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At least 145 records · Page 8

Geometry of divergent-beam diffraction.

Divergent-beam diffraction geometry for interpretation of Kossel diffraction patterns in space group assignment lattice parameters and structure factor evaluation

CRYSTAL STRUCTURE↗

Crystallization and preliminary X-ray diffraction analysis of restriction endonuclease EcoRII

Crystals of the restriction endonuclease EcoRII have been obtained by the vapor-diffusion technique in the presence of ammonium sulfate or polyethylene glycol. The best crystals were grown with ammonium sulfate as a precipitant. Crystals with dimensions of up to 0.6 x 0. 6 x 0.6 mm have been observed. The crystals diffract to about 4.0 A resolution at a cryo-temperature of 100 K using a rotating-anode X-ray source and a Rigaku R-AXIS IV imaging-plate detector. The space group has been determined to be either I23 or I2(1)3, with unit-cell parameters a = b = c = 160.3 A, alpha = beta = gamma = 90 degrees. The crystal asymmetric unit contains two protein molecules, and self-rotation function analysis shows a pseudo-twofold symmetry relating the two monomers. Attempts to improve the resolution of crystal diffraction and to search for heavy-atom derivatives are under way.

Deoxyribonucleases, Type II Site-Specific/chemistr↗

Residual Stress Measurements of Ni-base Superalloys through Neutron Diffraction

Linear friction welding (LFW) is being considered for joining single crystal to polycrystalline nickel-base alloys for advanced high temperature gas turbine disks. Unfortunately, the transient thermal cycle during the welding generates undesirable residual stresses. Additionally, upon thermal treatment to relieve these residual stresses the weld joints often crack. To understand this issue, state-of-the-art neutron diffraction was performed near weld joints to quantify the residual stresses created by varying linear friction weld conditions. The residual stresses were measured along three orthogonal axes in both the polycrystalline LSHR and single crystal SC-180 alloys. Residual stress measurements using a contour method were used to compare the calculations obtained by neutron diffraction. The results suggest high residual stresses can be successfully reduced using both pre- and post-weld processing steps. Moreover, the effect of grain size and pre-heat temperatures on the LFW process were explored.

Superalloys↗

Noise diffraction patterns eliminated in coherent optical systems

Lens rotation technique of noise diffraction pattern elimination spreads diffracted energy, normally concentrated over small area of image, over much larger annular area. Technique advantages include simplified lens selecting process, reduced clean room requirements, and low cost equipment requirements.

Grebowsky, G. R.↗

Ray tracing program with options for diffraction gratings

Diffraction theory, developed in vectorial form and coded into ray tracing routines, permits tracing rays of any wavelength through surfaces that are plane, spherical, conical, or aspheric polynomial. Ruled diffraction gratings may run in either X-direction or Y-direction, where Z is optical axis.

Howell, B. J.↗

Diffraction of a plane wave by a three-dimensional corner

By the superposition of the conical solution for the diffraction of a plane pulse by a three dimensional corner, the solution for a general incident plane wave is constructed. A numerical program is presented for the computation of the pressure distribution on the surface due to an incident plane wave of any wave form and at any incident angle. Numerical examples are presented to show the pressure signature at several points on the surface due to incident wave with a front shock wave, two shock waves in succession, or a compression wave with same peak pressure. The examples show that when the distance of a point on the surface from the edges or the vertex is comparable to the distance for the front pressure raise to reach the maximum, the peak pressure at that point can be much less than that given by a regular reflection, because the diffracted wave front arrives at that point prior to the arrival of the peak incident wave.

Ting, L.↗

High voltage electron microscopy and electron diffraction of pyroxenes in type B lunar samples from Apollo 11

Lunar pyroxene 10044 specimens cleaved and sectioned by diamond knife ultramicrotomy were examined by standard (75 to 100 kV) and high voltage (200 kV) electron microscopy and diffraction. Salient findings based on evaluation of 2000 plates show uniform 300 to 600 A-wide bands, probably corresponding to single crystal domains, with lattice spacings of 2. A High resolution bright and dark field images of iron-rich and magnesium-rich crystals were compared with corresponding electron diffraction patterns. Possible relations of observed structures to magnetic domains were considered.

Fernandez-Moran, H.↗

Electron microscopy and diffraction of layered, superconducting intercalation complexes.

Several layered, transition metal dichalcogenide intercalation complexes with unique superconducting properties have been examined by high-resolution electron microscopy and electron diffraction. Details of the crystalline lattice and of the lattice imperfections have been directly resolved. The results can be correlated with the available X-ray diffraction and chemical data, and they confirm and extend the postulated models.

Fernandez-Moran, H.↗

Optical grating evaluator - A device for detailed measurement of diffraction grating efficiencies in the vacuum ultraviolet

A device for detailed measurement of diffraction grating efficiencies and over-all performance in the VUV has been designed and constructed at the Naval Research Laboratory. The system employs semiautomated mechanisms to scan the face of the grating with a narrow monochromatic beam, and an efficiency map of the grating surface is produced on a strip chart recorder. Grating efficiency in the various diffracted orders and intensity of light scattered between orders may also be measured. A unique feature is the ability to determine the angle and effectiveness of grating blaze and variations in blaze under different conditions of illumination.

Michels, D. J.↗

Diffraction theory techniques applied to aperture antennas on finite circular and square ground planes

Expressions which represent the elevation-plane patterns of a large TEM mode coax aperture and a TM-01 mode circular aperture on finite circular and square ground planes have been derived using geometrical theory of diffraction; design curves for the coax case are presented. The expressions for the field pattern were obtained by superposing the infinite ground plane solutions, the first-order diffracted field solutions, and the axial caustic solutions in their respective regions of validity. The pattern analyses for the coax and circular apertures are verified experimentally.

Cockrell, C. R.↗

Pinhole diffraction filter

Multistage diffraction filter consisting of coalined series of pinholes on parallel sheets can be used as nondegradable UV filter. Beam is attenuated as each pinhole diffracts radiation in controlled manner into divergent beam, and following pinhole accepts only small part of that beam.

Woodgate, B. E.↗

Diffraction effects on angular response of X-ray collimators

Angular responses have been measured for X-ray collimators with half-widths ranging from minutes of arc down to 10 arcsec. In the seconds-of-arc range, diffraction peaks at off-axis angles can masquerade as side lobes of the collimator angular response. Measurements and qualitative physical arguments lead to a rule of thumb for collimator design; namely, the angle of first minimum in the Fraunhofer single-slit diffraction pattern should be less than one-fourth of the collimator geometrical full-width at half-maximum intensity.

Blake, R. L.↗

Diffraction of sound by nearly rigid barriers

The diffraction of sound by barriers with surfaces of large, but finite, acoustic impedance was analyzed. Idealized source-barrier-receiver configurations in which the barriers may be considered as semi-infinite wedges are discussed. Particular attention is given to situations in which the source and receiver are at large distances from the tip of the wedge. The expression for the acoustic pressure in this limiting case is compared with the results of Pierce's analysis of diffraction by a rigid wedge. An expression for the insertion loss of a finite impedance barrier is compared with insertion loss formulas which are used extensively in selecting or designing barriers for noise control.

Hadden, W. J., Jr.↗

Diffraction calculation of occultation light curves in the presence of an isothermal atmosphere

From diffraction theory, light curves are calculated for stellar occultations by a planetary body with an isothermal atmosphere. The character of the resulting curves is determined by the scale height H, the Fresnel zone size l, the surface atmospheric refractivity, and the planetary radius. An exact general solution and two approximations are presented which are valid when H is much greater than l. The importance is assessed of accounting for diffraction effects of the limb when deducing atmospheric parameters from occultation light curves

French, R. G.↗