to reduce the data for analysis are explained, and a discussion of the results is given. Finally, conclusions from this study that may guide further work in this area are presented.

Inlet Characterization Curves↗
DOE OSTI2018

Mechanical Characterization Study of Sintered Silver Pastes: Preprint

Sintered silver-based bonded interfaces are a critical enabling technology for high-temperature, compact, high-performance, and reliable wide-bandgap packages and components. High-pressure (about 40 MPa) sintered silver interfaces have been implemented commercially, most notably the commercial products offered by Semikron. To reduce manufacturing complexity, there is significant industry interest in pressure-less sintered silver interfaces. To this end, current formulations of sintered silver paste are comprised of purely nano-sized silver particles or a combination of nano- and micro-sized silver particles/flakes. It is essential to quantify the mechanical properties and determine the reliability of these interfaces prior to use in automotive power electronics applications. In this paper, research efforts at the National Renewable Energy Laboratory, in collaboration with Virginia Polytechnic Institute and State University and an industry partner, in optimizing the synthesis procedure and mechanical characterization of sintered silver double-lap samples are described. These double-lap samples were synthesized using pressure-less sintering techniques. Shear testing was conducted at multiple temperatures and displacement rates on these samples sintered using two types of sintered silver pastes, one of them consisting of nano-silver particles and the other a hybrid paste or a combination of nano- and micron-sized silver flakes, employed in a double-lap configuration. Maximum values of shear stress obtained from the characterization study are reported.

33 ADVANCED PROPULSION SYSTEMS↗
DOE OSTI2019

CGI for Impedance Characterization of Inverter-Coupled Generation

This presentation provides an overview of impedance characterization of inverter-coupled generation using the 7 MVA/13.2 kV grid simulator (controllable grid interface) at the National Wind Technology Center of NREL. The presentation shows how sequence impedance responses of multi-megawatt inverters and wind turbines are measured using the grid simulator. Applications of the measured impedance responses for the evaluation of dynamic interactions and high-fidelity model validation are demonstrated. The presentation also shows application of large-signal impedance theory for the prediction of harmonics generated by subsynchronous resonance (SSR) of DFIG-based Type-III wind turbines with series-compensated transmission lines. Finally, a new method for impedance-based characterization of power system frequency response is presented to enable real-time estimation of system inertia and primary frequency response (PFR), and to support control design for frequency support by inverter-coupled generation.

17 WIND ENERGY↗
DOE OSTI2022

Advanced Characterization capability at INL/MFC

I am invited to give a 5-minute one slide presentation on the characterization capability of the Advanced Characterization group (U500) at the Mountain State Society of Electron Microscopy meeting on June 30th. I will only have bullet points information of the microscopy instruments we have at INL/MFC and the contact information of corresponding instrument scientists.

36 MATERIALS SCIENCE↗
DOE OSTI2023

MATBOX, an Open-Source Microstructure Analysis Toolbox for Meshing, Generation, Segmentation, and Characterization of 3D Heterogenous Volumes

Battery performance is strongly correlated with electrode microstructural properties. To account for its impact, lithium-ion battery (LIB) models either abstract the microstructural heterogeneity of composite electrodes using effective macroscopic properties (macro- or meso- scale models) or directly solve the system of equations on the microstructure geometry or mesh (microstructure-scale models). Therefore, to be adequate, both families of models require information from the microstructure geometry, which can be provided by the numerical tool presented in this work. MATBOX is a MATLAB open-source application [1] developed by NREL for performing various microstructure-related tasks including microstructure numerical generation, image filtering and microstructure segmentation, microstructure characterization and correlation, visualization, and microstructure meshing. MATBOX was originally developed for the analysis of LIB electrode microstructures; however, the algorithms provided by the toolbox are widely applicable to other heterogeneous materials. The toolbox provides a user-friendly experience thanks to a Graphical-User Interface, requires no coding by the user, and is well documented. This presentation will illustrate various MATBOX features for the characterization of a LIB electrode, including a fully automated Representative Volume Element (RVE) analysis, the numerical generation of complex 'virtual' microstructure, including dual-layer electrodes and carbon-binder additive phase, and the meshing of a complex NMC/graphite full cell microstructure suitable for 3D finite-element modeling. Other modules (segmentation, visualization, and correlation) will be briefly presented. Thanks to its modular, open-source approach, MATBOX can easily incorporate third-party algorithms to eventually build a standard in the field that will benefit the whole scientific community. Effective diffusion coefficient [2], additive phase numerical generation [3], and meshing [4] third-party algorithms have been already integrated in the toolbox with more to come.

DIRECT ENERGY CONVERSION,MATHEMATICS AND COMPUTING↗
DOE OSTI2023

Baseline Graphite Characterization

Presentation will include baseline graphite characterization information, such as purpose and results, baseline property measurements, baseline graphite characterization method, baseline progress, split disc tensile strength: ASTM Tensile Strength Alternative, Identification of proper split disk fracture, baseline graphite ASTM D8289, horizontal orientation, digital image correlation, and DIC Analyzation.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗
DOE OSTI2024

Baseline Characterization Database Verification Report ? NBG-17 Billet V104

The purpose of this report is to present data collected in the Baseline Graphite Characterization Program, which is directly tasked with supporting the Idaho National Laboratory’s (INL’s) research and development efforts on the Advanced Reactor Technologies (ART) Program. This program populates a comprehensive database that reflects the baseline properties of nuclear-grade graphite regarding individual grade, billet, and position within individual billets. The physical- and mechanical-property information being collected will be transferred to the Nuclear Data Management and Analysis System (NDMAS), and that database will help populate the handbook of property data available to member nations of the Generation-IV International Forum. Transfer of these data from the applicable technical lead to the dissemination databases available to other end users requires a full review of the test procedures and data-collection efforts through an analysis of the multiple summary spreadsheets and values being collected. This report represents the analysis for NBG-17 Billet V104 and facilitates release of associated data to the NDMAS custodians. Millions of raw data points have been collected during testing and quantification analyses for these billets. The summary scalar property values and supplementary traceability data are collected into comprehensive spreadsheets. Data sets are composed of single billets of graphite for any given grade, organized by mechanical test-specimen type, and further subdivided into individual spreadsheet tabs according to the specific test or evaluation being performed. A direct analysis of properties was not conducted, and this report does not provide information on the validity or performance characteristics of the graphite itself. Rather, this report is intended as a verification of the completeness of actual data collected in accordance with PLN-3467, “Baseline Graphite Characterization Plan: Electromechanical Testing,” [1] and PLN-3348 “Graphite Mechanical Testing” [2] and their representation of the measurement and test results with sole regard to the graphite billets under evaluation.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗
DOE OSTI2026

Identification of Solid-Electrolyte Interphase Species by Joint Characterization of Li-Ion Battery Chemistry by Mass Spectrometry and Electrochemical Reaction Networks

The formation and stability of the solid-electrolyte interphase (SEI) play central roles in determining the long-term performance and safety of modern electrochemical energy storage systems. Despite decades of research, the SEI’s heterogeneous, dynamic, and multiphase nature has defied comprehensive molecular-level characterization, creating a critical knowledge gap that limits rational battery design. In this work, we introduce a computational−experimental framework that integrates high-throughput quantum chemistry calculations, data-driven electrochemical reaction networks (eCRNs), stochastic algorithms, and laser desorption/ionization Fourier transform ion cyclotron resonance mass spectrometry (LDI-FTICR-MS) to unravel SEI formation in carbonatebased electrolytes without imposing predefined mechanisms. We constructed the most comprehensive eCRN to date, spanning over 10,000 species and 209 million reactions. Through stochastic network analysis, we successfully recovered 27 species that were previously reported in the literature and predicted 28 novel SEI species nearly doubling our scientific knowledge in this area. Each new species was rigorously confirmed through advanced mass spectral analysis of its distinct molecular and isotopic signatures. We kinetically refined the formation pathways for a select set of both previously reported and novel SEI products, revealing kinetically feasible elementary reaction mechanisms with activation barriers below 1 eV. This computational−experimental approach deepens our molecular-level understanding of SEI chemistry by resolving which species form and through which decomposition mechanisms they emerge. Such knowledge provides the foundation necessary to connect electrolyte composition to the resulting SEI components, a critical step toward a more informed electrolyte development in next-generation lithium-based batteries.

25 ENERGY STORAGE↗
DOE OSTI2022

Grain‐Boundary‐Rich Noble Metal Nanoparticle Assemblies: Synthesis, Characterization, and Reactivity

Abstract Here, a comprehensive study on the synthesis, characterization, and reactivity of grain‐boundary (GB)‐rich noble metal nanoparticle (NP) assemblies is presented. A facile and scalable synthesis of Pt, Pd, Au, Ag, and Rh NP assemblies is developed, in which NPs are predominantly connected via Σ3 (111) twin GBs, forming a network. Driven by water electrolysis, the random collisions and oriented attachment of colloidal NPs in solution lead to the formation of Σ3 (111) twin boundaries and some highly mismatched GBs. This synthetic method also provides convenient control over the GB density without altering the crystallite size or GB type by varying the NP collision frequency. The structural characterization reveals the presence of localized tensile strain at the GB sites. The ultrahigh activity of GB‐rich Pt NP assembly toward catalytic hydrogen oxidation in air is demonstrated, enabling room‐temperature catalytic hydrogen sensing for the first time. Finally, density functional theory calculations reveal that the strained Σ3(111) twin boundary facilitates oxygen dissociation, drastically enhancing the hydrogen oxidation rate via the dissociative pathway. This reported large‐scale synthesis of the Σ3 (111) twin GB‐rich structures enables the development of a broad range of high‐performance GB‐rich catalysts.

Geng, Xin↗
DOE OSTI2023

Multimodal Characterization of Crystal Structure and Formation in Rubrene Thin Films Reveals Erasure of Orientational Discontinuities

Abstract Multimodal multiscale characterization provide opportunities to study organic semiconducting thin films with multiple length scales, across multiple platforms, to elucidate crystallization mechanisms of the various microstructures that impact functionality. With polarized scanning transmission X‐ray and 4D‐scanning transmission electron microscopy, hybrid crystalline structures in rubrene thin films in which large crystalline domains surround a common nucleus and transition to a spherulite morphology at larger radii is observed. These high‐resolution techniques reveal how azimuthal orientational discontinuities at smaller radii are erased as spherulite morphology takes hold. In situ crystallization in the films with optical microscopy is also captured, discovering the importance of considering the initial temperature increase of a film during thermal annealing over the crystallization timescale. This kinetic information of the radial crystallization rate and of corresponding film heating kinetics is used to estimate the temperature at which the larger crystalline regions transition into a spherulite. By combining the results obtained from the different characterization modes, it is learned that thermal conditions can sensitively affect the crystallization of rubrene and other organic thin films. The observations suggest opportunities for more complex temperature‐dependent processing to maximize hybrid structures’ functionality in organic thin films and demonstrate that multimodal studies deepen the understanding of structure‐function dynamics.

Tan, Jenna A.↗
DOE OSTI2018

Development and Characterization of 3D Printable Thermite Component Materials

Additive manufacturing (AM) has recently shown great promise as a means to tailor a wide range of material properties, both quasi-static and dynamic. An example of controlling the dynamic behavior is to tailor the chemical energy release rate in composite energetic materials such as thermites – which are a subset of pyrotechnics that use a metal fuel and a metal oxide as an oxidizer. Since these materials are most hazardous once finely mixed, the approach taken here is to formulate the fuel and oxidizer separately such that they can be mixed on-the-fly. The development, formulation, and characterization of two respective aqueous 3D printable inks consisting of Al and CuO are discussed. The rheological properties and ability of the material to span gaps are characterized. To demonstrate that the materials could be mixed and sustain a reaction, the inks are fed into a static mixing nozzle and extruded into a high-aspect ratio test strip. Upon drying, the material can be ignited and sustain a propagation through the part. These results present a facile, and safe, way to AM thermite which can be used for more detailed follow on studies looking at the role of architecture on the reactivity.

36 MATERIALS SCIENCE↗
DOE OSTI2024

Advancing Insights into Electrochemical Pre‐Treatments of Supported Nanoparticle Electrocatalysts by Combining a Design of Experiments Strategy with In Situ Characterization

Activation, break-in, and/or pre-treatment protocols are generally applied to energy conversion devices before regular operation to reach stable performance. There remains much to understand about the relationships among physical properties, performance, and electrochemical pre-treatments. Here, a design-of-experiments (DoE) strategy is employed to address this gap by demonstrating the influence of five pre-treatment parameters for carbon-supported Pt-nanoparticle catalysts on the electrocatalytic oxygen reduction reaction (ORR). A subset of pre-treatments, developed using a central composite design, are tested in a flow cell combined with an inductively-coupled plasma mass spectrometer (on-line ICP-MS). The DoE-based approach facilitates comprehensive insights from two orders of magnitude fewer experiments than a conventional grid search. The coupled on-line ICP-MS setup enables effective catalysis and real-time catalyst dissolution data. Leveraging insights from DoE for on-line ICP-MS and additional characterization, a model is built between the degradation of a multi-dimensional supported Pt surface, its performance, and applied electrochemical parameters. These investigations identify surface modifications, such as oxidation, and subsequent restructuring of Pt during pre-treatment as a primary cause of performance deterioration during ORR. By combining DoE with advanced characterization techniques, a powerful approach is demonstrated to gain a mechanistic understanding of pre-treatment protocols that can be broadly adapted to various reaction chemistries.

Platinum↗
DOE OSTI2017

Spectroscopic Evidence for a Monomeric Copper(I) Hydride and Crystallographic Characterization of a Monomeric Silver(I) Hydride

Abstract (1,3‐bis[2,6‐bis[di(4‐tert‐butylphenyl)methyl]‐4‐methylphenyl]imidazol‐2‐ylidene)CuOPh [(IPr**)CuOPh] reacts with poly(methylhydrosiloxane) as the hydride donor to afford the monomeric (IPr**)CuH complex, which was spectroscopically characterized. The latter is in equilibrium in solution with [(IPr**)CuH] 2 , the dimer being exclusively present in the solid state. These results support the hypothesis that copper hydride aggregates dissociate in solution. In contrast, addition of pinacolborane to [(IPr**)AgOPh] at −40 °C allows the isolation of the monomeric (IPr**)AgH complex, which was crystallographically characterized.

Romero, Erik A.↗