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NASA NTRS2012

Increased Accuracy in the Measurement of the Dielectric Constant of Seawater at 1.413 GHz

This paper describes the latest results for the measurements of the dielectric constant at 1.413 GHz by using a resonant cavity technique. The purpose of these measurements is to develop an accurate relationship for the dependence of the dielectric constant of sea water on temperature and salinity which is needed by the Aquarius inversion algorithm to retrieve salinity. Aquarius is the major instrument on the Aquarius/SAC-D observatory, a NASA/CONAE satellite mission launched in June of20ll with the primary mission of measuring global sea surface salinity to an accuracy of 0.2 psu. Aquarius measures salinity with a 1.413 GHz radiometer and uses a scatterometer to compensate for the effects of surface roughness. The core part of the seawater dielectric constant measurement system is a brass microwave cavity that is resonant at 1.413 GHz. The seawater is introduced into the cavity through a capillary glass tube having an inner diameter of 0.1 mm. The change of resonance frequency and the cavity Q value are used to determine the real and imaginary parts of the dielectric constant of seawater introduced into the thin tube. Measurements are automated with the help of software developed at the George Washington University. In this talk, new results from measurements made since September 2010 will be presented for salinities 30, 35 and 38 psu with a temperature range of O C to 350 C in intervals of 5 C. These measurements are more accurate than earlier measurements made in 2008 because of a new method for measuring the calibration constant using methanol. In addition, the variance of repeated seawater measurements has been reduced by letting the system stabilize overnight between temperature changes. The new results are compared to the Kline Swift and Meissner Wentz model functions. The importance of an accurate model function will be illustrated by using these model functions to invert the Aquarius brightness temperature to get the salinity values. The salinity values will be compared to co-located in situ data collected by Argo buoys.

Zhou, Y.↗

NASA NTRS2012

Active Region Moss: Doppler Shifts from Hinode/EIS Observations

Studying the Doppler shifts and the temperature dependence of Doppler shifts in moss regions can help us understand the heating processes in the core of the active regions. In this paper we have used an active region observation recorded by the Extreme-ultraviolet Imaging Spectrometer (EIS) onboard Hinode on 12-Dec- 2007 to measure the Doppler shifts in the moss regions. We have distinguished the moss regions from the rest of the active region by defining a low density cut-off as derived by Tripathi et al. (2010). We have carried out a very careful analysis of the EIS wavelength calibration based on the method described in Young, O Dwyer and Mason (2012). For spectral lines having maximum sensitivity between log T = 5.85 and log T = 6.25 K, we find that the velocity distribution peaks at around 0 km/s with an estimated error of 4 km/s. The width of the distribution decreases with temperature. The mean of the distribution shows a blue shift which increases with increasing temperature and the distribution also shows asymmetries towards blue-shift. Comparing these results with observables predicted from different coronal heating models, we find that these results are consistent with both steady and impulsive heating scenarios. Further observational constraints are needed to distinguish between these two heating scenarios.

Tripathi, Durgesh↗

NASA NTRS2011

A Novel Nonintrusive Method to Resolve the Thermal Dome Effect of Pyranometers: Radiometric Calibration and Implications

Traditionally the calibration equation for pyranometers assumes that the measured solar irradiance is solely proportional to the thermopile s output voltage; therefore, only a single calibration factor is derived. This causes additional measurement uncertainties because it does not capture sufficient information to correctly account for a pyranometer s thermal effect. In our updated calibration equation, temperatures from the pyranometer's dome and case are incorporated to describe the instrument's thermal behavior, and a new set of calibration constants are determined, thereby reducing measurement uncertainties. In this paper, we demonstrate why a pyranometer's uncertainty using the traditional calibration equation is always larger than a few percent, but with the new approach can become much less than 1% after the thermal issue is resolved. The highlighted calibration results are based on NIST traceable light sources under controlled laboratory conditions. The significance of the new approach lends itself to not only avoiding the uncertainty caused by a pyranometer's thermal effect but also the opportunity to better isolate and characterize other instrumental artifacts, such as angular response and nonlinearity of the thermopile, to further reduce additional uncertainties. We also discuss some of the implications, including an example of how the thermal issue can potentially impact climate studies by evaluating aerosol s direct radiative effect using field measurements with and without considering the pyranometer s thermal effect. The results of radiative transfer model simulation show that a pyranometer s thermal effect on solar irradiance measurements at the surface can be translated into a significant alteration of the calculated distribution of solar energy inside the column atmosphere.

Ji. Q.↗

NASA NTRS2008

New Techniques to Evaluate the Incendiary Behavior of Insulators

New techniques for evaluating the incendiary behavior of insulators is presented. The onset of incendive brush discharges in air is evaluated using standard spark probe techniques for the case simulating approaches of an electrically grounded sphere to a charged insulator in the presence of a flammable atmosphere. However, this standard technique is unsuitable for the case of brush discharges that may occur during the charging-separation process for two insulator materials. We present experimental techniques to evaluate this hazard in the presence of a flammable atmosphere which is ideally suited to measure the incendiary nature of micro-discharges upon separation, a measurement never before performed. Other measurement techniques unique to this study include; surface potential measurements of insulators before, during and after contact and separation, as well as methods to verify fieldmeter calibrations using a charge insulator surface opposed to standard high voltage plates. Key words: Kapton polyimide film, incendiary discharges, brush discharges, contact and frictional electrification, ignition hazards, insulators, contact angle, surface potential measurements.

Buhler, Charles↗

NASA NTRS2013

The IMACS Cluster Building Survey. I. Description of the Survey and Analysis Methods

The IMACS Cluster Building Survey uses the wide field spectroscopic capabilities of the IMACS spectrograph on the 6.5 m Baade Telescope to survey the large-scale environment surrounding rich intermediate-redshift clusters of galaxies. The goal is to understand the processes which may be transforming star-forming field galaxies into quiescent cluster members as groups and individual galaxies fall into the cluster from the surrounding supercluster. This first paper describes the survey: the data taking and reduction methods. We provide new calibrations of star formation rates (SFRs) derived from optical and infrared spectroscopy and photometry. We demonstrate that there is a tight relation between the observed SFR per unit B luminosity, and the ratio of the extinctions of the stellar continuum and the optical emission lines.With this, we can obtain accurate extinction-corrected colors of galaxies. Using these colors as well as other spectral measures, we determine new criteria for the existence of ongoing and recent starbursts in galaxies.

IMACS↗

NASA NTRS2013

Quantification of Residual Stress from Photonic Signatures of Fused Silica

A commercially available grey-field polariscope (GFP) instrument for photoelastic examination is used to assess impact damage inflicted upon the outer-most pane of Space Shuttle windows made from fused silica. A method and apparatus for calibration of the stress-optic coefficient using four-point bending is discussed. The results are validated on known material (acrylic) and are found to agree with literature values to within 6%. The calibration procedure is then applied to fused-silica specimens and the stress-optic coefficient is determined to be 2.43 +/- 0.54 x 10(exp -12)/Pa. Fused silica specimens containing impacts artificially made at NASA's Hypervelocity Impact Technology Facility (HIT-F), to simulate damage typical during space flight, are examined. The damage sites are cored from fused silica window carcasses and examined with the GFP. The calibrated GFP measurements of residual stress patterns surrounding the damage sites are presented. Keywords: Glass, fused silica, photoelasticity, residual stress

Cramer, K. Elliott↗

DOE OSTI2015

On the Statistical Calibration of Physical Models

ABSTRACT We introduce a novel statistical calibration framework for physical models, relying on probabilistic embedding of model discrepancy error within the model. For clarity of illustration, we take the measurement errors out of consideration, calibrating a chemical model of interest with respect to a more detailed model, considered as “truth” for the present purpose. We employ Bayesian statistical methods for such model‐to‐model calibration and demonstrate their capabilities on simple synthetic models, leading to a well‐defined parameter estimation problem that employs approximate Bayesian computation. The method is then demonstrated on two case studies for calibration of kinetic rate parameters for methane air chemistry, where ignition time information from a detailed elementary‐step kinetic model is used to estimate rate coefficients of a simple chemical mechanism. We show that the calibrated model predictions fit the data and that uncertainty in these predictions is consistent in a mean‐square sense with the discrepancy from the detailed model data.

Sargsyan, K.↗

DOE OSTI2022

Radon-222 Charcoal Canister Steady State Model Calibrations Performed in a Highly Controlled Environmental Chamber and a Natural Indoor Environment

Charcoal canisters are a common method of 222 Rn screening. The calibrations of different batches of activated charcoal used in different canister designs are typically performed in large volume controlled environmental chambers with known and controlled radon concentration, temperature, and humidity. Radon screening could be facilitated in locations without ready access to environmental chambers if canisters could be accurately calibrated and undergo quality control in less controlled environments. This study compares charcoal canister calibrations from a highly controlled radon chamber with calibrations from a basement storage area experiencing temporally varying radon. In addition, the impacts of exposure time and spectral region of interest selection on calibration accuracy are investigated by comparing calibrations calculated using three different choices. Approximately 30 mo after calibrations were completed, groups of canisters were exposed for different durations of time to investigate measurement accuracy and calibration validity over an extended time. A digital simulation of charcoal canister kinetics was also performed to establish limits on how stable radon must be in a space for equilibrium-based calibration to be performed there. Overall, the accuracy of measurements using calibrations from each space differed by less than 10% after 2 d exposure time, showing that carefully controlled conditions are not necessary for the accurate calibration of charcoal canisters. Furthermore, measurement accuracy differed by less than 2% for different spectral region selections. Accuracy improved slightly with canister exposure duration. Simulations suggest that radon instability is most tolerable near the beginning of canister calibration exposures, but this merits further experimental study.

07 ISOTOPE AND RADIATION SOURCES↗

NASA NTRS2016

The New Sun-Sky-Lunar Cimel CE318-T Multiband Photometer - A Comprehensive Performance Evaluation

This paper presents the new photometer CE318-T, able to perform daytime and night-time photometric measurements using the sun and the moon as light source. Therefore,this new device permits a complete cycle of diurnal aerosol and water vapour measurements valuable to enhance atmospheric monitoring to be extracted. In this study wehave found significantly higher precision of triplets when comparing the CE318-T master instrument and the Cimel AErosol RObotic NET work (AERONET) master (CE318-AERONET) triplets as a result of the new CE318-T tracking system. Regarding the instrument calibration, two new methodologies to transfer the calibration from a reference instrument using only daytime measurements (Sun Ratio and Sun-Moon gain factor techniques) are presented and discussed. These methods allow the reduction of the previous complexities inherent to nocturnal calibration. A quantitative estimation of CE318-T AOD uncertainty by means of error propagation theory during daytime revealed AOD uncertainties (u(sup D)(sub AOD)) for Langley-calibrated instruments similar to the expected values for other reference instruments (0.002-0.009). We have also found u(sup D)(sub AOD) values similar to the values reported in sun photometry for field instruments (approximately 0.015). In the case of the night-time period, the CE318-T-estimated standard combined uncertainty (u(sup N)(sub AOD)) is dependent not only on the calibration technique but also on illumination conditions and the instrumental noise. These values range from 0.011-0.018 for Lunar Langley-calibrated instruments to 0.012-0.021 for instruments calibrated using the Sun Ratio technique. In the case of moon-calibrated instruments using the Sun-Moon gain factor method and sun calibrated using the Langley technique, we found u(sup N)(sub AOD) ranging from 0.016 to 0.017 (up to 0.019 in 440 nm channel), not dependent on any lunar irradiance model. A subsequent performance evaluation including CE318-T and collocated measurements from independent reference instruments has served to assess the CE318-T performance as well as to confirm its estimated uncertainty. Daytime AOD evaluation, performed at Izana station from March to June 2014, encompassed measurements from a reference CE318-T, a CE318-AERONET master instrument, a Precision Filter Radiometer (PFR) and a Precision Spectroradiometer (PSR) prototype, reporting low AOD discrepancies between the four instruments (up to 0.006). The nocturnal AOD evaluation was performed using CE318-T- and starphotometer-collocated measurements and also by means of a day/night coherence transition test using the CE318-T master instrument and the CE318 daytime data from the CE318-AERONET master instrument. Results showed low discrepancies with the star photometer at 870 and 500 nm channels(less tna or equal to 0.013) and differences with AERONET daytime data (1 h after and before sunset and sunrise) in agreement with the estimated u(sup N)(sub AOD) values at all illumination conditions in the case of channels within the visible spectral range, and only for high moon's illumination conditions in the case of near infrared channels. Perceptible water vapour (PWV) validation showed a good agreement between CE318-T and Global Navigation Satellite System (GNSS) PWV values for all illumination conditions, within the expected precision for sun photometry. Finally, two case studies have been included to highlight the ability of the new CE318-T to capture the diurnal cycle of aerosols and water vapour as well as short-term atmospheric variations, critical for climate studies.

Barreto, Africa↗

DOE OSTI2017

Detecting Proxima b’s Atmosphere with JWST Targeting CO{sub 2} at 15 μ m Using a High-pass Spectral Filtering Technique

Exoplanet Proxima b will be an important laboratory for the search for extraterrestrial life for the decades ahead. Here, we discuss the prospects of detecting carbon dioxide at 15 μ m using a spectral filtering technique with the Medium Resolution Spectrograph (MRS) mode of the Mid-Infrared Instrument (MIRI) on the James Webb Space Telescope ( JWST ). At superior conjunction, the planet is expected to show a contrast of up to 100 ppm with respect to the star. At a spectral resolving power of R = 1790–2640, about 100 spectral CO{sub 2} features are visible within the 13.2–15.8 μ m (3B) band, which can be combined to boost the planet atmospheric signal by a factor of 3–4, depending on the atmospheric temperature structure and CO{sub 2} abundance. If atmospheric conditions are favorable (assuming an Earth-like atmosphere), with this new application to the cross-correlation technique, carbon dioxide can be detected within a few days of JWST observations. However, this can only be achieved if both the instrumental spectral response and the stellar spectrum can be determined to a relative precision of ≤1 × 10{sup −4} between adjacent spectral channels. Absolute flux calibration is not required, and the method is insensitive to the strong broadband variability of the host star. Precise calibration of the spectral features of the host star may only be attainable by obtaining deep observations of the system during inferior conjunction that serve as a reference. The high-pass filter spectroscopic technique with the MIRI MRS can be tested on warm Jupiters, Neptunes, and super-Earths with significantly higher planet/star contrast ratios than the Proxima system.

79 ASTRONOMY AND ASTROPHYSICS↗

NASA NTRS1997

Development and Operation of a Material Identification and Discrimination Imaging Spectroradiometer

Many imaging applications require quantitative determination of a scene's spectral radiance. This paper describes a new system capable of real-time spectroradiometric imagery. Operating at a full-spectrum update rate of 30Hz, this imager is capable of collecting a 30 point spectrum from each of three imaging heads: the first operates from 400 nm to 950 nm, with a 2% bandwidth; the second operates from 1.5 micro-m to 5.5 micro-m with a 1.5% bandwidth; the third operates from 5 micro-m to 12 micro-m, also at a 1.5% bandwidth. Standard image format is 256 x 256, with 512 x 512 possible in the VIS/NIR head. Spectra of up to 256 points are available at proportionately lower frame rates. In order to make such a tremendous amount of data more manageable, internal processing electronics perform four important operations on the spectral imagery data in real-time. First, all data in the spatial/spectral cube of data is spectro-radiometrically calibrated as it is collected. Second, to allow the imager to simulate sensors with arbitrary spectral response, any set of three spectral response functions may be loaded into the imager including delta functions to allow single wavelength viewing; the instrument then evaluates the integral of the product of the scene spectral radiances and the response function. Third, more powerful exploitation of the gathered spectral radiances can be effected by application of various spectral-matched filtering algorithms to identify pixels whose relative spectral radiance distribution matches a sought-after spectral radiance distribution, allowing materials-based identification and discrimination. Fourth, the instrument allows determination of spectral reflectance, surface temperature, and spectral emissivity, also in real-time. The spectral imaging technique used in the instrument allows tailoring of the frame rate and/or the spectral bandwidth to suit the scene radiance levels, i.e., frame rate can be reduced, or bandwidth increased to improve SNR when viewing low radiance scenes. The unique challenges of design and calibration are described. Pixel readout rates of 160 MHz, for full frame readout rates of 1000 Hz (512 x 512 image) present the first challenge; processing rates of nearly 600 million integer operations per second for sensor emulation, or over 2 billion per second for matched filtering, present the second. Spatial and spectral calibration of 66,536 pixels (262,144 for the 512 x 512 version) and up to 1,000 spectral positions mandate novel decoupling methods to keep the required calibration memory to a reasonable size. Large radiometric dynamic range also requires care to maintain precision operation with minimum memory size.

Dombrowski, Mark↗

DOE OSTI2025

The track-length extension fitting algorithm for energy measurement of interacting particles in liquid argon TPCs and its performance with ProtoDUNE-SP data

This paper introduces a novel track-length extension fitting algorithm for measuring the kinetic energies of inelastically interacting particles in liquid argon time projection chambers (LArTPCs). The algorithm finds the most probable offset in track length for a track-like object by comparing the measured ionization density as a function of position with a theoretical prediction of the energy loss as a function of the energy, including models of electron recombination and detector response. The algorithm can be used to measure the energies of particles that interact before they stop, such as charged pions that are absorbed by argon nuclei. The algorithm's energy measurement resolutions and fractional biases are presented as functions of particle kinetic energy and number of track hits using samples of stopping secondary charged pions in data collected by the ProtoDUNE-SP detector, and also in a detailed simulation. Additional studies describe the impact of the dE/dx model on energy measurement performance. The method described in this paper to characterize the energy measurement performance can be repeated in any LArTPC experiment using stopping secondary charged pions.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2015

Characterization of cartridge filters from the IEA-R1 Nuclear Reactor

The management of radioactive waste ensures safety to human health and the environment nowadays and for the future, without overwhelming the upcoming generations. The primary characterization of radioactive waste is one of the main steps in the management of radioactive waste. This step permits to choose the best treatment for the radioactive waste before forwarding it to its final disposal. The aim of the present work is the primary characterization of cartridge filters from the IEA-R1 nuclear reactor utilizing gamma-ray spectrometry, and the method of Monte Carlo for calibration. The IEA-R1 is located in the Nuclear and Energy Research Institute (IPEN - CNEN) in the city of Sao Paulo, Brazil. Cartridge filters are used for purification of the cooling water that is pumped through the core of the pool type nuclear research reactors. Once worn out, these filters are replaced and then become radioactive waste. Determination of the radioactive inventory is of paramount importance in the management of such radioactive waste, and one of the main methods for doing so is the gamma-ray spectrometry, which can identify and quantify high energy photon emitters. The technique chosen for the characterization of radioactive waste in the present work is the gamma-ray spectrometry with High purity Germanium (HPGe) detectors. From the energy identified in the experimental spectrum, three radioisotopes were identified in the cartridge filter: {sup 108m}Ag, {sup 110m}Ag, {sup 60}Co. For the estimated activity of the filter, the calibration in efficiency was made utilizing the MCNP4C code of the Monte Carlo method. Such method was chosen because there is no standard source available in the same geometry of the cartridge filter, therefore a simulation had to be developed in order to reach a calibration equation, necessary to estimate the activity of the radioactive waste. The results presented an activity value in the order of MBq for all radioisotopes. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

DOE OSTI2023

INVESTIGATION OF HUMAN RELIABILITY ANALYSIS METHODS FOR ANALYZING PRE-INITIATORS

As a type of human actions defined in human reliability analysis (HRA), pre-initiator refers to the human actions that may lead to the unavailability of systems, typically committed during maintenance, test, or calibration. This paper investigates representative HRA methods used for analyzing pre-initiators. The HRA methods are Technique for Human Error Rate Prediction (THERP), Korean Standard HRA (K-HRA) and Standard Plant Risk HRA (SPAR-H). In this paper, characteristics of each HRA method are compared for qualitative and quantification aspects. Two pre-initiators, i.e., a calibration task and a valve restoration task, are analyzed using the HRA methods to compare human error probabilities. Then, insights from the analysis and additional research requirements are discussed in this paper.

99 GENERAL AND MISCELLANEOUS↗

DOE OSTI2023

INVESTIGATION OF HUMAN RELIABILITY ANALYSIS METHODS FOR ANALYZING PRE-INITIATORS

99 GENERAL AND MISCELLANEOUS↗

DOE OSTI2026

Towards Robust Calibration of the AWSD Reactive Burn Model

Calibration of a reactive burn model for detonation of high explosive is an important step towards predictive hy drodynamic simulations of detonation. A typical calibration consists of varying model parameters (e.g., rate constants, activation energies) until results of hydrodynamic simulations match the experimental data for a certain set of ex periments. Hydrodynamic simulations of the dependence of steady detonation velocity on the radius of a cylindrical high-explosive charge - often used in such calibrations - can be computationally expensive. In this work, we propose a method where such expensive simulations are performed infrequently, and only to parameterize and refine a surrogate model for the dependence of the detonation velocity on calibrated parameters. The method is developed, implemented and applied to an example problem - calibration of the AWSD reactive burn model for important high explosive PBX 9502. Two different flavors of the surrogate model are investigated, and the calibration is performed successfully.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

DOE OSTI2015

Precise and direct method for the measurement of the torsion spring constant of the atomic force microscopy cantilevers

A direct method for the evaluation of the torsional spring constants of the atomic force microscope cantilevers is presented in this paper. The method uses a nanoindenter to apply forces at the long axis of the cantilever and in the certain distance from it. The torque vs torsion relation is then evaluated by the comparison of the results of the indentations experiments at different positions on the cantilever. Next, this relation is used for the precise determination of the torsional spring constant of the cantilever. The statistical analysis shows that the standard deviation of the calibration measurements is equal to approximately 1%. Furthermore, a simple method for calibration of the photodetector’s lateral response is proposed. The overall procedure of the lateral calibration constant determination has the accuracy approximately equal to 10%.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

NASA NTRS1986

Further investigation into calibration techniques for a magnetic suspension and balance system

Calibrations performed on three different magnetic cores for wind tunnel models suspended in the Southampton University Magnetic Suspension and Balance System (SUMSBS) are detailed. The first core investigated was the Southampton University pilot Superconducting Solenoid model, first flown in July 1983. Static calibrations of lift force, drag force and pitching moment, together with lift force and pitching moment calibrations determined by the dynamic method are detailed in this report. Other types of core investigated in a similar manner were conventional permanent magnets, Alnico and samarium-cobalt. All static calibrations gave a linear dependence of force on electromagnet current as expected. Dynamic calibrations are faster to perform but are proving to be not as easily analyzed as static calibrations. There are still some effects to be explained but dynamic lift calibration results were obtained agreeing to within 2 percent of the static calibration value.

Eskins, J.↗