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All sourcesNASA NTRSDOE OSTI
NASA NTRS2004

GPS FOM Chimney Analysis using Generalized Extreme Value Distribution

Many a time an objective of a statistical analysis is to estimate a limit value like 3-sigma 95% confidence upper limit from a data sample. The generalized Extreme Value Distribution method can be profitably employed in many situations for such an estimate. . .. It is well known that according to the Central Limit theorem the mean value of a large data set is normally distributed irrespective of the distribution of the data from which the mean value is derived. In a somewhat similar fashion it is observed that many times the extreme value of a data set has a distribution that can be formulated with a Generalized Distribution. In space shuttle entry with 3-string GPS navigation the Figure Of Merit (FOM) value gives a measure of GPS navigated state accuracy. A GPS navigated state with FOM of 6 or higher is deemed unacceptable and is said to form a FOM 6 or higher chimney. A FOM chimney is a period of time during which the FOM value stays higher than 5. A longer period of FOM of value 6 or higher causes navigated state to accumulate more error for a lack of state update. For an acceptable landing it is imperative that the state error remains low and hence at low altitude during entry GPS data of FOM greater than 5 must not last more than 138 seconds. I To test the GPS performAnce many entry test cases were simulated at the Avionics Development Laboratory. Only high value FoM chimneys are consequential. The extreme value statistical technique is applied to analyze high value FOM chimneys. The Maximum likelihood method is used to determine parameters that characterize the GEV distribution, and then the limit value statistics are estimated.

Ott, Rick↗
DOE OSTI2025

Data and scripts associated with “Point-scale organic-matter decomposition in streambeds is weakly associated with reach-scale respiration”

This data package is associated with “Point-scale organic-matter decomposition in streambeds is weakly associated with reach-scale respiration” published in EGU Biogeosciences (Stegen et al., 2026; https://doi.org/10.5194/bg-23-3981-2026). It contains cotton strip decomposition rates (Kcd and Kdd) collected across the Yakima River Basin (YRB), Washington, USA. These data were collected to support a broader study examining the drivers of spatial variability in sediment respiration rates in the Yakima River Basin. Associated data used in analysis, metadata, and field protocols can be accessed at https://data.ess-dive.lbl.gov/datasets/doi:10.15485/1923689, https://data.ess-dive.lbl.gov/datasets/doi:10.15485/1969566, and https://data.ess-dive.lbl.gov/datasets/doi:10.15485/1987520. This data package is associated with the repository found at https://github.com/river-corridors-sfa/rcsfa-ST-2B-SSS-cotton-strip. A preliminary version of this data package was published in December 2025 at the time of manuscript submission. It was updated in June 2026, at the time of manuscript acceptance, to include additional metadata (this readme, data dictionary, and file level metadata). The data did not change. For details on how to navigate data packages generated by this project, see https://data.ess-dive.lbl.gov/portals/PNNLRiverCorridorSFA/About. In addition to a readme, this data package also includes a file-level metadata (FLMD) file that describes each file and a data dictionary (DD) that describes all column/row headers and variable definitions. This data package consists of (1) readme; (2) data dictionary (dd); (3) file level metadata (flmd); and (4) four folders: (1) R-scripts; (2) figures; (3) outputs from the scripts; and (4) published data. The published data folder contains a readme directing the user to download data in order to run the R-scripts. All files are .csv, .pdf, .R, .Rmd, and .txt. We acknowledge the Yakama Nation as owners and caretakers of the lands where we collected these data. We thank the Confederated Tribes and Bands of the Yakama Nation Tribal Council and Yakama Nation Fisheries for working with us to facilitate sample collection and optimization of data usage according to their values and worldview.

54 ENVIRONMENTAL SCIENCES↗
NASA NTRS1995

Formal methods demonstration project for space applications

The Space Shuttle program is cooperating in a pilot project to apply formal methods to live requirements analysis activities. As one of the larger ongoing shuttle Change Requests (CR's), the Global Positioning System (GPS) CR involves a significant upgrade to the Shuttle's navigation capability. Shuttles are to be outfitted with GPS receivers and the primary avionics software will be enhanced to accept GPS-provided positions and integrate them into navigation calculations. Prior to implementing the CR, requirements analysts at Loral Space Information Systems, the Shuttle software contractor, must scrutinize the CR to identify and resolve any requirements issues. We describe an ongoing task of the Formal Methods Demonstration Project for Space Applications whose goal is to find an effective way to use formal methods in the GPS CR requirements analysis phase. This phase is currently under way and a small team from NASA Langley, ViGYAN Inc. and Loral is now engaged in this task. Background on the GPS CR is provided and an overview of the hardware/software architecture is presented. We outline the approach being taken to formalize the requirements, only a subset of which is being attempted. The approach features the use of the PVS specification language to model 'principal functions', which are major units of Shuttle software. Conventional state machine techniques form the basis of our approach. Given this background, we present interim results based on a snapshot of work in progress. Samples of requirements specifications rendered in PVS are offered to illustration. We walk through a specification sketch for the principal function known as GPS Receiver State processing. Results to date are summarized and feedback from Loral requirements analysts is highlighted. Preliminary data is shown comparing issues detected by the formal methods team versus those detected using existing requirements analysis methods. We conclude by discussing our plan to complete the remaining activities of this task.

Divito, Ben L.↗
NASA NTRS2007

Separation Control Over A Wall-Mounted Hump

Separation control by means of steady suction or zero efflux oscillatory jets is known to be effective in a wide variety of flows under different flow conditions. Control is effective when applied in a nominally two-dimensional manner, for example, at the leading-edge of a wing or at the shoulder of a deflected flap. Despite intuitive understanding of the flow, at present there is no accepted theoretical model that can adequately explain or describe the observed effects of the leading parameters such as reduced suction-rate, or frequency and momentum input. This difficulty stems partly from the turbulent nature of the flows combined with superimposed coherent structures, which are usually driven by at least one instability mechanism. The ever increasing technological importance of these flows has spurned an urgent need to develop turbulence models with a predictive capability. Present attempts to develop such models are hampered in one way or another by incomplete data sets, uncertain or undocumented inflow and boundary conditions, or inadequate flow-field measurements. This paper attempts to address these issues by conducting an experimental investigation of a lowspeed separated flow over a wall-mounted hump model. The model geometry was designed by Seifert & Pack, who measured static and dynamic pressures on the model for a wide range of Reynolds and Mach numbers and control conditions. This paper describes the present experimental setup, as well as the types and range of data acquired. Sample data is presented and future work is discussed.

Greenblatt, D.↗
NASA NTRS2011

CO2 Insulation for Thermal Control of the Mars Science Laboratory

The National Aeronautics and Space Administration (NASA) is sending a large (>850 kg) rover as part of the Mars Science Laboratory (MSL) mission to Mars in 2011. The rover's primary power source is a Multi-Mission Radioisotope Thermoelectric Generator (MMRTG) that generates roughly 2000 W of heat, which is converted to approximately 110 W of electrical power for use by the rover electronics, science instruments, and mechanism-actuators. The large rover size and extreme thermal environments (cold and hot) for which the rover is designed for led to a sophisticated thermal control system to keep it within allowable temperature limits. The pre-existing Martian atmosphere of low thermal conductivity CO2 gas (8 Torr) is used to thermally protect the rover and its components from the extremely cold Martian environment (temperatures as low as -130 deg C). Conventional vacuum based insulation like Multi Layer Insulation (MLI) is not effective in a gaseous atmosphere, so engineered gaps between the warm rover internal components and the cold rover external structure were employed to implement this thermal isolation. Large gaps would lead to more thermal isolation, but would also require more of the precious volume available within the rover. Therefore, a balance of the degree of thermal isolation achieved vs. the volume of rover utilized is required to reach an acceptable design. The temperature differences between the controlled components and the rover structure vary from location to location so each gap has to be evaluated on a case-by-case basis to arrive at an optimal thickness. For every configuration and temperature difference, there is a critical thickness below which the heat transfer mechanism is dominated by simple gaseous thermal conduction. For larger gaps, the mechanism is dominated by natural convection. In general, convection leads to a poorer level of thermal isolation as compared to conduction. All these considerations play important roles in the optimization process. A three-step process was utilized to design this insulation. The first step is to come up with a simple, textbook based, closed-form equation assessment of gap thickness vs. resultant thermal isolation achieved. The second step is a more sophisticated numerical assessment using Computational Fluid Dynamics (CFD) software to investigate the effect of complicated geometries and temperature contours along them to arrive at the effective thermal isolation in a CO2 atmosphere. The third step is to test samples of representative geometries in a CO2 filled chamber to measure the thermal isolation achieved. The results of these assessments along with the consistency checks across these methods leads to the formulation of design-guidelines for gap implementation within the rover geometry. Finally, based on the geometric and functional constraints within the real rover system, a detailed design that accommodates all these factors is arrived at. This paper will describe in detail this entire process, the results of these assessments and the final design that was implemented.

CO2↗
DOE OSTI2015

Moving Toward Quantifying Reliability - The Next Step in a Rapidly Maturing PV Industry: Preprint

Some may say that PV modules are moving toward being a simple commodity, but most major PV customers ask: 'How can I minimize chances of a module recall?' Or, 'How can I quantify the added value of a 'premium' module?' Or, 'How can I assess the value of an old PV system that I'm thinking of purchasing?' These are all questions that PVQAT (the International PV Quality Assurance Task Force) and partner organizations are working to answer. Defining standard methods for ensuring minimal acceptable quality of PV modules, differentiating modules that provide added value in the toughest of environments, and creating a process (e.g. through IECRE [1]) that can follow a PV system from design through installation and operation are tough tasks, but having standard approaches for these will increase confidence, reduce costs, and be a critical foundation of a mature PV industry. This paper summarizes current needs for new tests, some challenges for defining those tests, and some of the key efforts toward development of international standards, emphasizing that meaningful quantification of reliability (as in defining a service life prediction) must be done in the context of a specific product with design parameters defined through a quality management system.

14 SOLAR ENERGY↗
NASA NTRS2011

Sensitivity of C-Band Polarimetric Radar-Based Drop Size Distribution Measurements to Maximum Diameter Assumptions

The estimation of rain drop size distribution (DSD) parameters from polarimetric radar observations is accomplished by first establishing a relationship between differential reflectivity (Z(sub dr)) and the central tendency of the rain DSD such as the median volume diameter (D0). Since Z(sub dr) does not provide a direct measurement of DSD central tendency, the relationship is typically derived empirically from rain drop and radar scattering models (e.g., D0 = F[Z (sub dr)] ). Past studies have explored the general sensitivity of these models to temperature, radar wavelength, the drop shape vs. size relation, and DSD variability. Much progress has been made in recent years in measuring the drop shape and DSD variability using surface-based disdrometers, such as the 2D Video disdrometer (2DVD), and documenting their impact on polarimetric radar techniques. In addition to measuring drop shape, another advantage of the 2DVD over earlier impact type disdrometers is its ability to resolve drop diameters in excess of 5 mm. Despite this improvement, the sampling limitations of a disdrometer, including the 2DVD, make it very difficult to adequately measure the maximum drop diameter (D(sub max)) present in a typical radar resolution volume. As a result, D(sub max) must still be assumed in the drop and radar models from which D0 = F[Z(sub dr)] is derived. Since scattering resonance at C-band wavelengths begins to occur in drop diameters larger than about 5 mm, modeled C-band radar parameters, particularly Z(sub dr), can be sensitive to D(sub max) assumptions. In past C-band radar studies, a variety of D(sub max) assumptions have been made, including the actual disdrometer estimate of D(sub max) during a typical sampling period (e.g., 1-3 minutes), D(sub max) = C (where C is constant at values from 5 to 8 mm), and D(sub max) = M*D0 (where the constant multiple, M, is fixed at values ranging from 2.5 to 3.5). The overall objective of this NASA Global Precipitation Measurement Mission (GPM/PMM Science Team)-funded study is to document the sensitivity of DSD measurements, including estimates of D0, from C-band Z(sub dr) and reflectivity to this range of D(sub max) assumptions. For this study, GPM Ground Validation 2DVD's were operated under the scanning domain of the UAHuntsville ARMOR C-band dual-polarimetric radar. Approximately 7500 minutes of DSD data were collected and processed to create gamma size distribution parameters using a truncated method of moments approach. After creating the gamma parameter datasets the DSD's were then used as input to a T-matrix model for computation of polarimetric radar moments at C-band. All necessary model parameterizations, such as temperature, drop shape, and drop fall mode, were fixed at typically accepted values while the D(sub max) assumption was allowed to vary in sensitivity tests. By hypothesizing a DSD model with D(sub max) (fit) from which the empirical fit to D0 = F[Z(sub dr)] was derived via non-linear least squares regression and a separate reference DSD model with D(sub max) (truth), bias and standard error in D0 retrievals were estimated in the presence of Z(sub dr) measurement error and hypothesized mismatch in D(sub max) assumptions. Although the normalized standard error for D0 = F[Z(sub dr)r] can increase slightly (as much as from 11% to 16% for all 7500 DSDs) when the D(sub max) (fit) does not match D(sub max) (truth), the primary impact of uncertainty in D(sub max) is a potential increase in normalized bias error in D0 (from 0% to as much as 10% over all 7500 DSDs, depending on the extent of the mismatch between D(sub max) (fit) and D(sub max) (truth)). For DSDs characterized by large Z(sub dr) (Z(sub dr) > 1.5 to 2.0 dB), the normalized bias error for D0 estimation at C-band is sometimes unacceptably large (> 10%), again depending on the extent of the hypothesized D(sub max) mismatch. Modeled errors in D0 retrievals from Z(sub dr) at C-band are demonstrated in detail and comparedo similar modeled retrieval errors at S-band and X-band where the sensitivity to D(sub max) is expected to be less. The impact of D(sub max) assumptions to the retrieval of other DSD parameters such as Nw, the liquid water content normalized intercept parameter, are also explored. Likely implications for DSD retrievals using C-band polarimetric radar for GPM are assessed by considering current community knowledge regarding D(sub max) and quantifying the statistical distribution of Z(sub dr) from ARMOR over a large variety of meteorological conditions. Based on these results and the prevalence of C-band polarimetric radars worldwide, a call for more emphasis on constraining our observational estimate of D(sub max) within a typical radar resolution volume is made

Carey, Lawrence D.↗
DOE OSTI2013

A Database and Meta-Analysis of Ecological Responses to Flow in the South Atlantic Region

Generalized and quantitative relationships between flow and ecology are pivotal to developing environmental flow standards based on socially acceptable ecological conditions. Informing management at regional scales requires compiling sufficient hydrologic and ecological sources of information, identifying information gaps, and creating a framework for hypothesis development and testing. We compiled studies of empirical and theoretical relationships between flow and ecology in the South Atlantic region (SAR) of the United States to evaluate their utility for the development of environmental flow standards. Using database searches, internet searches, and agency contacts, we gathered 186 sources of information that provided a qualitative or quantitative relationship between flow and ecology within states encompassing the SAR. A total of 109 of the 186 sources had sufficient information to support quantitative analyses. Ecological responses to natural changes in flow magnitude, frequency, and duration were highly variable regardless of the direction and magnitude of changes in flow. In contrast, the majority of ecological responses to anthropogenic-induced flow alterations were negative. Fish consistently showed negative responses to anthropogenic flow alterations whereas other ecological groups showed somewhat variable responses (e.g. macroinvertebrates and riparian vegetation) and even positive responses (e.g. algae). Fish and organic matter had sufficient sample sizes to stratify natural flow-ecology relationships by specific flow categories (e.g. high flow, baseflows) or by region (e.g. coastal plain, uplands). After stratifying relationships, we found that significant correlations existed between changes in natural flow and ecological responses. In addition, a regression tree explained 57% of the variation in fish responses to anthropogenic and natural changes in flow. Because of some ambiguity in interpreting the directionality in ecological responses, we utilized ecological gains or losses, where each represents a benefit or reduction to ecosystem services, respectively. Variables explained 49% of the variation in ecological gains and losses for all ecological groups combined. Altogether, our results suggested that the source of flow change and the ecological group of interest played primary roles in determining the direction and magnitude of ecological responses. Furthermore, our results suggest that developing broadly generalized relationships between ecology and changes in flow at a regional scale is unlikely unless relationships are placed within meaningful contexts, such as environmental flow components or by geomorphic setting.

Environmental flow↗
DOE OSTI2019

Research Technology Laboratory (RTL) Disposition Program Final Status Survey Report

As part of the Battelle Facility Restoration Program (Smoter and Biebesheimer 2017), the Research Technology Laboratory (RTL) Complex was remediated through demolition and surveyed to show it meets the radiological release criteria for unrestricted use under the clearance process (DOE 2011). The restoration program has directed the implementation of the Multi-Agency Radiation Survey and Site Investigation Manual (MARSSIM) methodology (NRC 2011) to verify the suitability of the site to be released for unrestricted use under the clearance process in U.S. Department of Energy (DOE) Order 458.1 (Biebesheimer 2018a; DOE 2011). The use of MARSSIM is accepted by federal and state agencies, including DOE. This report documents how the MARSSIM process was used to assure any residual radioactivity is within acceptable levels and as low as reasonably achievable. Past land use for the RTL Complex property included agricultural, residential, and industrial activity. The historical site assessment (HSA) (Lindenmeier et al. 2015; Biebesheimer 2018b) identified use of radionuclides in past RTL Complex research and development activities from commissioning in 1966 until it was vacated in 2017. Based on the information provided in the HSA, the RTL Complex was delineated into six survey units. The 520 building footprint, tank vault and 530 building footprint, other building footprints, and pipeline survey units included excavated areas. The paved areas and open areas survey units were unexcavated areas. Survey units were all determined to be Class 3, with low probability of containing residual radioactivity, after demolition of the structures within the RTL Complex. The Research Technology Laboratory (RTL) Disposition Program: Final Status Survey Plan (Bunn et al. 2018) was designed and conducted to provide quantitative data regarding the residual radioactivity present in each survey unit. Authorized radiological release limits were developed and approved by the DOE Office of Science in December 2016 (DOE 2017). Fourteen random sample locations were identified within each survey unit. Forty-four specific judgmental sample locations were selected across the site based on information in the HSA. The number of sample locations within a survey unit ranged from 15 to 28, for a total of 127 random and judgmental sample locations identified across the RTL Complex. Sampling for the final status survey occurred over 12 days between November 11 and December 7, 2018. Laboratory results were independently validated by Analytical Quality Associates prior to evaluation. All of the over 880 residual radioactivity measurements were less than the release limits and action levels established through the RTL Disposition Program. A sum of fractions calculation for each survey unit resulted in values that were less than unity. Based on the results presented in this report, the restoration program recommends that the RTL Complex be released for unrestricted use.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
NASA NTRS1995

Evaluation testing of a portable vapor detector for Part-Per-Billion (PPB) level UDMH and N2H4

Trace level detection of hydrazine (N2H4), monomethyl hydrazine (MMH) and unsymmetrical dimethylhydrazine (UDMH) has been receiving increased attention over the past several years. In May 1995 the American Conference of Government Industrial Hygienists (ACGIH) lowered their acceptable threshold limit value (TLV) from 100 parts-per-billion (ppb) to 10 ppb. Several types of ppb-level detectors are being developed by the United States Air Force (USAF) Space and Missile Systems Center (SMSC). A breadboard version of a portable, lightweight hydrazine detection sensor was developed and produced by Giner Corp. for the USAF. This sensor was designed for ppb level UDMH and N2H4 vapor detection in near real-time. This instrument employs electrochemical sensing, utilizing a three electrode cell with an anion-exchange polymer electrolyte membrane as the only electrolyte in the system. The sensing, counter and reference electrodes are bonded to the membrane forming a single component. The only liquid required to maintain the sensor is deionized water which hydrates the membrane. At the request of the USAF SMSC, independent testing and evaluation of the breadboard instrument was performed at NASA's Toxic Vapor Detection Laboratory (TVDL) for response to ppb-level N2H4 and UDMH and MMH. The TVDL, located at Kennedy Space Center (KSC) has the unique ability to generate calibrated sample vapor streams of N2H4, UDMH, and MMH over a range from less than 10 ppb to thousands of parts per million (ppm) with full environmental control of relative humidity (0-90%) and temperature (0-50 C). The TVDL routinely performs these types of tests. Referenced sensors were subjected to extensive testing, including precision, linearity, response/recovery times, zero and span drift, humidity and temperature effects as well as ammonia interference. Results of these tests and general operation characteristics are reported.

Curran, Dan↗
DOE OSTI2023

Grating-Based Imaging-Scattering with Portable Neutron Generator

Company: Adelphi Technology, Inc. Title: Grating-Based Imaging-Scattering with Portable Neutron Generator PI: Dr. Jay Theodore Cremer, Jr. Topic: 26a Statement of the problem or situation that is being addressed. Successful plant growth depends upon an efficient and robust root system. The plant root is part of a larger system of water and microbial flows in the soil system. While much effort has been exerted to develop an imaging system for water, microbes, and roots, the problem is challenging, and no widely accepted imaging method currently exists. The optical solutions use a highly modified soil system. X-ray imaging methods are insensitive to the soft tissues in the presence of sand. Thermal neutron imaging has been often tested, but found inadequate, due to limited access and low image resolution. This project will develop a new strategy for neutron imaging of plant/soil systems. The project will allow long duration experiments in greenhouse environments and increase the image information content to the micron scale. General statement of how this problem is being addressed. Portable, rugged thermal and fast neutron sources are being developed where portable means a two-soldier team can carry the source and power unit to survey rough terrain for explosives. In the past decade, microfabrication of X-ray and thermal/cold neutron optics has opened a new imaging strategy. The standard transmission image is now supplemented with simultaneous acquisition of a phase contrast image and an image revealing scattering features. In materials science, the interferometric neutron scattering image has been used to detect early crack formation in stressed additive manufacturing test samples. The detection requires sensitivity to scattering features at the 1-micron scale. By addition of our proposed grating-optic to Adelphi Technology’s radiographic/tomographic imaging system, which is based on portable thermal neutron source, the resulting thermal neutron scatter image of the plant/soil system, will reveal details at 1-micron. Commercial Applications and Other Benefits Neutron interferometry imaging has greater penetration through large metal components compared to industrial X-ray imaging. The low-cost, large area optics developed for greenhouse applications, combined with the robust, portable neutron generator, can then be marketed as a system for inspection of additive manufactured components. In the aerospace industry, all freshly printed components are validated with X-ray CT. Scheduled maintenance again requires X-ray CT as the ability to predict aerospace component lifetime does not yet exist. Large aerospace components are only partially observed with X-ray imaging. Key Words Neutron radiography/tomography, grating interferometry, thermal neutron generator imaging, plant root and soil imaging, rhizosphere imaging, deployable neutron imaging systems Summary for Members of Congress A rugged, portable source of thermal neutrons is adapted for neutron interferometry imaging with the addition of low-cost, 3D printed optics. The first application of our proposed deployable, compact thermal neutron generator imaging system, using a grating optic, is plant root/soil science in greenhouse settings and agricultural laboratories.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
NASA NTRS1962

PYROLYTIC GRAPHITE ROCKET THRUST CHAMBER INVESTIGATION PROJECT. MONTHLY LETTER

This is the Monthly Letter Progress Report for the eighth month of a twelve month technical study directed toward the following objectives: A. Determining analytically and experimentally the feasibility and attractiveness of using free-standing pyrolytic graphite for a radiation cooled liquid rocket thrust chamber and exit nozzle for space application. B. Establishing through analysis and experimental demonstration, a set of design principles to facilitate the design of a reliable pyrolytic graphite thrust chamber assembly for a specific range of operating conditions. C. Demonstrate by means of test firings of complete thrust chamber assemblies, the validity of the design data and principles developed during the program. Preparations have been completed for test firing the two 100 lb. thrust Boron Pyralloy chambers at Marquardt during the first week in March 1962. These two chambers will first be static pressure checked with water to a pressure of 135 psig. The chambers will then be test fired with N204/N2H4-MMH propellants . Test samples of eleven different pyrolytic carbide and nitride materials have been ordered for high temperature oxidation tests and should be delivered by the end of March for evaluation in the plasma torch facility. The specific materials ordered in free- standing condition in thicknesses from 0.030 inch to 0.065 inch were as follows: (a) Pyrolytic graphite (on hand) (b) Pyrolytic graphite-boron alloy (on hand) (c) Pyrolytic graphite-tungsten alloy (d)Boron nitride (e) Titanium nitride (f) Silicon carbide (g) Titanium carbide (h) Zirconium carbide (i) Hafnium carbide (j) Niobium carbide (k) Tantalum carbide (l) High density (1 1-90) graphite (m) High density graphite (heat treated) These materials were ordered from Raytheon, HTM, and American Meta 1 Products . A summary of the available data on the oxidation rates of pyrolytic materials under slow air and rocket motor conditions is shown in Figure 1. High Temperature Materials, Inc. has been contacted relative to providing Pyrographite thrust chambers with extra-thick walls . They believe they can deliver chambers with substantially thicker walls than were possible a short time ago. Such a configuration, with acceptable residual stresses, would provide a longer firing life since it is ultimately limited by the oxidation rate of the chamber wall material. Stress and structural studies have continued. The analytical stress studies point out some of the problems associated with the experimental determination of the elastic constants of this highly anisotropic material. Further analysis may shed light on improved techniques for making these experimental determinations. The large potential weight saving available with the use of pyrolytic graphite as a thrust chamber wall material in a radiation cooled rocket motor has been calculated and is shown graphically in Figure 2. Figure A presents the program progress schedule and the actual expenditures as of 7 February 1962.

ROCKET ENGINE↗
DOE OSTI2019

Structural investigation and applications of glassy sodium phosphate including the kinetics of dissolution rates and spectral analysis of the prepared samples with a focus on their effects on water treatment

This paper discuss the preparation of the binary system of Phosphate Based Glass (PBG) xP{sub 2}O{sub 5}–(100 − x) Na{sub 2}O mol% and investigates the compositions that form glassy matrix. It is found that x in the range between x = 40–60 mol% and divided in to 5 glass samples (x = 40, 45, 50, 55, 60) and for compositions of 40 > x > 60 no glassy matrix is formed. The intensities of the peak centers of the IR spectra of sodium phosphate glasses and the suggested vibrational modes of structural phosphate chains, terminal groups and tabulated data imply a shift in absorption bands with increasing the Na{sub 2}O mol% content. The amount of bridging phosphorous, shows a maximum value for the glass containing 60 mol% Na{sub 2}O due to the depolymerization of the phosphate matrix with increasing Na{sub 2}O content from 40 to 60 mol% via a breakdown of some terminal bonds (P=O) in the glass network which decreases the bond strength, consequently the peak center is shifted towards lower wave number. Essentially, five compositions of glassy samples were investigated: (x = 40, 45, 50, 55, and 60) mol%. The kinetics of dissolution rate were investigated by two ways: 1—the weight loss data and 2—electrical properties of the solution (pH, Electrical Conductivity) leached by the glass sample in to the deionized water. It is found that with increasing the Na{sub 2}O% content, the pH values, the dissolution rate and the solubility are increasing. It could be noticed that the ionic levels increased with the immersion time and were directly related to the solubility of the glasses. The highest in solubility (x = 40) is the highest in EC and pH values caused by high Na{sub 2}O%. By studying the effect of PBG on the real water medium physical characteristics the following results were achieved: Softening of (Treated drinking water, Nile raw water) by removal of hardness (Ca, Mg) by x = 50; 50% P{sub 2}O{sub 5}–50% Na{sub 2}O, Sequestering and agglomerating of (groundwater, wastewater) of some heavy metals as (Fe, Mn) up to 100% removal by x = 60; 60% P{sub 2}O{sub 5}–40% Na{sub 2}O and the electrical properties (pH, EC) were discussed. Results are assuring the possibility of applying PBG for groundwater treatment of high Fe and Mn content. The data show that municipal groundwater supplies become acceptable according to the guidelines of American Chemistry Council for safe drinking water by using of polyphosphates for water treatment.

54 ENVIRONMENTAL SCIENCES↗
NASA NTRS1960

Analytical Investigation of Cycle Characteristics for Advanced Turboelectric Space Power Systems

An investigation was made of the relative influence of turbine inlet temperature, radiator temperature, and turbine efficiency on radiator area for Rankine cycles with rubidium, potassium, and sodium as working fluids. It was determined that, whereas turbine inlet temperature and turbine efficiency have gross effects on radiator size for a given inlet temperature a considerable latitude in the selection of radiator temperature may be accepted with only minor effects on required radiator size. Also investigated was the influence on turbine efficiency and design of the factors that distinguish alkali-metal vapor turbines from conventional gas turbines. The turbine configuration was determined to be a function of the involved working fluids and rotor blade speed. For a given blade speed, the number of stages required for high turbine efficiency was found to vary directly with turbine specific work output, and therefore to vary in the ratio 5 to 2.5 to 1 for sodium, potassium, and rubidium, respectively. Lower blade speeds than employed in conventional gas turbines may be required to satisfy critical stress considerations resulting from the elevated temperatures involved and the criterion of long-duration reliability. This will increase the number of turbine stages necessary to obtain high turbine efficiency and consequently increase turbine weight. The question of moisture formation was discussed and a calculation was made to indicate the nature of the aerodynamic losses due to moisture content. Various means of reducing moisture content were considered, including mechanical removal, increased radiator temperature, inefficient expansion, superheat, and reheat. Sample calculations were made in most cases to indicate their comparative effectiveness and resultant penalty in required radiator area.

Moffitt, Thomas P.↗
NASA NTRSDate not supplied

Center for Isotope Cosmochemistry and Geochronology at NASA Johnson Space Center

The Center for Isotope Cosmochemistry and Geochronology (CICG) at the NASA Johnson Space Center, led by Justin Simon, applies novel elemental and isotopic analytical techniques to understand solar system formation, from processes occurring during the earliest Solar Nebula, to the evolution of planetary bodies during planet formation and differentiation. CICG consists of an integrated suite of labs including dedicated spaces for specialized handling and preparation of meteorites and planetary return samples, metal-free clean chemistry, and mass spectrometry. In addition to a Thermo-Scientific Triton thermal ionization mass spectrometer (TIMS) for high precision isotopic analyses in processed samples, CICG houses two additional mass spectrometry instruments with added laser ablation capabilities for high spatial resolution in-situ measurements: (1) a Thermo-Scientific Element-XR inductively coupled mass spectrometer (ICP-MS) with a Teledyne Photon Machines Analyte Excite+ laser ablation system, and (2) a Nu Sapphire 1700 multi-collector ICP-MS, a large geometry instrument with a multi-pole collision cell for interference removal, with an Applied Spectra J200 tandem laser induced breakdown spectroscopy (LIBS) femto-second laser ablation system. We detail the analytical capabilities of CICG in the context of current and future research projects related to the studies of protoplanetary disk evolution via early-formed Solar System solids, volatile abundances and distribution within the inner solar system, and geochemical and temporal investigations related to planet formation and differentiation. We also highlight opportunities through the relationship with the Center of the Advancement of Space Safety and Mission Assurance Research (CASSMAR) at the University of Texas at El Paso. CICG is open to collaborations and participates in the NASA Facility for Astromaterials Research (NFAR) program, which accepts research proposals for access to the unique facility capabilities.

Jacob B. Setera↗
DOE OSTI2012

Monte Carlo depletion calculations using VESTA 2.1 new features and perspectives

VESTA is a Monte Carlo depletion interface code that is currently under development at IRSN. With VESTA, the emphasis lies on both accuracy and performance, so that the code will be capable of providing accurate and complete answers in an acceptable amount of time compared to other Monte Carlo depletion codes. From its inception, VESTA is intended to be a generic interface code so that it will ultimately be capable of using any Monte-Carlo code or depletion module and that can be tailored to the users needs. A new version of the code (version 2.1.x) will be released in 2012. The most important additions to the code are a burn up dependent isomeric branching ratio treatment to improve the prediction of metastable nuclides such as {sup 242m}Am and the integration of the PHOENIX point depletion module (also developed at IRSN) to overcome some of the limitations of the ORIGEN 2.2 module. The task of extracting and visualising the basic results and also the calculation of physical quantities or other data that can be derived from the basic output provided by VESTA will be the task of the AURORA depletion analysis tool which will be released at the same time as VESTA 2.1.x. The experimental validation database was also extended for this new version and it now contains a total of 35 samples with chemical assay data and 34 assembly decay heat measurements. (authors)

22 GENERAL STUDIES OF NUCLEAR REACTORS↗
DOE OSTI2020

Progress on Advancing the Robotic Air-slot Volumetric Inspection System (RAVIS) for Hanford Under-tank Inspection - 20519

The 27 in-service double-shell tank (DST) systems at Hanford provide interim storage for nearly 56 million gallons of nuclear and hazardous chemical legacy waste. The safe and reliable storage of the waste is critical to the site's extended cleanup mission. While in service, the leak integrity of the DSTs must be demonstrated to satisfy the Washington Administrative Code, inform decisions on tank management, and gauge fitness for continued service beyond originally intended design lives. The carbon steel plates and welds that comprise DST primary tank sidewalls and lower knuckles are routinely 'sampled' for volumetric non-destructive testing using ultrasonic inspection technology to determine whether corrosion pitting, cracking, or general corrosion are occurring that could compromise tank leak integrity. However, the carbon steel plates and welds that comprise the bottoms of primary tanks have not been thoroughly inspected since the DSTs were constructed (i.e., since 1968-1986) due to limited physical access to the exterior tank bottoms. The Robotic Air-slot Volumetric Inspection System, or 'RAVIS,' is being engineered to overcome the challenge of tank bottom in-service inspection. The system will be deployed under primary tanks within the small cooling channels/air-slots in the refractory pads upon which the tanks rest and will use ultrasonic guided wave inspection technology to volumetrically inspect physically inaccessible regions that make up ∼90% of a tank bottom, as well as regions that are physically accessible from the air-slots but comprise only ∼10% of a tank bottom. This paper describes the air-slot sensor and robotic deployment system and focuses on the testing approach and methods that are being applied to support (1) design feedback and performance acceptance (requirement verification) and (2) performance repeatability/reliability assessments (qualification) to ensure the RAVIS is prepared for successful inservice inspections of primary tank bottoms. Test progress made against the test plan, the results of 2019 testing, and the future outlook are included. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2015

Prognostication of LED Remaining Useful Life and Color Stability in the Presence of Contamination

The reliability of LED products may be affected by both luminous flux drop and color shift. Previous research on the topic focuses on either luminous maintenance or color shift. However, luminous flux degradation usually takes very long time to observe in LEDs under normal operating conditions. In this paper, the impact of a VOC (volatile organic compound) contaminated luminous flux and color stability are examined. As a result, both luminous degradation and color shift had been recorded in a short time. Test samples are white, phosphorconverted, high-power LED packages. Absolute radiant flux is measured with integrating sphere system to calculate the luminous flux. Luminous flux degradation and color shift distance were plotted versus aging time to show the degradation pattern. A prognostic health management (PHM) method based on the state variables and state estimator have been proposed in this paper. In this PHM framework, unscented kalman filter (UKF) was deployed as the carrier of all states. During the estimation process, third order dynamic transfer function was used to implement the PHM framework. Both of the luminous flux and color shift distance have been used as the state variable with the same PHM framework to exam the robustness of the method. Predicted remaining useful life is calculated at every measurement point to compare with the tested remaining useful life. The result shows that state estimator can be used as the method for the PHM of LED degradation with respect to both luminous flux and color shift distance. The prediction of remaining useful life of LED package, made by the states estimator and data driven approach, falls in the acceptable errorbounds (20%) after a short training of the estimator.

Lall, Pradeep↗