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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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All sourcesNASA NTRSDOE OSTI
DOE OSTI2015

Prognostics Health Management Model for LED Package Failure Under Contaminated Environment

The reliability consideration of LED products includes both luminous flux drop and color shift. Previous research either talks about luminous maintenance or color shift, because luminous flux degradation usually takes very long time to observe. In this paper, the impact of a VOC (volatile organic compound) contaminated luminous flux and color stability are examined. As a result, both luminous degradation and color shift had been recorded in a short time. Test samples are white, phosphor-converted, high-power LED packages. Absolute radiant flux is measured with integrating sphere system to calculate the luminous flux. Luminous flux degradation and color shift distance were plotted versus aging time to show the degradation pattern. A prognostic health management (PHM) method based on the state variables and state estimator have been proposed in this paper. In this PHM framework, unscented kalman filter (UKF) was deployed as the carrier of all states. During the estimation process, third order dynamic transfer function was used to implement the PHM framework. Both of the luminous flux and color shift distance have been used as the state variable with the same PHM framework to exam the robustness of the method. Predicted remaining useful life is calculated at every measurement point to compare with the tested remaining useful life. The result shows that state estimator can be used as the method for the PHM of LED degradation with respect to both luminous flux and color shift distance. The prediction of remaining useful life of LED package, made by the states estimator and data driven approach, falls in the acceptable error-bounds (20%) after a short training of the estimator.

Lall, Pradeep↗
DOE OSTI2012

A NEW INFRARED COLOR CRITERION FOR THE SELECTION OF 0 < z < 7 AGNs: APPLICATION TO DEEP FIELDS AND IMPLICATIONS FOR JWST SURVEYS

It is widely accepted that observations at mid-infrared (mid-IR) wavelengths enable the selection of galaxies with nuclear activity, which may not be revealed even in the deepest X-ray surveys. Many mid-IR color-color criteria have been explored to accomplish this goal and tested thoroughly in the literature. Besides missing many low-luminosity active galactic nuclei (AGNs), one of the main conclusions is that, with increasing redshift, the contamination by non-active galaxies becomes significant (especially at z {approx}> 2.5). This is problematic for the study of the AGN phenomenon in the early universe, the main goal of many of the current and future deep extragalactic surveys. In this work new near- and mid-IR color diagnostics are explored, aiming for improved efficiency-better completeness and less contamination-in selecting AGNs out to very high redshifts. We restrict our study to the James Webb Space Telescope wavelength range (0.6-27 {mu}m). The criteria are created based on the predictions by state-of-the-art galaxy and AGN templates covering a wide variety of galaxy properties, and tested against control samples with deep multi-wavelength coverage (ranging from the X-rays to radio frequencies). We show that the colors K{sub s} - [4.5], [4.5] - [8.0], and [8.0] - [24] are ideal as AGN/non-AGN diagnostics at, respectively, z {approx}< 1, 1 {approx}< z {approx}< 2.5, and z {approx}> 2.5-3. However, when the source redshift is unknown, these colors should be combined. We thus develop an improved IR criterion (using K{sub s} and IRAC bands, KI) as a new alternative at z {approx}< 2.5. KI does not show improved completeness (50%-60% overall) in comparison to commonly used Infrared Array Camera (IRAC) based AGN criteria, but is less affected by non-AGN contamination (revealing a >50%-90% level of successful AGN selection). We also propose KIM (using K{sub s} , IRAC, and MIPS 24 {mu}m bands, KIM), which aims to select AGN hosts from local distances to as far back as the end of reionization (0 < z {approx}< 7) with reduced non-AGN contamination. However, the necessary testing constraints and the small control-sample sizes prevent the confirmation of its improved efficiency at z {approx}> 2.5. Overall, KIM shows a {approx}30%-40% completeness and a >70%-90% level of successful AGN selection. KI and KIM are built to be reliable against a {approx}10%-20% error in flux, are based on existing filters, and are suitable for immediate use.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2017

Scaling Up Data-Parallel Analytics Platforms: Linear Algebraic Operation Cases

Linear algebraic operations such as matrix manipulations form the kernel of many machine learning and other crucial algorithms. Scaling up as well as scaling out such algorithms are key to supporting large scale data analysis that require efficient processing over millions of data samples. To this end, we present, ARION, a hardware acceleration based approach for scaling-up individual tasks of Spark, a popular data-parallel analytics platform. We support both linear algebraic operations of between two dense matrices, and between sparse and dense matrices in distributed environments. ARION provides a flexible control of acceleration according to matrix density, along with efficient scheduling based on runtime resource utilization. We demonstrate the benefit of our approach for general matrix multiplication operations over large matrices with up to four billion elements by using Gramian matrix computation that is commonly used in machine learning. Experiments show that our approach achieves more than 2× and 1.5× end-to-end performance speedups for dense and sparse matrices, respectively, and up to 57.04× faster computation compared to MLlib, a state of the art Spark-based implementation. This work is sponsored in part by the NSF under the grants: CNS-1565314, CNS-1405697, and CNS-1615411. The manuscript has been authored by UT-Battelle, LLC under Contract No. DE-AC05-00OR22725 with the U.S. Department of Energy. The United States Government retains and the publisher, by accepting the article for publication, acknowledges that the United States Government retains a non-exclusive, paid-up, irrevocable, world-wide license to publish or reproduce the published form of this manuscript, or allow others to do so, for United States Government purposes. The Department of Energy will provide public access to these results of federally sponsored research in accordance with the DOE Public Access Plan (http://energy.gov/downloads/doe-public-access-plan). This research used resources of the Oak Ridge Leadership Computing Facility at the Oak Ridge National Laboratory, which is supported by the Office of Science of the U.S. Department of Energy under Contract No. DE-AC05-00OR22725.

Xu, Luna↗
DOE OSTI2017

Stellar clusterings around 'isolated' Massive YSOs in the LMC

Observations suggest that there is a significant fraction of O stars in the field of the Milky Way that appear to have formed in isolation or in low-mass clusters (<100 M{sub ⊙}). The existence of these high-mass stars that apparently formed in the field challenges the generally accepted paradigm, which requires star formation to occur in clustered environments. In order to understand the physical conditions for the formation of these stars, it is necessary to observe isolated high-mass stars while they are still forming. With the Hubble Space Telescope, we observe the seven most isolated massive (>8 M{sub ⊙}) young stellar objects (MYSOs) in the Large Magellanic Cloud. The observations show that while these MYSOs are remote from other MYSOs, OB associations, and even known giant molecular clouds, they are actually not isolated at all. Imaging reveals ∼100 to several hundred pre-main-sequence (PMS) stars in the vicinity of each MYSO. These previously undetected PMS stars form prominent compact clusters around the MYSOs, and in most cases they are also distributed sparsely across the observed regions. Contrary to what previous high-mass field star studies show, these observations suggest that high-mass stars may not be able to form in clusters with masses less than 100 M{sub ⊙}. If these MYSOs are indeed the best candidates for isolated high-mass star formation, then the lack of isolation is at odds with random sampling of the initial mass function. Moreover, while isolated MYSOs may not exist, we find evidence that isolated clusters containing O stars can exist, which in itself is rare.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2020

Test for Reconditioning RA Waste with Simulated Bitumen and Concrete in a 1,2 MW Plasma Test Facility - 20092

The operation and maintenance of nuclear power plants, the non nuclear fuel cycle, etc generate low-level radioactive waste which, along with the historical radioactive waste from past nuclear activities, needs to be treated and stored, awaiting final disposal. Plasma technology offers a very effective way of treating this waste with a high volume reduction factor (VRF), free from organics, liquids and moisture, and meets without a doubt the acceptance criteria for safe storage and disposal. By means of a plasma beam of approximately 5000 deg. C, the inorganic materials are melted into a glassy slag, containing most of the radioactive isotopes while the organic material is gasified, oxidized and purified in an off-gas cleaning system. First the paper describes the new full-scale Plasma Melting Facility (PMF) at the Kozloduy Nuclear Power Plant in Bulgaria which was taken in nuclear operation In May 2018. The plant has a capacity of 250 tons per year and the maximum contact dose rates of the incoming waste is 2 mSv/h. Different mixtures of radioactive waste packed in 200 l drums were successfully treated resulting in a glassy slag free from liquids and organic material with an important volume reduction factor (VRF). The Project was co-financed through a grant by Kozloduy International Decommissioning fund (KIDSF) administrated by the EBRD through Bulgarian national funding. Plasma is a suitable technology for treatment of problematic waste or even reconditioning waste so Belgoprocess was contracted to do plasma tests with simulated conditioned waste types. One can do tests on a laboratory scale on smaller samples and torch capacities of e.g. 50 kW but Belgoprocess wanted to do more realistic and reliable tests. So Belgoprocess contracted Phoenix Solutions Co who has a full-scope test facility equipped with a 1200 kW plasma torch for full-scope treatment of simulated conditioned waste. For a first confidential contract simulated 200 l (55 gallon) bitumen drums were treated. The drums contained different pucks of compacted waste such as rags, used filters, granulates, etc. The pucks were stacked in the 200 l drums and subsequently embedded with bitumen. A total of 6 drums were treated in the plasma facility. For a second contract simulated homogeneous 200 l (55 gallon) concrete drums with on the one hand concentrates and on the other hand spent resins were selected. A total of 6 drums with concrete and spent resins were treated and melted in the plasma testing facility. The paper describe the test facility, volume reduction factor (VRF) of different waste streams and most important parameters. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2024

Binary pseudo-random array standards for calibration of 3D optical surface profilers used for metrology with significantly curved x-ray optics

High-accuracy metrology is vitally important in manufacturing ultra-high-quality free-form mirrors designed to manipulate X-ray light with nanometer-scale wavelengths. The current capabilities and possibility for improvements in X-ray mirror manufacturing are limited by inherent imperfections of the integrated metrology tools. In the case of Fizeau interferometry, metrology tools are currently calibrated with super-polished flat test-standard/reference mirrors. This is acceptable for measuring slightly curved X-ray optics. However, for even moderately curved aspherical X-ray mirrors the flat-reference calibration is not sufficiently accurate and stitching Fizeau interferometer-based surface metrology is used to mitigate the problem. But still, the retrace and aberration errors, as well as the limited spatial resolution, described with the instrument transfer function (ITF), can be transferred into the optical surface topography of X-ray mirrors obtained in stitching metrology. For ITF calibration, we have developed an original technique, based on test standards structured as two-dimensional (2D) highly-randomized (HR) binary pseudo-random arrays (BPRAs). The technique employs the unique properties of the HR BPRA patterns in the spatial frequency domain., i.e. the inherent 2D power spectral density of the HR BPRA pattern has a deterministic white-noise-like character that allows direct determination of the ITF with uniform sensitivity over the entire spatial frequency range and field-of-view of an instrument. Here, we explore technological, metrological, and analytical aspects essential for calibration of the retrace and aberration errors of Fizeau interferometers using different types of tilted test samples, including a super-polished reference mirror for the re-trace calibration and the uniformly redundant array (URA) BPRA standards for the geometrical distortion (aberration) calibration. While the first method was previously demonstrated by researchers at DIAMOND Light Source, a method based on the URA BPRA is described and demonstrated here for the first time. We outline the design and fabrication process used in fabrication of URA BPRA test standards, and present the results of application of the URA BPRA standards demonstrating the high efficacy of our approach to geometrical distortion calibration of Fizeau interferometers. We also discuss the possible sources of unexpected peculiarities of the systematic errors, including an astigmatic character of the retrace error, observed with Fizeau interferometers at the Advanced Light Source X-Ray Optics Laboratory.

Munechika, Keiko↗
NASA NTRS2020

Novel High Barrier Films for Packaging Food and Medicine

Long manned missions require food packaging to maintain food safety, nutrition, and acceptability for the length of 3-5 years1,2 while the shelf life assigned by NASA for current provisions is 18-24 months1. The focus of this design project was to make a polymer film specifically to function as a high oxygen barrier to later be included in an improved multi-layer packaging system of other specialized polymers with capabilities to allow for a 5-year shelf-life. To qualify as a high oxygen barrier film and to be a successful design for the future packaging, the resulting film is required to have an oxygen transmission rate (OTR) less than 0.06 cc/ m2/24 hr/atm, the standard for the current packaging3. This new film was designed to have a decreased permeability by increasing the “tortuous path” a gas molecule travels to permeate through a film. The increase in the “tortuous path” of a gas molecule is accomplished by introducing a 2D material additive. The additive chosen for this project was hexagonal boron nitride (h-BN) which exfoliates into boron nitride nanosheets (BNNs). Nylon 6 was chosen as the candidate for the matrix. This project is required to determine the best methods to synthesize the sample film and then to test the OTR of the film to determine if this design was successful. This project examined methods for pulverizing polymer resin pellets, h-BN exfoliation, and film fabrication using a hot press. This report includes the exfoliation and analysis of h-BN, procedural preparations for films, and a modeling study of estimated OTR of the h-BN/Nylon. The work in this report did not yield a high barrier composite film because of the laboratory closure in response to COVID -19 guidance but provides a concise method of the additive preparation and film synthesis. This gives a good starting point for future research in high barrier films by 2D additive composites.

Polymer, Nylon, PET, boron nitride, nanocomposite↗
NASA NTRS2018

Flight Plasma Diagnostics for High-Power, Solar-Electric Deep-Space Spacecraft

NASA’s Asteroid Redirect Robotic Mission (ARRM) mission concept plans included a set of plasma and space environment instruments, the Plasma Diagnostic Package (PDP), to fulfill ARRM requirements for technology extensibility to future missions. The PDP objectives were divided into the classes of 1) Plasma thruster dynamics, 2) Solar array-specific environmental effects, 3) Plasma environmental spacecraft effects, and 4) Energetic particle spacecraft environment. A reference design approach and interface requirements for ARRM’s PDP was generated by the PDP team at JPL and GRC. The reference design consisted of redundant single-string avionics located on the ARRM spacecraft bus as well as solar array, driving and processing signals from multiple copies of several types of plasma, effects, and environments sensors distributed over the spacecraft and array. The reference design sensor types were derived in part from sensors previously developed for USAF Research Laboratory (AFRL) plasma effects campaigns such as those aboard TacSat-2 in 2007 and AEHF-2 in 2012. ARRM project leadership also encouraged the PDP team to convene a team of topical subject matter experts from across the country to review and confirm the reference design and to consider effective alternatives and/or enhancements to the reference design. This activity was proposed and accepted as an interactive, informal JPL “A-team” study and a cadre of 25 participants gathered in early 2017 for discussions. The outcome of the two-day A-team study was that the PDP reference design would allow the most important induced-environment unknowns to be measured in the appropriate space environment. Another outcome addressed technology developments of new or improved space plasma environmental sensors. The A-team study concluded that selected developments would lead to improved measurements that could efficiently provide important and otherwise unavailable information about plasma thruster operation in the space environment as well as the plasma induced spacecraft environment. Specifically, the A-team group recommended greater sensor diversity, by inclusion of deployed sensor capabilities in the thruster plume, or by occasional gimbaling of the thruster(s) toward the sensor arrays. The A-team also recommended developing high-speed probes, optical plasma probes, energy selective probes, and direct erosion/deposition sensors, among others; and recommended the inclusion of cameras as well as, since ARRM was to be recovered in cis-lunar orbit by a crewed mission, astronaut assessments of thruster induced environments and collection of sample coupons. Overall, the PDP A-team study provided a clear, consensus supported validation of the reference design PDP approach and pointed out important directions for future flight plasma sensor development.

Choi, Maria↗
NASA NTRS2002

Evaluation of SAGE II and Balloon-Borne Stratospheric Aerosol Measurements

Under funding from this proposal we evaluated measurements of stratospheric sulfate aerosols from three platforms. Two were satellite platforms providing solar extinction measurements, the Stratospheric Aerosol and Gas Experiment (SAGE) II using wavelengths from 0.386 - 1.02 microns, and the Halogen Occultation Experiment (HALOE) using wavelengths from 2.45 to 5.26 microns. The third set of measurements was from in situ sampling by balloonborne optical particle counters (OPCs). The goal was to determine the consistency among these data sets. This was accomplished through analysis of the existing measurement records, and through additional balloonborne OPC flights coinciding with new SAGE II observations over Laramie, Wyoming. All analyses used the SAGE II v 6.0 data. This project supported two balloon flights per year over Laramie dedicated to SAGE II coincidence. Because logistical factors, such as poor surface weather or unfavorable payload impact location, can make it difficult to routinely obtain close coincidences with SAGE II, we attempt to conduct nearly every Laramie flight (roughly one per month) in conjunction with a SAGE II overpass. The Laramie flight frequency has varied over the years depending on field commitments and funding sources. Current support for the Laramie measurements is from the National Science Foundation in addition to support from this NASA grant. We have also completed a variety of comparisons using aerosol measurements from SAGE II, OPCs, and HALOE. The instruments were compared for their various estimates of aerosol extinction at the SAGE II wavelengths and for aerosol surface area. Additional results, such as illustrated here, can be found in a recently accepted manuscript describing comparisons between SAGE II, HALOE, and OPCs for the period 1982 - 2000. While overall, the impression from these results is encouraging, the agreement of the measurements changes with latitude, altitude, time, and parameter. In the broadest sense, these comparisons fall into two categories: high aerosol loading (volcanic periods) and low aerosol loading (background periods and altitudes above 25 km). When the aerosol amount is low SAGE II and HALOE extinctions are higher than the OPC estimates, while the SAGE II surface areas are lower than HALOE and the OPCS. Under high loading conditions, all three instruments mutually agree to within 50%.

Source record↗
DOE OSTI2013

BROAD ABSORPTION LINE VARIABILITY ON MULTI-YEAR TIMESCALES IN A LARGE QUASAR SAMPLE

We present a detailed investigation of the variability of 428 C IV and 235 Si IV broad absorption line (BAL) troughs identified in multi-epoch observations of 291 quasars by the Sloan Digital Sky Survey-I/II/III. These observations primarily sample rest-frame timescales of 1-3.7 yr over which significant rearrangement of the BAL wind is expected. We derive a number of observational results on, e.g., the frequency of BAL variability, the velocity range over which BAL variability occurs, the primary observed form of BAL-trough variability, the dependence of BAL variability upon timescale, the frequency of BAL strengthening versus weakening, correlations between BAL variability and BAL-trough profiles, relations between C IV and Si IV BAL variability, coordinated multi-trough variability, and BAL variations as a function of quasar properties. We assess implications of these observational results for quasar winds. Our results support models where most BAL absorption is formed within an order-of-magnitude of the wind-launching radius, although a significant minority of BAL troughs may arise on larger scales. We estimate an average lifetime for a BAL trough along our line-of-sight of a few thousand years. BAL disappearance and emergence events appear to be extremes of general BAL variability, rather than being qualitatively distinct phenomena. We derive the parameters of a random-walk model for BAL EW variability, finding that this model can acceptably describe some key aspects of EW variability. The coordinated trough variability of BAL quasars with multiple troughs suggests that changes in 'shielding gas' may play a significant role in driving general BAL variability.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2011

Corrective Action Decision Document/Closure Report for Corrective Action Unit 367: Area 10 Sedan, Ess and Uncle Unit Craters Nevada National Security Site, Nevada, Revision 0 with ROTC 1

Corrective Action Unit 367 comprises four corrective action sites (CASs): • 10-09-03, Mud Pit • 10-45-01, U-10h Crater (Sedan) • 10-45-02, Ess Crater Site • 10-45-03, Uncle Crater Site The purpose of this Corrective Action Decision Document/Closure Report is to provide justification and documentation of the corrective actions and site closure activities implemented at CAU 367. A corrective action of closure in place with use restrictions was completed at each of the three crater CASs (10-45-01, 10-45-02, and 10-45-03); corrective actions were not required at CAS 10-09-03. In addition, a limited soil removal corrective action was conducted at the location of a potential source material release. Based on completion of these correction actions, no additional corrective action is required at CAU 367, and site closure is considered complete. Corrective action investigation (CAI) activities were performed from February 2010 through March 2011, as set forth in the Corrective Action Investigation Plan for Corrective Action Unit 367: Area 10 Sedan, Ess and Uncle Unit Craters, Nevada Test Site, Nevada. The approach for the CAI was divided into two facets: investigation of the primary release of radionuclides, and investigation of non-test or other releases (e.g., migration in washes and potential source material). Based on the proximity of the Uncle, Ess, and Sedan craters, the impact of the Sedan test on the fallout deposited from the two earlier tests, and aerial radiological surveys, the CAU 367 investigation was designed to study the releases from the three crater CASs as one combined release (primary release). Corrective Action Site 10-09-03, Mud Pit, consists of two mud pits identified at CAU 367. The mud pits are considered non-test releases or other releases and were investigated independent of the three crater CASs. The purpose of the CAI was to fulfill data needs as defined during the data quality objective (DQO) process. The CAU 367 dataset of investigation results was evaluated based on a data quality assessment. This assessment demonstrated the dataset is complete and acceptable for use in fulfilling the DQO data needs. Analytes detected during the CAI were evaluated against final action levels (FALs) established in this document. For the primary release, radiological doses exceeding the FAL of 25 millirem per year were not found to be present in the surface or shallow subsurface soil outside the default contamination boundary. However, it was assumed that radionuclides are present in subsurface media within each of the three craters (Sedan, Ess, and Uncle) due to prompt injection of radionuclides from the tests. Based on the assumption of radiological dose exceeding the FAL, corrective actions were undertaken that consisted of implementing a use restriction and posting warning signs at each crater CAS. These use restrictions were recorded in the FFACO database; the U.S. Department of Energy, National Nuclear Security Administration Nevada Site Office (NNSA/NSO) Facility Information Management System; and the NNSA/NSO CAU/CAS files. With regard to other releases, no contaminants of concern were identified at the mud pits or any of the other release locations, with one exception. Potential source material in the form of lead was found at one location. A corrective action of clean closure was implemented at this location, and verification samples indicated that no further action is necessary. Therefore, NNSA/NSO provides the following recommendations: • A Notice of Completion to NNSA/NSO is requested from the Nevada Division of Environmental Protection for closure of CAU 367. • Corrective Action Unit 367 should be promoted from Appendix III to Appendix IV of the FFACO.

54 ENVIRONMENTAL SCIENCES↗
NASA NTRSDate not supplied

Zircon (U-Th)/He Impact Crater Thermochronometry and the Effects of Shock Microstructures on Helium Diffusion Kinetics

Absolute age determination of impact cratering events remains difficult and often controversial; a challenge that has resulted in < 50% of known impact craters regarded as accurately and precisely dated. Besides conventional 40Ar/39Ar and U-Pb methods, zircon (U-Th)/He (ZHe) dating of impactites has been applied to large- to medium-sized impact structures. ZHe dates can be fully reset in minutes at 1000°C, which is commonly reached in central sections of the melt sheet, whereas resetting of ZHe at <300°C, which might be encountered near the crater margins or persist in post-impact hydrothermal systems, may take >103-6 years. There is a critical need to quantify the effects of shock-induced microstructures and impact metamorphism on helium diffusion kinetics in well-characterized, variably shocked zircon to further establish the reliability of (U-Th)/He for dating impacts. For this purpose, we investigated suevite and impact melt samples from two impact structures, the Chicxulub multi-ring basin and the Ries complex crater, which enables us to compare zircon helium diffusion kinetics from impact structures with differing sizes, ages, and hydrothermal system longevities. Shock microstructures were characterized by backscattered-electron (BSE) imaging prior to diffusion step-heating fractional release experiments using light-bulb furnace with prograde and retrograde incremental 10°C steps from 250°C to 600°C. Afterward, we characterize the diffusion domain sizes and their interconnectivity within the shocked zircon grains using electron backscatter diffraction (EBSD). We find that zircon with few shock microstructures exhibit no significant deviation from helium diffusion kinetics of undamaged zircon. In contrast, zircon grains with planar deformation features (PDFs) and granular textures classified by BSE and EBSD are characterized by a dramatic decrease in helium retentivity, similar to radiation damaged grains, due to a reduction in the effective domain size and the introduction of interconnected fast diffusion pathways created by shock microstructures. A subset of grains were dated by ZHe after the external morphology of the grains was determined by BSE imaging. The euhedral grains yielded a weighted mean age within the uncertainty of the accepted impact ages, whereas the grains with PDFs or granular textures exhibited younger ages. Thus, these diffusion experiments and ZHe dates suggest that the dramatic decrease in domain size likely renders shocked grains more susceptible to impact-induced hydrothermal resetting and subsequent overprinting. Hence, characterization of shock microstructures is critical for determining accurate impact ages using ZHe methods especially when applied to previously unconstrained craters. The thermochronometer also offers the opportunity to determine the magnitude and duration of post-impact hydrothermal circulation.

zircon↗
DOE OSTI2023

HFTS-1 (Final Report)

Despite the long history of hydraulic fracturing, the optimal number of fracturing stages during multi-stage fracture stimulation in horizontal wells can be a complex subject. In addition to the increased expense of multistage fracturing in horizontal wells, increasing the number of fracturing stages does not always correlate with a commensurate increase in production. The problem is the application of a uniform fracture stimulation design to all stages with no consideration for geological variations along the wellbore. The result is an inefficient use and costly waste of energy and water. Optimization of the fracturing process requires an understanding of the cause-and-effect relationship between fracturing parameters and local geological properties at a given location along the wellbore. Realizing that the generalized rock mechanics theories and hypotheses are not truly applicable to fractured and laminated shales, quantifiable impacts of a shale’s geomechanical and depositional features are a prerequisite for design and implementation of optimized hydraulic fractures. The overarching goal of this project is to understand and define the relationships of shale geology and fracture dynamics using detailed field data that includes coring of the fracture domain. Finally, resource recovery from shale formations is estimated to be less than fifteen percent. Research proposed in this project will establish the foundations for investigating enhanced recovery techniques for increased resource recovery in existing fracture treated wells. Natural gas as an EOR fluid is in the initial stages of being used broadly in the oil and gas industry and as such, many aspects of the process need to be researched and addressed prior to widespread acceptance. In addition, re-fracturing techniques, particularly using cemented liners also need to be further investigated. This project explores several of these EOR techniques in greater detail, not just at the theoretical level, but through actual field test sites. This report delves into the research program, identified tasks, several studies, observations, results, and conclusions under the Hydraulic Fracturing Test Site (HFTS) project. This test project is subdivided into three distinct phases and each phase is discussed in detail under separate sections. The original test site for Phase 1 as well as the Phase 2 site are in Midland Basin in Texas and operated by Laredo Petroleum. In the first two phases, the program targeted the Wolfcamp formation in Midland Basin. Phase 3 of the study targeted the EagleFord play in South Texas with Devon Energy as the operator. Significant conclusions from this study include: 1) lateral and vertical fracture growth mapping as well as proppant transport behavior, 2) Use of field gas and its applicability for huff n puff EOR injection in the Midland Basin, 3) Development and validation of proppant log, both at core scale as well as in-fill well implementation by analyzing drilling mud return samples, 4) Applicability of liner refracturing including best practices for enhanced unit level productivity. This report will detail all these studies as well as technical results and conclusions from said studies. These include general subsurface characterization work, completion designs as implemented, studies looking at fracture geometry, high resolution microseismic study, advanced crosswell strain mapping studies including drainage characterization, core characterization results, proppant analysis (core and observation wells), geochemistry, etc. to name a few.

02 PETROLEUM↗
NASA NTRS2019

Discovery of Activities via Statistical Clustering of Fixation Patterns

Human behavior often consists of a series of distinct activities, each characterized by a unique signature of visual behavior. This is true even in a restricted domain, such as piloting an aircraft, where patterns of visual signatures might represent activities like communicating, navigating, and monitoring. We propose a novel analysis method for gaze-tracking data, to perform blind discovery of these activities based on their behavioral signatures. The method is in some respects similar to recurrence analysis, but here we compare not individual fixations, but groups of fixations aggregated over a fixed time interval. The duration of this interval is a parameter that we will refer to as τ. We assume that the environment has been divided into a set of N different areas-of-interest (AOIs). For a given interval of time of duration τ, we compute the proportion of time spent fixating each AOI, resulting in an N-dimensional vector. These proportions can be converted to counts by multiplying by τ divided by the average fixation duration (another parameter that we fix at 280 milliseconds). We compare different intervals by computing the chi-square statistic. The p-value associated with the statistic is the likelihood of observing the data under the hypothesis that the data in the two intervals were generated by a single process with a single set of probabilities governing the fixation of each AOI. We have investigated the method using a set of 10 synthetic "activities," that sample 4 AOIs. Four of these activities visit 3 of the 4 AOIs, with equal probability; as there are four different ways to leave-one- out, there are four such activities. Similarly, there are six different activities that leave-two-out. Sequences of simulated behavior were generated by running each activity for 40 seconds, in sequence, for a total of 6.7 minutes. The figure to the right shows the matrix of chi-square statistics, using a value of 2.8 seconds for τ, corresponding to 10 fixations. Low values (dark) indicate poor evidence for activity differences, while high values (bright) indicate strong evidence. The dark squares along the main diagonal each correspond to the forty second intervals in which the activity was held constant; the 4x4 block at the lower left corresponds to the four leave-one-out activities, while the 6x6 block in the upper right corresponds to the leave-two-out activities. (The anti-diagonal pattern of white squares indicates those activity pairs that share no AOIs.) The chi-square values can be binarized by choosing a particular significance level; we are interested in grouping bins that represent the same activity, effectively accepting the null hypothesis. Therefore, we may adopt a relatively lax criterion; for example, choosing a p-value of 0.2 means that two behaviors that have only a 1-in-5 chance of being produced by a single activity might nevertheless be clustered together. We have explored several methods to perform clustering on the data and solving for the activity probabilities. Greedy methods begin by selecting the time bin that is similar to the most (or least) other bins, and then forming a cluster from it and all other non-discriminable bins. These methods show mediocre performance, as they do not take into account temporal contiguity. Preliminary results indicate that methods that "grow" clusters in time from seed points perform better.

activity analysis↗
DOE OSTI2013

Measurement of the Υ ( 1 S ) , Υ ( 2 S ) , and Υ ( 3 S ) cross sections in pp collisions at s = 7 TeV

The $\Upsilon$(1S), $\Upsilon$(2S), and $\Upsilon$(3S) production cross sections are measured using a data sample corresponding to an integrated luminosity of 35.8 $\pm$ 1.4 inverse picobarns of proton-proton collisions at $\sqrt{s}$ = 7 TeV, collected with the CMS detector at the LHC. The Upsilon resonances are identified through their decays to dimuons. Integrated over the $\Upsilon$ transverse momentum range $p_{t}^{\Upsilon} \lt$ 50GeV and rapidity range |$y^\Upsilon$| $\lt$ 2.4, and assuming unpolarized Upsilon production, the products of the Upsilon production cross sections and dimuon branching fractions are \begin{equation*}\sigma(pp \to \Upsilon(1S) X) . B(\Upsilon(1S) \to \mu^+ \mu^-) = (8.55 \pm 0.05^{+0.56}_{-0.50} \pm 0.34) nb,\end{equation*} \begin{equation*}\sigma(pp \to \Upsilon(2S) X) . B(\Upsilon(2S) \to \mu^+ \mu^-) = (2.21 \pm 0.03^{+0.16}_{-0.14} \pm 0.09) nb,\end{equation*} \begin{equation*}\sigma(pp \to \Upsilon(3S) X) . B(\Upsilon(3S) \to \mu^+ \mu^-) = (1.11 \pm 0.02^{+0.10}_{-0.08} \pm 0.04) nb, \end{equation*} where the first uncertainty is statistical, the second is systematic, and the third is from the uncertainty in the integrated luminosity. The differential cross sections in bins of transverse momentum and rapidity, and the cross section ratios are presented. Cross section measurements performed within a restricted muon kinematic range and not corrected for acceptance are also provided. These latter measurements are independent of Upsilon polarization assumptions. The results are compared to theoretical predictions and previous measurements.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
NASA NTRS2000

Leonardo-BRDF: A New Generation Satellite Constellation

Instantaneous net radiation flux at the top of the atmosphere is one of the primary drivers of climate and global change. Since the dawn of the satellite era, great efforts and expense have gone into measuring this flux from single satellites and even (for a several-year period) from a constellation of three satellites called ERBE. However, the reflected solar flux is an angular and spectral integral over the so-called "BRDF" or Bidirectional Reflectance Distribution Function, which is the angular distribution of reflected solar radiation for each solar zenith angle and each wavelength. Previous radiation flux satellites could not measure instantaneous BRDF, so scientists have had to fall back on models or composites. Because their range of observed solar zenith angles was very limited due to sunsynchronous orbits, the resultant flux maps are too inaccurate to see the dynamics of radiation flux or to reliably correlate it with specific phenomena (hurricanes, biomass fires, urban pollution, dust outbreaks, etc.). Accuracy only becomes acceptable after monthly averaging, but this washes out almost all cause-and-effect information, further exacerbated by the lack of spectral resolution. Leonardo-BRDF is a satellite system designed to measure the instantaneous spectral BRDF using a formation of highly coordinated satellites, all pointing at the same Earth targets at the same time. It will allow scientists for the first time to assess the radiative forcing of climate due to specific phenomena, which is bound to be important in the ongoing debate about global warming and what is causing it. The formation is composed of two satellite types having, as instrument payloads, single highly-integrated miniature imaging spectrometers or radiometers. Two nearby "keystone" satellites anchor the formation and fly in static orbits. They employ wide field of view imaging spectrometers that are extremely light and compact. The keystone satellites are identical and can operate in alongtrack or cross-track mode, or anything in between, at ground command. This provides inherent system redundancy and cross-calibration capability. Several "wing-man" satellites in non-static orbits fly in formation up to 1000 km out from the keystone satellites to provide additional along- and cross-track angular sampling. They view the target(s) observed by the keystone satellites from different zenith and azimuth angles and are maneuverable within a limited range of zenith angle using thrusters, and within a large range of azimuth angle using clever orbit design. The wing-man satellites carry single miniature imaging radiometers with just a few wavelength bands in order to be lighter and more agile.

Esper, Jaime↗
DOE OSTI2020

KENO-VI Primer: Performing Calculations using SCALE’s Criticality Safety Analysis Sequence (CSAS6) with Fulcrum

The SCALE code system developed at Oak Ridge National Laboratory is widely used and accepted around the world for criticality safety analysis. The well-known KENO-VI three-dimensional Monte Carlo criticality computer code is one of the primary criticality safety analysis tools in SCALE. The KENO-VI primer is designed to help a new user understand and use the SCALE/KENO-VI Monte Carlo code for nuclear criticality safety analysis. It assumes that the user has a college education in a technical field. There is no assumption of familiarity with Monte Carlo codes in general or with SCALE/KENO-VI in particular. The primer is designed to teach by example, with each example illustrating two or three features of SCALE/KENO-VI that are useful in criticality analysis. The primer is based on SCALE 6.2 and 6.3, which includes the Fulcrum graphical user interface. Each example uses Fulcrum to provide the framework for preparing input data and viewing output results. Starting with a Quickstart section, the primer gives an overview of the basic requirements for SCALE/KENO-VI input and allows the user to quickly run a simple criticality problem with SCALE/KENO-VI. Each following section begins with a list of basic objectives identifying the goal of the section and the individual SCALE/KENO-VI features covered in detail in the section’s sample problems. Upon completion of the primer, a new user should be comfortable using Fulcrum to set up criticality problems in SCALE/KENO-VI. The primer provides a starting point for the criticality safety analyst who uses SCALE/KENO-VI. Complete descriptions are provided in the SCALE/KENO-VI manual. Although the primer is self-contained, it is intended as a companion volume to the SCALE/KENO-VI training and documentation. The SCALE manual and training schedule are available at https://scale.ornl.gov. The primer provides specific examples of using SCALE/KENO-VI for criticality analysis; the SCALE/KENO-VI manual provides information on the use of SCALE/KENO-VI and all its modules. The primer also contains an appendix with sample input files. In addition, this primer, its errata, and sample inputs are also available at https://code.ornl.gov/scale/primers/kenovi/.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗
DOE OSTI2015

Load planning in the dark: RH-TRU waste container load planning at Sandia National Laboratories/New Mexico - 15116

Sandia National Laboratories (Sandia) performed several sets of experiments during the 1970's and 1980's with fresh and irradiated mixed oxide (MOX) and uranium oxide (UO{sub 2}) materials designed to simulate various fuel responses under varying reactor conditions. These research materials were from light water and breeder mixed oxide reactors. The experimental vessels and extraneous piece parts resulting from the experiments were identified as eligible for disposal at the Waste Isolation Pilot Plant (WIPP) as remote-handled (RH) transuranic (TRU) waste. Once Sandia received the approval to dispose at WIPP, discussions began with the Carlsbad Field Office (CBFO) and Nuclear Waste Partnerships, LLC (NWP) to provide Central Characterization Program (CCP) support for certified acceptable knowledge, visual examination, and dose-to-curie for the repackaging effort. In addition to the WIPP support, Sandia was required to prepare a load plan describing the configuration of the parent containers and how they could be repackaged to meet WIPP and other regulatory requirements. However, all of these containers were packaged as material twenty (20) or thirty (30) years ago and the records of the packaging process and configuration were not documented as waste. Therefore, it seemed that the load plans were prepared with limited information regarding parent container configuration, hence in the dark. The design of the Auxiliary Hot Cell Facility (AHCF) in technical area (TA) V, where the repackaging was to take place, along with the shipping requirements for the RH 72-B cask, limited the options for repackaging. This configuration required that 0.114 m{sup 3} (30-gallon) containers be packaged in the hot cell, removed and placed into 0.208 m{sup 3} (55-gallon) containers to mitigate contamination issues. The material had been tracked as accountable nuclear material and Sandia had verified Material Control and Accountability (MC and A) data on each parent container. Based on the MC and A data, scaling factors could be determined and sampling and analysis was not required. However, it meant that parent containers could not be split into two daughter containers, though two or more parent containers could be combined into one daughter. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗