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At least 1,423 records · Page 79

Extraction of mechanical properties of materials through deep learning from instrumented indentation

Instrumented indentation has been developed and widely utilized as one of the most versatile and practical means of extracting mechanical properties of materials. This method is particularly desirable for those applications where it is difficult to experimentally determine the mechanical properties using stress–strain data obtained from coupon specimens. Such applications include material processing and manufacturing of small and large engineering components and structures involving the following: three-dimensional (3D) printing, thin-film and multilayered structures, and integrated manufacturing of materials for coupled mechanical and functional properties. Here, we utilize the latest developments in neural networks, including a multifidelity approach whereby deep-learning algorithms are trained to extract elastoplastic properties of metals and alloys from instrumented indentation results using multiple datasets for desired levels of improved accuracy. We have established algorithms for solving inverse problems by recourse to single, dual, and multiple indentation and demonstrate that these algorithms significantly outperform traditional brute force computations and function-fitting methods. Moreover, we present several multifidelity approaches specifically for solving the inverse indentation problem which 1) significantly reduce the number of high-fidelity datasets required to achieve a given level of accuracy, 2) utilize known physical and scaling laws to improve training efficiency and accuracy, and 3) integrate simulation and experimental data for training disparate datasets to learn and minimize systematic errors. The predictive capabilities and advantages of these multifidelity methods have been assessed by direct comparisons with experimental results for indentation for different commercial alloys, including two wrought aluminum alloys and several 3D printed titanium alloys.

36 MATERIALS SCIENCE↗

GNOSIS: THE FIRST INSTRUMENT TO USE FIBER BRAGG GRATINGS FOR OH SUPPRESSION

The near-infrared is an important part of the spectrum in astronomy, especially in cosmology because the light from objects in the early universe is redshifted to these wavelengths. However, deep near-infrared observations are extremely difficult to make from ground-based telescopes due to the bright background from the atmosphere. Nearly all of this background comes from the bright and narrow emission lines of atmospheric hydroxyl (OH) molecules. The atmospheric background cannot be easily removed from data because the brightness fluctuates unpredictably on short timescales. The sensitivity of ground-based optical astronomy far exceeds that of near-infrared astronomy because of this long-standing problem. GNOSIS is a prototype astrophotonic instrument that utilizes 'OH suppression fibers' consisting of fiber Bragg gratings and photonic lanterns to suppress the 103 brightest atmospheric emission doublets between 1.47 and 1.7 {mu}m. GNOSIS was commissioned at the 3.9 m Anglo-Australian Telescope with the IRIS2 spectrograph to demonstrate the potential of OH suppression fibers, but may be potentially used with any telescope and spectrograph combination. Unlike previous atmospheric suppression techniques GNOSIS suppresses the lines before dispersion and in a manner that depends purely on wavelength. We present the instrument design and report the results of laboratory and on-sky tests from commissioning. While these tests demonstrated high throughput ( Almost-Equal-To 60%) and excellent suppression of the skylines by the OH suppression fibers, surprisingly GNOSIS produced no significant reduction in the interline background and the sensitivity of GNOSIS+IRIS2 is about the same as IRIS2. It is unclear whether the lack of reduction in the interline background is due to physical sources or systematic errors as the observations are detector noise dominated. OH suppression fibers could potentially impact ground-based astronomy at the level of adaptive optics or greater. However, until a clear reduction in the interline background and the corresponding increasing in sensitivity is demonstrated optimized OH suppression fibers paired with a fiber-fed spectrograph will at least provide a real benefit at low resolving powers.

79 ASTRONOMY AND ASTROPHYSICS↗

KEPLER MISSION STELLAR AND INSTRUMENT NOISE PROPERTIES REVISITED

An earlier study of the Kepler Mission noise properties on timescales of primary relevance to detection of exoplanet transits found that higher than expected noise followed, to a large extent, from the stars rather than instrument or data analysis performance. The earlier study over the first six quarters of Kepler data is extended to the full four years ultimately comprising the mission. Efforts to improve the pipeline data analysis have been successful in reducing noise levels modestly as evidenced by smaller values derived from the current data products. The new analyses of noise properties on transit timescales show significant changes in the component attributed to instrument and data analysis, with essentially no change in the inferred stellar noise. We also extend the analyses to timescales of several days, instead of several hours to better sample stellar noise that follows from magnetic activity. On the longer timescale there is a shift in stellar noise for solar-type stars to smaller values in comparison to solar values.

79 ASTRONOMY AND ASTROPHYSICS↗

Formaldehyde chemistry in cometary ices: on the prospective detection of NH{sub 2}CH{sub 2}OH, HOCH{sub 2}OH, and POM by the on-board ROSINA instrument of the Rosetta mission

The thermal reactivity of a water-dominated cometary ice analog containing H{sub 2}CO and NH{sub 3} is investigated by means of Fourier transform infrared spectroscopy, mass spectrometry, and B3LYP calculations. Three products are characterized by these techniques: aminomethanol (NH{sub 2}CH{sub 2}OH), methyleneglycol (HOCH{sub 2}OH), and polyoxymethylene (POM, HO-(CH{sub 2}-O) {sub n}-H). Their formation strongly depends on the initial NH{sub 3}/H{sub 2}CO ratio. In addition, the influence of the initial ice composition on the thermal stability of POM has also been investigated. It is shown that POM formed during warming of the ices consists of short-chain polymers (i.e., oligomers of formaldehyde HO-(CH{sub 2}-O) {sub n}-H, n < 5), which are volatile at temperatures higher than 200 K. This suggests that gas-phase detection by the ROSINA instrument on board the Rosetta mission would be the most appropriate method to detect POM. Moreover, the mass spectra presented in this work might help in the interpretation of data that will be recorded by this instrument. Finally, a new scenario to explain the distributed source of formaldehyde observed in comets is discussed.

79 ASTRONOMY AND ASTROPHYSICS↗

Robustness of cosmic birefringence measurement against Galactic foreground emission and instrumental systematics

The polarization of the cosmic microwave background (CMB) can be used to search for parity-violating processes like that predicted by a Chern-Simons coupling to a light pseudoscalar field. Such an interaction rotates E modes into E modes in the observed CMB signal through an effect known as cosmic birefringence. Even though isotropic birefringence can be confused with the rotation produced by a miscalibration of the detectors' polarization angles, the degeneracy between both effects is broken when Galactic foreground emission is used as a calibrator. Here, in this work, we use realistic simulations of the High-Frequency Instrument of the Planck mission to test the impact that Galactic foreground emission and instrumental systematics have on the recent birefringence measurements obtained through this technique. Our results demonstrate the robustness of the methodology against the miscalibration of polarization angles and other systematic effects, like intensity-to-polarization leakage, beam leakage, or cross-polarization effects. However, our estimator is sensitive to the EB correlation of polarized foreground emission. Here we propose to correct the bias induced by dust EB by modeling the foreground signal with templates produced in Bayesian component-separation analyses that fit parametric models to CMB data. Acknowledging the limitations of currently available dust templates like that of the Commander sky model, high-precision CMB data and a characterization of dust beyond the modified blackbody paradigm are needed to obtain a definitive measurement of cosmic birefringence in the future.

79 ASTRONOMY AND ASTROPHYSICS↗

“MODAL NOISE” IN SINGLE-MODE FIBERS: A CAUTIONARY NOTE FOR HIGH PRECISION RADIAL VELOCITY INSTRUMENTS

Exploring the use of single-mode fibers (SMFs) in high precision Doppler spectrometers has become increasingly attractive since the advent of diffraction-limited adaptive optics systems on large-aperture telescopes. Spectrometers fed with these fibers can be made significantly smaller than typical “seeing-limited” instruments, greatly reducing cost and overall complexity. Importantly, classical mode interference and speckle issues associated with multi-mode fibers, also known as “modal noise,” are mitigated when using SMFs, which also provide perfect radial and azimuthal image scrambling. However, SMFs do support multiple polarization modes, an issue that is generally ignored for larger-core fibers given the large number of propagation modes. Since diffraction gratings used in most high resolution astronomical instruments have dispersive properties that are sensitive to incident polarization changes, any birefringence variations in the fiber can cause variations in the efficiency profile, degrading illumination stability. Here we present a cautionary note outlining how the polarization properties of SMFs can affect the radial velocity (RV) measurement precision of high resolution spectrographs. This work is immediately relevant to the rapidly expanding field of diffraction-limited, extreme precision RV spectrographs that are currently being designed and built by a number of groups.

79 ASTRONOMY AND ASTROPHYSICS↗

VISION: a modular AI assistant for natural human-instrument interaction at scientific user facilities

Scientific user facilities, such as synchrotron beamlines, are equipped with a wide array of hardware and software tools that require a codebase for human-computer-interaction. This often necessitates developers to be involved to establish connection between users/researchers and the complex instrumentation. The advent of generative AI presents an opportunity to bridge this knowledge gap, enabling seamless communication and efficient experimental workflows. Here we present a modular architecture for the Virtual Scientific Companion by assembling multiple AI-enabled cognitive blocks that each scaffolds large language models (LLMs) for a specialized task. With VISION, we performed LLM-based operation on the beamline workstation with low latency and demonstrated the first voice-controlled experiment at an x-ray scattering beamline. The modular and scalable architecture allows for easy adaptation to new instruments and capabilities. Development on natural language-based scientific experimentation is a building block for an impending future where a science exocortex—a synthetic extension to the cognition of scientists—may radically transform scientific practice and discovery.

36 MATERIALS SCIENCE↗

Validation of emission-line galaxies target selection algorithms for the Dark Energy Spectroscopic Instrument using the MMT Binospec

ABSTRACT The forthcoming Dark Energy Spectroscopic Instrument (DESI) experiment plans to measure the effects of dark energy on the expansion of the Universe and create a 3D map of the Universe using galaxies up to z ∼ 1.6 and QSOs up to z ∼ 3.5. In order to create this map, DESI will obtain spectroscopic redshifts of over 30 million objects; among them, a majority are [O ii] emitting star-forming galaxies known as emission-line galaxies (ELGs). These ELG targets will be pre-selected by drawing a selection region on the g − r versus r − z colour–colour plot, where high-redshift ELGs form a separate locus from the lower redshift ELGs and interlopers. In this paper, we study the efficiency of three ELG target selection algorithms – the Final Design Report (FDR) cut based on the DEEP2 photometry, Number Density Modelling (NDM) and Random Forest – to determine how the combination of these three algorithms can be best used to yield a simple selection boundary that will be best suited to meet DESI’s science goals. To do this, we selected 17 small patches in the DESI footprint where we run the three target selection algorithms to pre-select ELGs based on their photometry. We observed the pre-selected ELGs using the MMT Binospec, which is similar in functionality to the DESI instrument, to obtain their spectroscopic redshifts and fluxes of 1054 ELGs. By analysing the redshift and fluxing distribution of these galaxies, we find that although NDM performed the best, simple changes in the FDR definition would also yield sufficient performance.

79 ASTRONOMY AND ASTROPHYSICS↗

Hooks versus Pedicle Screws at the Upper Instrumented Level: An In Vitro Biomechanical Comparison

Study Design. Controlled laboratory study Objective. To compare motions at the upper instrumented vertebra (UIV) and supra-adjacent level (UIV+1) between two fixation techniques in thoracic posterior spinal fusion (PSF) constructs. We hypothesized there would be greater motion at UIV+1 after cyclic loading across all constructs and bilateral pedicle screws (BPS) with posterior ligamentous compromise would demonstrate the greatest UIV+1 range of motion (ROM). Summary of Background Data. Proximal junctional kyphosis (PJK) is a well-recognized complication following long thoraco-lumbar PSF, however its mechanism is poorly understood. Methods. Twenty-seven thoracic functional spine units (FSU) were randomly divided into three UIV fixation groups (n=9): (1) BPS, (2) bilateral transverse process hooks (TPH), and (3) BPS with compromise of the posterior elements between UIV and UIV+1 (BPS-C). Specimens were tested on a servohydraulic materials testing system in native state, following instrumentation, and after cyclic loading. FSUs were loaded in flexion-extension (FE), lateral bending (LB), and axial rotation (AR). Results. After cyclic testing, the TPH group had a mean 29.4% increase in FE ROM at UIV+1 versus 76.6% in the BPS group ( P <0.05). The BPS-C group showed an increased FE of 49.9% and 62.19% with sectioning of the facet joints and interspinous ligament respectively prior to cyclic testing. Conclusion. Bilateral pedicle screws at the UIV led to greater motion at UIV+1 compared to bilateral TPH after cyclic loading. This is likely due to the increased rigidity of BPS compared to TPH leading to a “softer” transition between the TPH construct and native anatomy at the supra-adjacent level. Facet capsule compromise led to a 49.9% increase in UIV+1 motion, underscoring the importance of preserving the posterior ligamentous complex. Clinical studies that account for fusion rates are warranted to determine if constructs with a “soft transition” result in less PJK in vivo.

Neurosciences & Neurology↗

An iterative CMB lensing estimator minimizing instrumental noise bias

Noise maps from cosmic microwave background (CMB) experiments are generally statistically anisotropic, due to scanning strategies, atmospheric conditions, or instrumental effects. Any mismodeling of this complex noise can bias the reconstruction of the lensing potential and the measurement of the lensing power spectrum from the observed CMB maps. We introduce a new CMB lensing estimator based on the maximum (MAP) reconstruction that is minimally sensitive to these instrumental noise biases. By modifying the likelihood to rely exclusively on correlations between CMB map splits with independent noise realizations, we minimize autocorrelations that contribute to biases. In the regime of many independent splits, this maximum closely approximates the optimal MAP reconstruction of the lensing potential. In simulations, we demonstrate that this method is able to determine lensing observables that are immune to any noise mismodeling with a negligible cost in signal-to-noise ratio. Our estimator enables unbiased and nearly optimal lensing reconstruction for next-generation CMB surveys.

Legrand, Louis [University of Cambridge (United Ki↗

The 40m General Purpose Small-Angle Neutron Scattering Instrument at Oak Ridge National Laboratory

A high-flux, 40m long small-angle neutron scattering (SANS) instrument has been constructed at Oak Ridge National Laboratory (ORNL). The facility utilizes a mechanical velocity selector, pinhole collimation and a high count-rate (> 105 Hz), large-area (1m2) two-dimensional position-sensitive detector. The incident wavelength (λ), resolution (Δλ/λ), incident collimation and sample-detector distance are independently variable under computer control. The detector can translate 45cm off axis to increase the overall Q-range (< 0.001 < Q = 4πλ-1sin θ < 1 Å-1), where 2θ is the angle of scatter. The design and characteristics of this instrument are described along with examples of scattering data to illustrate the performance.

biology↗

The Soft X-ray research instrument at the Linac Coherent Light Source

The Soft X-ray Research instrument provides intense ultrashort X-ray pulses in the energy range 280–2000 eV. A diverse set of experimental stations may be installed to investigate a broad range of scientific topics such as ultrafast chemistry, highly correlated materials, magnetism, surface science, and matter under extreme conditions. A brief description of the main instrument components will be given, followed by some selected scientific highlights.

43 PARTICLE ACCELERATORS↗

The matter in extreme conditions instrument at the Linac Coherent Light Source

The LCLS beam provides revolutionary capabilities for studying the transient behavior of matter in extreme conditions. The particular strength of the Matter in Extreme Conditions instrument is that it combines the unique LCLS beam with high-power optical laser beams, and a suite of dedicated diagnostics tailored for this field of science. In this paper an overview of the beamline, the capabilities of the instrumentation, and selected highlights of experiments and commissioning results are presented.

43 PARTICLE ACCELERATORS↗

The X-ray Pump–Probe instrument at the Linac Coherent Light Source

The X-ray Pump–Probe instrument achieves femtosecond time-resolution with hard X-ray methods using a free-electron laser source. It covers a photon energy range of 4–24 keV. A femtosecond optical laser system is available across a broad spectrum of wavelengths for generating transient states of matter. The instrument is designed to emphasize versatility and the scientific goals encompass ultrafast physical, chemical and biological processes involved in the transformation of matter and transfer of energy at the atomic scale.

43 PARTICLE ACCELERATORS↗

Beamline K11 DIAD: a new instrument for dual imaging and diffraction at Diamond Light Source

The Dual Imaging and Diffraction (DIAD) beamline at Diamond Light Source is a new dual-beam instrument for full-field imaging/tomography and powder diffraction. This instrument provides the user community with the capability to dynamically image 2D and 3D complex structures and perform phase identification and/or strain mapping using micro-diffraction. The aim is to enable in situ and in operando experiments that require spatially correlated results from both techniques, by providing measurements from the same specimen location quasi-simultaneously. Using an unusual optical layout, DIAD has two independent beams originating from one source that operate in the medium energy range (7–38 keV) and are combined at one sample position. Here, either radiography or tomography can be performed using monochromatic or pink beam, with a 1.4 mm × 1.2 mm field of view and a feature resolution of 1.2 µm. Micro-diffraction is possible with a variable beam size between 13 µm × 4 µm and 50 µm × 50 µm. One key functionality of the beamline is image-guided diffraction, a setup in which the micro-diffraction beam can be scanned over the complete area of the imaging field-of-view. This moving beam setup enables the collection of location-specific information about the phase composition and/or strains at any given position within the image/tomography field of view. The dual beam design allows fast switching between imaging and diffraction mode without the need of complicated and time-consuming mode switches. Real-time selection of areas of interest for diffraction measurements as well as the simultaneous collection of both imaging and diffraction data of (irreversible) in situ and in operando experiments are possible.

36 MATERIALS SCIENCE↗

The time-resolved atomic, molecular and optical science instrument at the Linac Coherent Light Source

The newly constructed time-resolved atomic, molecular and optical science instrument (TMO) is configured to take full advantage of both linear accelerators at SLAC National Accelerator Laboratory, the copper accelerator operating at a repetition rate of 120 Hz providing high per-pulse energy as well as the superconducting accelerator operating at a repetition rate of about 1 MHz providing high average intensity. Both accelerators power a soft X-ray free-electron laser with the new variable-gap undulator section. With this flexible light source, TMO supports many experimental techniques not previously available at LCLS and will have two X-ray beam focus spots in line. Thereby, TMO supports atomic, molecular and optical, strong-field and nonlinear science and will also host a designated new dynamic reaction microscope with a sub-micrometer X-ray focus spot. The flexible instrument design is optimized for studying ultrafast electronic and molecular phenomena and can take full advantage of the sub-femtosecond soft X-ray pulse generation program.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗

Hands-On Computer Science: The Array of Things Experimental Urban Instrument

Chicago's Array of Things (AoT) project is aptly described as a technology experiment or a "smart city" prototype. The concept of such an extensible "instrument" arose within a larger translational research vision applying computer science and engineering research for the multidimensional benefit of people and communities in cities. The AoT project hypothesized that wireless intelligent sensor networks could enable both quantitative social science and urban monitoring while also stimulating youth interest in science and technology. Successful deployment of such sensor networks could provide open data from urban measurements not only in support of diverse research questions-in environmental dynamics, urban architecture, engineering, and social sciences-but also informing community groups and city planners. Further, the AoT project and its successor SAGE project are a computer science and engineering experiment, but its success is inextricably tied to community engagement and experiential education. Simply put, community acceptance is a prerequisite to installing and testing the instrument.

97 MATHEMATICS AND COMPUTING↗

Instrumentation to Monitor Transient Periodic Developing Flow in Non-Newtonian Slurries

Staff at Pacific Northwest National Laboratory have conducted mixing and mobilization experiments with non-Newtonian slurries that exhibit Bingham plastic and shear thinning behavior and shear strength. This paper describes measurement techniques applied to identify the interface between flowing and stationary regions of non-Newtonian slurries that are subjected to transient, periodic, developing flows. Techniques were developed to identify the boundary between the flowing and stationary regions, time to mix, characteristic velocities of the flow field produced by the symmetrically spaced nozzles, and the velocity of the upwell formed in the center of the tank by the intersection of flow from four symmetrically spaced nozzles that impinge upon the tank floor. Descriptions of the instruments and instrument performance are presented. These techniques were an effective approach to characterize mixing phenomena, determine mixing energy required to fully mobilize vessel contents and to determine mixing times for process evaluation.

Non-Newtonian Slurries↗