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At least 145 records · Page 8

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NASA NTRS1985

Characterization of Mode I and mixed-mode delamination growth in T300/5208 graphite/epoxy

The roles played by Mode I and Mode II strain-energy release rates (G-I and G-II, respectively) in inducing delamination growth under static and fatigue loading were investigated, using T300/5208 graphite/epoxy specimens. Double cantilever beam (DCB) specimens and cracked lap shear (CLS) specimens were used for pure Mode I and mixed-mode tests, respectively. Fatigue-induced delamination growth was characterized by constant-amplitude fatigue tests at a minimum to maximum cyclic load ratio of 0.05 and a frequency of 10 Hz. During the tests, the maximum and minimum strain-energy release rates (Gmax, Gmin) and the delamination growth rate (da/dN) were monitored. Static tests on mixed-mode CLS specimens measured the total strain-energy release rate, which was broken into G-I and G-II components using finite-element analysis. A power-law relationship between da/dN and G-Imax, and da/dN and Gmax were obtained from fatigue test results on DCB and CLS specimens, respectively. The power law for a pure Mode II delamination was derived from CLS results by subtracting the contribution due to G-I.

Ramkumar, R. L.↗

NASA NTRS1985

Effects of strain rate on delamination fracture toughness of graphite/epoxy

The objective of this paper is to evaluate various experimental techniques and analysis methods for the characterization of interlaminar fracture toughness, and to determine the effects of strain rate on that property for a graphite/epoxy composite. Mode I interlaminar fracture was investigated by means of a double-cantilever beam (DCB) specimen for AS-4/3501-6 graphite/epoxy. Hinged tabs were used to insure unrestrained rotation at the free ends. Specimens were loaded at quasi-static deflection rates of up to 8.5 mm/s corresponding to crack extension rates of over 51 mm/s. Crack extension was monitored by means of strain gages mounted on the surface of the specimen, or a conductive-paint circuit attached to the edge of the DCB specimen. Continuous records were obtained of load, deflection, and crack extension for determination of the strain energy release rate. The latter was expressed as a power law of the crack extension velocity. Results indicate that the strain energy release rate increases with crack velocity by up to 28 percent for the range of rates considered.

Daniel, I. M.↗

NASA NTRS1986

Fracture toughness tests on plasma-sprayed coatings

Fracture toughness measurements have been performed on plasma-sprayed coatings. The intrinsic fracture toughness of plasma-sprayed coatings may be ascertained by means of a double cantilever beam (DCB) test. Emphasis is placed on calibration of the specimen geometry. Representative values for alumina coatings are presented.

Berndt, C. C.↗

NASA NTRS1986

Tetraglycidyl epoxy resins and graphite fiber composites cured with flexibilized aromatic diamines

Studies were performed to synthesize new ether modified, flexibilized aromatic diamine hardeners for curing epoxy resins. The effect of moisture absorption on the glass transition temperatures of a tetraglycidyl epoxy, MY 720, cured with flexibilized hardeners and a conventional aromatic diamine was studied. Unidirectional composites, using epoxy-sized Celion 6000 graphite fiber as the reinforcement, were fabricated. The room temperature and 300 F mechanical properties of the composites, before and after moisture exposure, were determined. The Mode I interlaminar fracture toughness of the composites was characterized using a double cantilever beam technique to calculate the critical strain energy release rate.

Delvigs, P.↗

NASA NTRS1986

Impact resistance and interlaminar fracture toughness of through-the-thickness reinforced graphite/epoxy

Five through-the-thickness stitch configurations are analyzed to determine the effect of impact resistance and interlaminar fracture toughness on T3000/3501-6 graphite/epoxy. The test specimens were stitched with either polyester or Kevlar yarns and with various stitch parameters. Tension and compression mechanical, impact and compression-after-impact, and double cantilever beam tests were conducted. It is observed that the stitched laminates have tension and compression strengths 20-25 percent lower than the strengths of unstitched laminates, the tension strength of stitched laminates is reduced with increasing number of stitches, and the compression strength increases as the number of stitches are increased. The impact data reveal that the Kevlar stitched laminates have less damage than unstitched laminates; the most effective configuration for suppressing impact damage and improving interlaminar fracture toughness consists of Kevlar yarns 1/4 inch apart with eight stitches per inch. The mode 1 critical strain energy release rate for the 1/4 inch Kevlar eight stitch laminate was calculated as 30 times higher than that of the unstitched.

Dexter, H. B.↗

NASA NTRS1986

Characterization of mode I and mixed-mode failure of adhesive bonds between composite adherends

A combined experimental and analytical investigation of an adhesively bonded composite joint was conducted to characterize both the static and fatigue beyond growth mechanism under mode 1 and mixed-mode 1 and 2 loadings. Two bonded systems were studied: graphite/epoxy adherends bonded with EC 3445 and FM-300 adhesives. For each bonded system, two specimen types were tested: a double-cantilever-beam specimen for mode 1 loading and a cracked-lapshear specimen for mixed-mode 1 and 2 loading. In all specimens tested, failure occurred in the form of debond growth. Debonding always occurred in a cohesive manner with EC 3445 adhesive. The FM-300 adhesive debonded in a cohesive manner under mixed-mode 1 and 2 loading, but in a cohesive, adhesive, or combined cohesive and adhesive manner under mode 1 loading. Total strain-energy release rate appeared to be the driving parameter for debond growth under static and fatigue loadings.

Mall, S.↗

NASA NTRS1986

Effect of loading rate on dynamic fracture of reaction bonded silicon nitride

Wedge-loaded, modified tapered double cantilever beam (WL-MTDCB) specimens under impact loading were used to determine the room temperature dynamic fracture response of reaction bonded silicon nitride (RBSN). The crack extension history, with the exception of the terminal phase, was similar to that obtained under static loading. Like its static counterpart, a distinct crack acceleration phase, which was not observed in dynamic fracture of steel and brittle polymers, was noted. Unlike its static counterpart, the crack continued to propagate at nearly its terminal velocity under a low dynamic stress intensity factor during the terminal phase of crack propagation. These and previously obtained results for glass and RBSN show that dynamic crack arrest under a positive dynamic stress intensity factor is unlikely in static and impact loaded structural ceramics.

Liaw, B. M.↗

NASA NTRS1985

Tough composite materials: Recent developments

The present volume broadly considers topics in composite fracture toughness and impact behavior characterization, composite system constituent properties and their interrelationships, and matrix systems' synthesis and characterization. Attention is given to the characterization of interlaminar crack growth in composites by means of the double cantilever beam specimen, the characterization of delamination resistance in toughened resin composites, the effect of impact damage and open holes on the compressive strength of tough resin/high strain fiber laminates, the effect of matrix and fiber properties on compression failure mechanisms and impact resistance, the relation of toughened neat resin properties to advanced composite mechanical properties, and constituent and composite properties' relationships in thermosetting matrices. Also treated are the effect of cross-link density on the toughening mechanism of elastomer-modified epoxies, the chemistry of fiber/resin interfaces, novel carbon fibers and their properties, the development of a heterogeneous laminating resin, solvent-resistant thermoplastics, NASA Lewis research in advanced composites, and opportunities for the application of composites in commercial aircraft transport structures.

Vosteen, L. F.↗

NASA NTRS1986

Loading rate effect on interlaminar fracture toughness of a thermoplastic composite

A study was undertaken to investigate the loading rate effect on delamination fracture initiation toughness of a thermoplastic composite. For this purpose, double cantilever beam specimens of graphite/PEEK were tested in a displacement controlled mode using an Instron tensile test machine. Specimens were loaded at various crosshead speeds ranging from 0.05 cm/min to 100 cm/min. The interlaminar fracture toughness was found to decrease with increasing loading rate, and this decrease was more than one hundred percent over the five decades of loading rate employed.

Mall, S.↗

NASA NTRS1986

Mode 1 delamination growth in adhesively bonded joints under static and fatigue loads

The objective of this investigation was to characterize the pure mode 1 delamination growth in metal to metal adhesively bonded joints under static and fatigue loading conditions, using FM 73 adhesive. Double cantilever beam specimens (DCB) were used for pure mode 1 tests. Aluminum 2024-T3 adherends were bonded with FM 73 adhesive. Delamination was introduced during fabrication by inserting a Teflon film between the two adherends. The mode 1 strain energy release rate G sub I sub c was obtained directly from static DCB tests conducted in accordance with the ASTM designation D1876-12. Constant amplitude fatigue tests on DCB specimens were conducted to determine the relationship between delamination growth rate da/dN and strain energy release rate G sub I sub c for a pure mode 1 delamination growth. It is found that the debond propagation rate in adhesive joints using FM 73 is more sensitive to errors in design load than is typical crack growth rate in metallic structures.

Biswas, S. C.↗

NASA NTRS1986

The role of damage-softened material behavior in the fracture of composites and adhesives

Failure mechanisms of materials under very high strains experienced at and ahead of the crack tip such as formation, growth, and interaction of microvoids in ductile materials, microcracks in brittle solids or crazes in polymers and adhesives are represented by one-dimensional, nonlinear stress-strain relations possessing different ways by which the material loses capacity to carry load up to fracture or total separation. A double cantilever beam (DCB) type specimen is considered. The nonlinear material is confined to a thin strip between the two elastic beams loaded by a wedge. The problem is first modeled as a beam on a nonlinear foundation. The pertinent equation is solved numerically as a two-point boundary value problem for both the stationary and the quasi-stationay propagating crack. A finite element model is then used to model the problem in more detail in order to assess the adequacy of the beam model for the reduction of experimental data to determine in-situ properties of the thin interlayer.

Ungsuwarungsri, T.↗

NASA NTRS1986

Effect of adherend thickness and mixed mode loading on debond growth in adhesively bonded composite joints

Symmetric and unsymmetric double cantilever beam (DCB) specimens were tested and analyzed to assess the effect of: (1) adherend thickness, and (2) a predominantly mode I mixed mode loading on cyclic debond growth and static fracture toughness. The specimens were made of unidirectional composite (T300/5208) adherends bonded together with EC3445 structural adhesive. The thickness was 8, 16, or 24 plies. The experimental results indicated that the static fracture toughness increases and the cyclic debond growth rate decreases with increasing adherend thickness. This behavior was related to the length of the plastic zone ahead of the debond tip. For the symmetric DCB specimens, it was further found that displacement control tests resulted in higher debond growth rates than did load control tests. While the symmetric DCB tests always resulted in cohesive failures in the bondline, the unsymmetric DCB tests resulted in the debond growing into the thinner adherend and the damage progressing as delamination in that adherend. This behavior resulted in much lower fracture toughness and damage growth rates than found in the symmetric DCB tests.

Mangalgiri, P. D.↗

NASA NTRS1987

Micro and macro approaches to tough polymers for composites

The progress to date on the development of techniques to toughen continuous thermoplastic composites is summarized. The work, using the approach of toughening the polycarbonate composite matrix with rubber particles, has focused on determining the differences between Double Cantilever Beam (DCB) samples molded inhouse and those molded by NASA. Specifically, an effort was made to account for the differences in fracture toughness observed between the various specimens. In addition, preliminary results of tensile dilatometry tests are described; these tests suggest that processes leading to increased volume and enhanced shear banding are occurring within the rubber toughened system. The results of the effort using another approach, the preparation of random block copolycarbonates, are presented. The synthetic route to these species was modified so that higher molecular weights of these materials can be obtained. In addition, an attempt is being made to determine the exact block length or the number of functional groups in the oligomers since this procedure also should lead to high molecular weight materials. Dynamic mechanical analysis of the copolymer prepared so far indicates that the scale of cooperative molecular motion of the PBA polycarbonate at sub-Tg temperatures is larger than five monomer units. Efforts to find a suitable rubber-toughener for a thermoset system (bismaleimides) is also discussed. Included is a description of the various tougheners intended for use or currently being used.

Yee, Albert F.↗

NASA NTRS1986

The effects of radiation on the interlaminar fracture toughness of a graphite/epoxy composite

An experimental study is made of the effect of electron irradiation (10 to the 10th rad), simulating a 30-year geosynchronous orbit exposure, on the fracture toughness of a graphite/epoxy composite, T300/934. The double cantilever beam (DBC) test is used to determine Mode I (peel) critical strain energy release rate and the edge delamination tension (EDT) test is used to determine mixed Mode I and II (peel and shear) critical strain energy release rate. It is found that the electron interaction of the epoxy matrix material enhances the fracture toughness properties of the composite and that the test temperature has a significant effect on the fracture toughness of both baseline and irradiated material.

Funk, J. G.↗

NASA NTRS1987

Rate-dependent mode I interlaminar crack growth mechanisms in graphite/epoxy and graphite/PEEK

In this paper the mode I fracture behavior of graphite/epoxy and graphite/PEEK composites is examined over four decades of crosshead rates (0.25-250 mm/min). Straight-sided double-cantilever-beam specimens consisting of unidirectional laminates were tested at room temperature. For graphite/epoxy the load-deflection response was linear to fracture, and stable slow crack growth initiating at the highest load level was observed for all rates tested. In contrast, mode I crack growth in the graphite/PEEK material was often unstable and showed stick-slip behavior. Subcritical crack growth occurring prior to the onset of fracture was observed at intermediate displacement rates. A mechanism for the fracture behavior of the graphite/PEEK material (based on viscoelastic, plastic, and microcrack coalescence in the process zone) is proposed and related to the observed rate-dependent phenomena.

Gillespie, J. W., Jr.↗

NASA NTRS1987

Matrix resin effects in composite delamination - Mode I fracture aspects

A number of thermoset, toughened thermoset, and thermoplastic resin matrix systems were characterized for Mode I critical strain energy release rates, and their composites were tested for interlaminar critical strain energy release rates using the double cantilever beam method. A clear correlation is found between the two sets of data. With brittle resins, the interlaminar critical strain energy release rates are somewhat larger than the neat resin values due to a full transfer of the neat resin toughness to the composite and toughening mechanisms associated with crack growth. With tougher matrices, the higher critical strain energy release rates are only partially transferred to the composites, presumably because the fibers restrict the crack-tip deformation zones.

Hunston, Donald L.↗

NASA NTRS1987

Rate effects on delamiantion fracture toughness of a toughened graphite/epoxy

The objective of this study was to determine the effects of loading rate on interlaminar fracture toughness of T300/F-185 graphite/epoxy composite, having an elastomer-modified epoxy resin matrix. Mode I interlaminar fracture was investigated by means of uniform width and width-tapered double cantilever beam (DCB) specimens. Hinged tabs were used to insure unrestrained rotation at the free ends. Specimens were loaded at quasi-static deflection rates of up to 8.5 mm/s corresponding to crack extension rates of up to 21 mm/s. Crack extension was monitored by means of strain gages mounted on the surface of the specimen. Continuous records were obtained of load, deflection, and crack extension for determination of the strain energy release rate. The latter was calculated by means of the area method and beam analysis method, and expressed as a power law of the crack extension velocity. Results indicate that the strain energy release rate decreases with crack velocity by over 20 percent over three decades of crack velocity.

Daniel, Isaac M.↗

NASA NTRS1988

Measuring Flow By Holographic Interferometry

Flow field reconstructed by computer-aided tomography. Holographic interferogram formed on photographic plate by interference between object and reference beams. Double-exposure interferograms taken with blade rotating and stationary at various positions processed to reconstruct mathematically airflow about model helicopter rotor blade.

Yu, Yung H.↗