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All sources NASA NTRS DOE OSTI

DOE OSTI2022

Mapping 3D grain and precipitate structure during in situ mechanical testing of open-cell metal foam using micro-computed tomography and high-energy X-ray diffraction microscopy

Open-cell metal foams are ultra-low-density cellular metals with complex hierarchical structures that span bulk, cell, ligament, and sub-ligament scales and give rise to desirable properties such as high strength-to-weight ratio and excellent energy absorption. Although literature suggests that intrinsic material structures at sub-ligament length scales (e.g., grains and precipitates) play an important role in mechanical behavior of open-cell metal foams, there are very few experimental measurements of such structures in three dimensions and for meaningful volumes of foam. This study seeks to map and track the three-dimensional (3D) grain and precipitate structures of an intact volume of open-cell aluminum foam by advancing microstructural characterization techniques that leverage X-ray micro-computed tomography (μCT) and far-field high-energy X-ray diffraction microscopy (FF-HEDM). A 6%-relative-density aluminum foam sample was mechanically tested in compression while μCT and FF-HEDM measurements were collected at interrupted loading states at beamline 1-ID of the Advanced Photon Source. Further, a new scanning strategy and reconstruction algorithm were established to enable characterization of a foam volume with diameter approximately four times wider than the nominal width of the X-ray beam. The result is a set of maps that detail both the 3D grain and precipitate structures throughout the foam volume at successive strain steps. A novel grain tracking procedure was developed to track individual grains within the foam volume by accounting for the large rigid-body motions that individual ligaments can undergo during mechanical loading. The ability to track grains and precipitate structures in three dimensions throughout large bulk deformation of ultra-low-density polycrystalline materials enables new possibilities for validating numerical models and investigating local failure mechanisms. Furthermore, the methods and procedures developed in this study could be applied to other ultra-low-density structures, such as additively manufactured lattices.

36 MATERIALS SCIENCE↗

DOE OSTI2025

Acoustic waves from the 2023 April 20 SpaceX Starship rocket explosion travelling in the elevated ‘AtmoSOFAR’ channel

SUMMARY The ability to detect low-frequency sounds from distant energetic events depends on the temperature and wind structure of the atmosphere. Thus, from time to time surface-based acoustic detectors may not be able to capture sounds arriving from certain directions. However, the temperature minimum at the tropopause may create an acoustic duct called the ‘AtmoSOFAR’ channel that could transmit acoustic waves laterally—but perhaps not to the ground. If true, then elevated sensors such as those borne aloft by balloons would record the signatures even in regions where ground-based sensors cannot. This has been difficult to prove because high altitude acoustic sources are rare and balloon deployments are sporadic. This work describes the detection and characterization of powerful acoustic waves generated during the launch and terminal explosion of the SpaceX Starship rocket on 2023 April 20 using a pair of microbarometers on a stratospheric balloon. The signals travelled through the AtmoSOFAR channel, carrying information about the size and nature of their source. This channel also appears to leak some acoustic energy to the ground, in agreement with previous studies. The acoustic yield of the Starship terminal explosion was on the order of $10^3$ tons trinitrotoluene equivalent, which agrees with the estimated fuel load of the vehicle to about a factor of 2, but is two orders of magnitude larger than optical estimates. These results support an earlier study that claimed lateral transmission of sound from a smaller rocket through the AtmoSOFAR channel. The transmission of source information through the AtmoSOFAR channel motivates its use for monitoring other natural and anthropogenic events using balloon-borne sensors. This may become increasingly important as more and more private and government entities conduct spacecraft launches and reentries. It may also provide a means of monitoring clear air turbulence and other sound-generating atmospheric phenomena at a distance.

58 GEOSCIENCES↗

NASA NTRS2006

Statistical of a Characterization and the Simulation of a Reverberation Chamber Using Finite-Element Techniques

The statistical characterization of a simulation reverberation chamber is performed by considering a two-dimensional finite element model. This model includes a source to study the particular modal fields that couple into either a transverse electric or transverse magnetic configuration. The analysis includes a characterization of the basic field statistics, max-to-average ratio, normalized standard deviation, stirring ratio, and field uniformity. The shielding effectiveness of an aperture will be studied that will provide some insight into the nature of the fields coupled from a complex to a noncomplex environment.

Bunting, Charles F.↗

NASA NTRS1986

Pb, Sr, Nd, and Hf isotopic constraints on the origin of Hawaiian basalts and evidence for a unique mantle source

The isotopic Pb, Sr, Nd, and Hf compositions of rocks from nine Hawaiian volcanos are determined using the analytical procedures described by Tatsumoto and Unruh (1976) and Patchett and Tatsumoto (1980). The results are presented in graphs, tables, and maps and characterized in detail. The mantle plume, the oceanic lithosphere, and the depleted mantle are identified as distinct sources of the Hawaiian basalts, with different mechanisms responsible for the formation of shield-building tholeiites, late-stage alkalic rocks, and posterosional basalts. The uniqueness of the Hawaiian basalts and the possibility that the Koolau end member represents an undepleted 'primitive' mantle reservoir are considered.

Stille, P.↗

DOE OSTI2016

Global sensitivity analysis in stochastic simulators of uncertain reaction networks

Stochastic models of chemical systems are often subjected to uncertainties in kinetic parameters in addition to the inherent random nature of their dynamics. Uncertainty quantification in such systems is generally achieved by means of sensitivity analyses in which one characterizes the variability with the uncertain kinetic parameters of the first statistical moments of model predictions. In this work, we propose an original global sensitivity analysis method where the parametric and inherent variability sources are both treated through Sobol’s decomposition of the variance into contributions from arbitrary subset of uncertain parameters and stochastic reaction channels. The conceptual development only assumes that the inherent and parametric sources are independent, and considers the Poisson processes in the random-time-change representation of the state dynamics as the fundamental objects governing the inherent stochasticity. Here, a sampling algorithm is proposed to perform the global sensitivity analysis, and to estimate the partial variances and sensitivity indices characterizing the importance of the various sources of variability and their interactions. The birth-death and Schlögl models are used to illustrate both the implementation of the algorithm and the richness of the proposed analysis method. The output of the proposed sensitivity analysis is also contrasted with a local derivative-based sensitivity analysis method classically used for this type of systems.

97 MATHEMATICS AND COMPUTING↗

DOE OSTI2018

Dynamic shear localization of a titanium alloy under high-rate tension characterized by x-ray digital image correlation

Highlights: • First systematic error analyses for XDIC • First XDIC study of Ti-6Al-4V under dynamic tension • Deformation mode transition induces dynamic ductility decrease. • Dynamic shear localization due to rate-dependent microvoid coalescence process. - Abstract: Dynamic and quasi-static tension experiments are conducted on Ti-6Al-4V alloys, with in situ, synchrotron-based, high-speed, x-ray phase contrast imaging implemented to characterize the dynamic deformation and fracture process of Ti alloys at the Advanced Photon Source. X-ray digital imaging correlation (XDIC) is applied for strain field mapping. The size distribution of x-ray speckles are quantified via a morphological analysis, with a mean of ∼20 μm. Systematic error analyses of displacement and strain field measurements are firstly conducted for XDIC, and demonstrate that the displacement and strain errors can be controlled below 0.01 pixel and 0.1%, respectively. Mesoscale strain characteristics measured via XDIC are consistent with and reveal mechanisms for the bulk-scale stress–strain responses. Under dynamic tension, a sharp transition to strain softening occurs when the bulk strain exceeds about 0.04, which leads to a lower dynamic fracture strain (0.08) than the quasi-static one (0.1). The corresponding strain filed mapping demonstrates that shear deformation localizations grow and coalesce rapidly into a narrow shear deformation band under dynamic loading, while tensile deformation and necking progresses gradually under quasi-static loading. Scanning electron microscopy shows that void nucleation occurs mainly at the interface of α and β phases for both quasi-static and dynamic tension. However, microvoids coalesce preferentially along colony boundaries or the boundary α phase under quasi-static tension, but along the maximum shear stress direction (across colonies) under dynamic tension. Fractography of recovered samples also shows consistent features.

36 MATERIALS SCIENCE↗

NASA NTRS2018

A Low Cost Thermal Control Method for Testing in a Mars Environment

Due to the unique thermal vacuum testing requirements for a Mars Rover instrument, NASA Goddard developed a low cost, high fidelity thermal control system utilizing Thermal Electric Coolers (TECs) combined with a heat rejection fluid loop to actively control 8 independent payload thermal boundary zones in a simulated Mars pressure vacuum chamber with a Carbon Dioxide atmosphere. These zones could control instrument components to a specific temperature as a function of time to simulate exact temporal flight boundary predictions.The Mars Organic Molecule Analyzer (MOMA) instrument is a dual source (pyrolysis gas chromatograph and laser desorption) mass spectrometer (MS) based package that detects and characterizes organic molecules, as part of ESA's 2020 ExoMars Rover mission to seek the signs of life on Mars.Due to the unique thermal vacuum testing requirements for a Mars Rover instrument, NASA Goddard developed a low cost, high fidelity thermal control system utilizing Thermal Electric Coolers (TECs) combined with a heat rejection fluid loop to actively control 8 independent payload thermal boundary zones in a simulated Mars pressure vacuum chamber with a Carbon Dioxide atmosphere. These zones could control instrument components to a specific temperature as a function of time to simulate exact temporal flight boundary predictions.The Mars Organic Molecule Analyzer (MOMA) instrument is a dual source (pyrolysis gas chromatograph and laser desorption) mass spectrometer (MS) based package that detects and characterizes organic molecules, as part of ESA's 2020 ExoMars Rover mission to seek the signs of life on Mars.

MOMA↗

DOE OSTI2018

Functional characterization of three GH10 xylanases

Decreased availability of fossil fuels has driven an increased demand for sustainable energy sources such as biofuels. One area of bioenergy research involves development of biocatalysts able to efficiently degrade biomass “waste”‐products, such as substrates derived from corn stover, rather than easily‐fermentable biomass used for food, such as starch from corn kernels. Xylanases are of interest for their ability to hydrolyze hemicellulosic sugars found in plant cell walls, allowing utilization of waste‐derived biomass. In this study, three xylanases of glycoside hydrolase family 10 (GH10) are functionally characterized and optimized for temperature and pH, as well as kinetically analyzed for xylose monomer and oligomer production. These enzymes, GH10‐4, GH10‐9, and GH10‐15, demonstrate activity upon substrates xylan and arabinoxylan. For GH10‐4, optima are 50°C at pH 8 on xylan and 45°C at pH 8 on arabinoxylan. For GH10‐9, optima are 70°C at pH 5 on xylan and 70°C at pH 5 on arabinoxylan. For GH10‐15, optima are 50°C at pH 8 on xylan and 45°C at pH 5 on arabinoxylan. Kinetic analysis reveals GH10‐4 produces xylose (X1), xylobiose (X2), xylotriose (X3), xylotetraose (X4), and xylopentaose (X5) from xylan, while GH10‐9 and GH10‐15 produce X1, X2, and X3. From arabinoxylan, GH10‐4 produces X1, X2, X3, X4, while GH10‐9 and GH10‐15 produce X1, X2, X3. Conclusive kinetic data may suggest applicability of these enzymes for industrial use within biocatalysts and contribute further insight to the functionality of enzymes within GH10. Support or Funding Information The authors are grateful for financial support by the Integrated Biological Sciences Summer Research Program (IBS‐SRP, NSF) at the University of Wisconsin‐Madison and the Great Lakes Bioenergy Research Center (GLBRC) of the U.S. Department of Energy. Presentation travel support is provided by the Ronald E. McNair Scholars Program of Winthrop University. The authors also thank Lai Bergeman, Craig Bingman, Bob Smith, Emily Beebe, Kirk Vander Meulen, Amber Smith, David Wassarman, and John Greenler for professional support.

Park, Jesslyn↗

NASA NTRS2004

Systems Characterization of Combustor Instabilities With Controls Design Emphasis

This effort performed test data analysis in order to characterize the general behavior of combustor instabilities with emphasis on controls design. The analysis is performed on data obtained from two configurations of a laboratory combustor rig and from a developmental aero-engine combustor. The study has characterized several dynamic behaviors associated with combustor instabilities. These are: frequency and phase randomness, amplitude modulations, net random phase walks, random noise, exponential growth and intra-harmonic couplings. Finally, the very cause of combustor instabilities was explored and it could be attributed to a more general source-load type impedance interaction that includes the thermo-acoustic coupling. Performing these characterizations on different combustors allows for more accurate identification of the cause of these phenomena and their effect on instability.

Kopasakis, George↗

NASA NTRS2005

Ferroelectric Devices Emit Charged Particles and Radiation

Devices called solid-state ferroelectric- based sources (SSFBSs) are under development as sources of electrons, ions, ultraviolet light, and x-rays for diverse applications in characterization and processing of materials. Whereas heretofore it has been necessary to use a different device to generate each of the aforementioned species of charged particles or radiation, a single SSFBS can be configured and operated to selectively generate any of the species as needed using a single source. Relative to comparable prior sources based, variously, on field emission, thermionic emission, and gaseous discharge plasmas, SSFBSs demand less power, and are compact and lightweight. An SSFBS exploits the unique physical characteristics of a ferroelectric material in the presence of a high-frequency pulsed electric field. The basic building block of an SSFBS is a ferroelectric cathode -- a ferroelectric wafer with a solid electrode covering its rear face and a grid electrode on its front face (see figure). The application of a voltage pulse -- typically having amplitude of several kilovolts and duration of several nanoseconds -- causes dense surface plasma to form near the grid wires on the front surface.

Bar-Cohen, Yoseph↗

DOE OSTI2017

Proposal of a Categorization of the Disused Sealed Radioactive Sources with a View to Safe - 17285

In the Nuclear and Energy Research Institute (IPEN-CNEN/Brazil) many works to improve and develop characterization of radioactive waste techniques have been deployed by the Radioactive Waste Management Department (IPEN-CNEN/SP). In this line, this work aims to suggest a new categorization of sealed sources, which considers their activities, as suggested by the International Atomic Energy Agency (IAEA), but also the time required for the activity to decrease to a safe value. We considered the sealed sources categorization system suggested by the IAEA and we applied such categorization system to various sources currently stored by institutes of Brazilian Nuclear and Energy Commission (CNEN). Then, we also applied the categorization system defined herein, it follows that the categorization system presented by the IAEA has many applications and their use should not be abandoned. However, since the new proposed categorization systems allow to differentiate sources that in the IAEA system are in the same category, they can help define the long-term management of radioactive waste. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

DOE OSTI2019

Non-residential Electricity Prices: A Review of Data Sources and Estimation Methods

This paper presents a review of electricity price data sources and estimation methods for non-residential consumers, including a detailed empirical study of tariff-based prices collected as part of Lawrence Berkeley Lab's Tariff Analysis Project (TAP). We compare the TAP data to two other data sources: utility-level annual sales, revenues and consumer counts published by the Energy Information Administration (EIA), and the Typical Bills reports published by the Edison Electric Institute. A brief overview of the types of rate structures included in the TAP database illustrates the often complex relationship between the consumer's energy use and the costs they see on their electricity bills. We provide mathematical definitions of the different types of electricity price that are useful in cost-benefit analysis, construct estimation methods appropriate to each data set, compare the results, and evaluate the relative strengths and weaknesses of each approach. We also examine how price variation is driven by differences in season, region, industry business model, and variables characterizing consumer energy use. Tables of regional price estimates for each data source, based on 2015 data, are included in the Appendix to this paper.

29 ENERGY PLANNING, POLICY, AND ECONOMY↗

DOE OSTI2017

Coarse spectral characterization of warm x-rays at the Z facility using a filtered thermoluminescent dosimeter array

A new collimated filtered thermoluminescent dosimeter (TLD) array has been developed at the Z facility to characterize warm x-rays (hν > 10 keV) produced by Z pinch radiation sources. This array includes a Kapton debris shield assembly to protect the TLDs from the source debris, a collimator array to limit the field of view of the TLDs to the source region, a filter wheel containing filters of aluminum, copper and tungsten up to 3 mm thick to independently filter each TLD, and a hermetically sealed cassette containing the TLDs as well as tungsten shielding on the sides and back of the array to minimize scattered radiation reaching the TLDs. Here experimental results from a krypton gas puff and silver wire array shot are analyzed using two different functional forms of the energy spectrum to demonstrate the ability of this diagnostic to consistently extend the upper end of the x-ray spectrum characterization from ~50 keV to >1 MeV.

47 OTHER INSTRUMENTATION↗

DOE OSTI2018

Attribution of gamma-ray background collected by a mobile detector system to its surroundings using panoramic video

Mobile radiation detector systems are important tools for detecting radiological and nuclear sources outside of regulatory control, but due to their mobility, they are subject to complex and varying backgrounds in most realistic operational scenarios. Recent work has found correlations between non-radiological contextual information and gamma-ray spectral features that can be used to decrease false alarm rates, however a more complete understanding of background source terms has been elusive. A measurement campaign developed a full radiological characterization of a controlled facility that roughly corresponded to two city blocks. As part of the campaign, the Radiological Multi-sensor Analysis Platform (RadMAP) collected extensive multi-sensor data. In this work, RadMAP’s panoramic video data were used to visually identify several different materials and quantify the detector response to each material. A linear model was fit between the material responses and radiological features, and the results demonstrate reasonable agreement with ground truth flux measurements for each material. This paper will describe the data collection, processing, and analysis of the gamma-ray and video data from RadMAP. The paper will conclude with perspectives on the applicability of such a method to less controlled environments both with respect to achieving better understanding the sources of variability of background radiation in urban environments and whether such methods could be leveraged in operational scenarios.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2023

Modulation of polar auxin transport identifies the molecular determinants of source–sink carbon relationships and sink strength in poplar

Abstract Source-to-sink carbon (C) allocation driven by the sink strength, i.e., the ability of a sink organ to import C, plays a central role in tissue growth and biomass productivity. However, molecular drivers of sink strength have not been thoroughly characterized in trees. Auxin, as a major plant phytohormone, regulates the mobilization of photoassimilates in source tissues and elevates the translocation of carbohydrates toward sink organs, including roots. In this study, we used an ‘auxin-stimulated carbon sink’ approach to understand the molecular processes involved in the long-distance source–sink C allocation in poplar. Poplar cuttings were foliar sprayed with polar auxin transport modulators, including auxin enhancers (AE) (i.e., IBA and IAA) and auxin inhibitor (AI) (i.e., NPA), followed by a comprehensive analysis of leaf, stem and root tissues using biomass evaluation, phenotyping, C isotope labeling, metabolomics and transcriptomics approaches. Auxin modulators altered root dry weight and branching pattern, and AE increased photosynthetically fixed C allocation from leaf to root tissues. The transcriptome analysis identified highly expressed genes in root tissue under AE condition including transcripts encoding polygalacturonase and β-amylase that could increase the sink size and activity. Metabolic analyses showed a shift in overall metabolism including an altered relative abundance levels of galactinol, and an opposite trend in citrate levels in root tissue under AE and AI conditions. In conclusion, we postulate a model suggesting that the source–sink C relationships in poplar could be fueled by mobile sugar alcohols, starch metabolism-derived sugars and TCA-cycle intermediates as key molecular drivers of sink strength.

59 BASIC BIOLOGICAL SCIENCES↗

DOE OSTI2026

Characterization of Precipitation-Induced Radon Progeny Deposition Events Using a City-Scale Sensor Network

Networks of radiation detectors provide a platform for real-time radioactive source detection and identification in urban environments. Detection algorithms in these systems must adapt to naturally-occurring changes in background, which requires well-characterized relationships between precipitation events and their corresponding radiological signature. Here, we present a quantitative and qualitative description of rain-induced radon progeny deposition events occurring in Chicago from September 2023 to February 2024. We measure ambient gamma radiation levels, precipitation rate, temperature, pressure, and relative humidity in a network of sensor nodes. For each identified precipitation period, we decompose spectra into static- and radon-associated components as defined by a non-negative matrix factorization (NMF) algorithm. We find a consistent power-law relationship between a precipitation-dependent peak of the radon progeny proxy (RPP) and the peak strength of the radon-associated NMF component for most precipitation events. We conduct a case study of a rainfall period with abnormally high levels of implied radon progeny concentration and describe its temporal and spatial evolution. We hypothesize that this phenomenon is due to the air mass path that intersects a uranium-rich region of Wyoming. Finally, we cluster precipitation events into three distinct categories. One category roughly corresponds to events with deep low-pressure systems and high relative radon concentration, while another is characteristic of light stratiform rain with slightly higher temperatures and intermediate relative radon concentration. The third category appears to contain weak-gradient or lake breeze convection showers with intermittent precipitation and low relative radon concentration. These findings suggest that radiological anomaly detection could be improved by training unique background models corresponding to each category of meteorological event.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

NASA NTRS2012

Characterization Approaches to Place Invariant Sites on SI-Traceable Scales

The effort to understand the Earth's climate system requires a complete integration of remote sensing imager data across time and multiple countries. Such an integration necessarily requires ensuring inter-consistency between multiple sensors to create the data sets needed to understand the climate system. Past efforts at inter-consistency have forced agreement between two sensors using sources that are viewed by both sensors at nearly the same time, and thus tend to be near polar regions over snow and ice. The current work describes a method that would provide an absolute radiometric calibration of a sensor rather than an inter-consistency of a sensor relative to another. The approach also relies on defensible error budgets that eventually provides a cross comparison of sensors without systematic errors. The basis of the technique is a model-based, SI-traceable prediction of at-sensor radiance over selected sites. The predicted radiance would be valid for arbitrary view and illumination angles and for any date of interest that is dominated by clear-sky conditions. The effort effectively works to characterize the sites as sources with known top-of-atmosphere radiance allowing accurate intercomparison of sensor data that without the need for coincident views. Data from the Advanced Spaceborne Thermal Emission and Reflection and Radiometer (ASTER), Enhanced Thematic Mapper Plus (ETM+), and Moderate Resolution Imaging Spectroradiometer (MODIS) are used to demonstrate the difficulties of cross calibration as applied to current sensors. Special attention is given to the differences caused in the cross-comparison of sensors in radiance space as opposed to reflectance space. The radiance comparisons lead to significant differences created by the specific solar model used for each sensor. The paper also proposes methods to mitigate the largest error sources in future systems. The results from these historical intercomparisons provide the basis for a set of recommendations to ensure future SI-traceable cross calibration using future missions such as CLARREO and TRUTHS. The paper describes a proposed approach that relies on model-based, SI-traceable predictions of at-sensor radiance over selected sites. The predicted radiance would be valid for arbitrary view and illumination angles and for any date of interest that is dominated by clear-sky conditions. The basis of the method is highly accurate measurements of at-sensor radiance of sufficient quality to understand the spectral and BRDF characteristics of the site and sufficient historical data to develop an understanding of temporal effects from changing surface and atmospheric conditions.

Thome, Kurtis↗

DOE OSTI2019

Dendrite-Free Flexible Fiber-Shaped Zn Battery with Long Cycle Life in Water and Air

Fiber-shaped aqueous rechargeable Zn batteries (FARZBs) show flexibility, good reliability, cost-effectiveness, high energy/power densities, and high safety that have attracted increasing attention as promising energy storage devices for future wearable applications. However, the development of FARZB is limited by its poor cycling life and inferior charge-discharge performance, mainly suffering from zinc dendrite growth and increasing electrode irreversibility. In this work, dendrite-free fiber-shaped Zn//Co 3 O 4 rechargeable batteries with a long cycle life tested in water and air, are obtained via tuning the surface binding energy of Zn on the anode using the zincophilic N,O-functional carbon fiber, as well as engineering the Co 3 O 4 cathode with a nanowire array structure. The fiber-shaped Zn//Co 3 O 4 full battery demonstrates remarkable long cycle life in water and air with high energy density, impressive flexibility, and excellent waterproof ability (fully immersed and charged/discharged under water for more than 33 h for 3000 cycles with capacity retention of ≈80%). The reversible electrochemical mechanisms of the FARZBs, without obvious zinc dendrite deposits and structural change of Co 3 O 4 nanowires, are confirmed by a series of characterizations. Furthermore, these results demonstrate that the FARZBs are promising power sources for emerging wearable electronics.

25 ENERGY STORAGE↗