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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 145 records · Page 8
All sourcesNASA NTRSDOE OSTI
DOE OSTI2021

In Situ Synchrotron Tensile Investigations on Ultrasonic Additive Manufactured (UAM) Zirconium

The microstructure evolution of ultrasonic additive manufactured (UAM) zirconium under room temperature uniaxial tensile straining is reported. Miniature dog-bone tensile specimens of two orientations were cut from a UAM zirconium bar for in situ synchrotron tensile tests. Wide-angle X-ray scattering (WAXS) scanning at the Advanced Photon Source (APS) at Argonne National Laboratory was used to unveil the changes in microstructure of the entire gauge regions throughout the straining. A series of WAXS data analysis methods were utilized to quantify both elastic and plastic deformation mechanisms within the strained specimens. Stress concentrations were identified during early stage of plastic deformation, which become candidate necking positions and eventually lead to failure. Fracture surface analysis implied that these stress concentration locations may be correlated to the fabrication defects, providing insightful guidance for future improvement of the UAM zirconium process.

36 MATERIALS SCIENCE↗
NASA NTRS1976

An experimental method to obtain the elastic strain energy function from torsion-tension tests

It is shown that by employing a torsion-tension test, it is possible to have a complete mapping near the origin of the two principal strain invariants associated with the rate of change of the strain energy function. However, the mathematical representation of the twist moment and normal forces vs strain and the strain energy function are complex. This problem is solved by using a set of solid cylindrical bars with different diameters such that the difference in diameter of two successive bars is small. The stress-strain equations can be grossly oversimplified by considering differences in twist moment and normal force as a function of difference in radius.

Peng, S. T. J.↗
NASA NTRS1978

Compression of rehydratable vegetables and cereals

Characteristics of freeze-dried compressed carrots, such as rehydration, volatile retention, and texture, were studied by relating histological changes to textural quality evaluation, and by determining the effects of storage temperature on freeze-dried compressed carrot bars. Results show that samples compressed with a high moisture content undergo only slight structural damage and rehydrate quickly. Cellular disruption as a result of compression at low moisture levels was the main reason for rehydration and texture differences. Products prepared from carrot cubes having 48% moisture compared favorably with a freshly cooked product in cohesiveness and elasticity, but were found slightly harder and more chewy.

Burns, E. E.↗
DOE OSTI2026

Insights into mixing of non-isothermal multi-polymer melts for complex plastics recycling

Catalytic recycling or upcycling of plastics is often limited not by catalyst performance, but by transport, arising from highly viscous, non-Newtonian polymer melts. In this work, we develop a reactor-scale framework that integrates rheological measurements, constitutive modeling, computational fluid dynamics (CFD), and experiments to quantify mixing, heat transfer, and dispersion in surrogate hydrocarbon melts representing mixed plastics systems. Temperature- and shear rate-dependent viscosity of low-density polyethylene (LDPE) and high-density polyethylene (HDPE) is measured to create two surrogate polymers (PLD and PHD) that capture the dominant shear-thinning flow behavior while neglecting strong elastic effects, enabling tractable simulation of non-isothermal, polymer-melt mixing using a Carreau-Arrhenius generalized Newtonian framework. Three-dimensional CFD simulations are employed to evaluate impeller performance in PLD using mixing time, cavern volume, thermal uniformity, and interfacial area for regimes in which viscoelastic effects are not dominant. We show that magnetic stir bars commonly used in lab-scale studies produce large thermal gradients (~60 °C) and poor mixing, even under idealized power delivery and polymer flow conditions. In contrast, close-clearance anchor impellers achieve near-isothermal operation, reduce mixing times by up to 5×, and provide >90% active circulation volume. We further demonstrate that, at low pseudo-Deborah number (De*), motor power requirements can be predicted directly from shear rate-dependent rheology using the Carreau-Arrhenius framework, enabling rational selection of operating conditions. Extension to surrogate immiscible multi-polymer systems based on PLD and PHD shows that interfacial area is highly sensitive to operating conditions and impeller design, with coaxial anchor-turbine configurations enhancing dispersion by up to 4 × .

Close-clearance impellers↗
NASA NTRS1999

Real-Time Leaky Lamb Wave Spectrum Measurement and Its Application to NDE of Composites

Numerous analytical and theoretical studies of the behavior of leaky Lamb waves (LLW) in composite materials were documented in the literature. One of the key issues that are constraining the application of this method as a practical tool is the amount of data that needs to be acquired and the slow process that is involved with such experiments. Recently, a methodology that allows quasi real-time acquisition of LLW dispersion data was developed. At each angle of incidence the reflection spectrum is available in real time from the experimental setup and it can be used for rapid detection of the defects. This technique can be used to rapidly acquire the various plate wave modes along various angles of incidence for the characterization of the material elastic properties. The experimental method and data acquisition technique will be described in this paper. Experimental data was used to examine a series of flaws including porosity and delaminations and demonstrated the efficiency of the developed technique.

Lih, Shyh-Shiuh↗
NASA NTRS2001

Theoretical Investigation of Thermo-Mechanical Behavior of Carbon Nanotube-Based Composites Using the Integral Transform Method

This project uses the integral transform technique to model the problem of nanotube behavior as an axially symmetric system of shells. Assuming that the nanotube behavior can be described by the equations of elasticity, we seek a stress function x which satisfies the biharmonic equation: del(exp 4) chi = [partial deriv(r(exp 2)) + partial deriv(r) + partial deriv(z(exp 2))] chi = 0. The method of integral transformations is used to transform the differential equation. The symmetry with respect to the z-axis indicates that we only need to consider the sine transform of the stress function: X(bar)(r,zeta) = integral(from 0 to infinity) chi(r,z)sin(zeta,z) dz.

Pawloski, Janice S.↗
NASA NTRS1971

Stability of circulatory elastic systems in the presence of magnetic damping.

The effect of a type of magnetic damping on the stability of equilibrium of some circulatory elastic systems is examined. A simple system with two degrees of freedom is considered first, and a destabilization is found to be caused by the magnetic field. The nature of the destabilization, however, is not identical to that caused by internal viscous damping. The differences and similarities between the two effects are discussed, and the results are also compared with those of linear external viscous damping. A continuous cantilever bar subjected to a follower force at its free end is then examined. It is found that the critical load is independent of the strength of the magnetic field, and is considerably lower than the corresponding critical load in the absence of a magnetic field. Finally, the continuous cantilever is treated approximately by Galerkin's procedure and also by using a two-degree-of-freedom model of the cantilever; the results obtained are qualitatively the same.

Smith, T. E.↗
NASA NTRS1973

Computational fracture mechanics

Numerical procedures for accurate determination of elastic stress intensity factors for the general two-dimensional crack problem are reviewed. The elastic perfectly plastic state of crack tip deformation is studied by a finite element procedure. Elastic-plastic fields in the immediate vicinity of a crack tip are determined numerically by finite element procedures based on asymptotic studies of crack tip singularities in plastic materials. The small-scale yielding problem is modeled, and expressions for crack tip opening displacement, shear singularity amplitude, and plastic zone extent are derived. A finite element solution to the large-scale yielding of a circumferentially cracked round tension bar is obtained. The three-dimensional aspects of flawed structures and numerical methods of treating them are studied. Ductile fracture mechanisms, in particular crack tip fracture on the microscale, are discussed.

Rice, J. R.↗
DOE OSTI2026

Dynamic crushing of metal lattice metamaterials: Shock mode diagrams and transition to topology-independent compaction regime

Additively manufactured lattice metamaterials offer design versatility in strength and energy absorption and provide an additional degree of freedom through the selection of the lattice topology. Under quasistatic loading, the unit cell structure can strongly affect the stiffness, yield, and post-yield behavior, but whether and to what degree the effect of lattice topology persists into dynamic loading scenarios, up to the compaction shock regime, has not been established. LLNL’ s ALE3D hydrocode was used to perform a computational investigation of dynamic loading in multiple lattice types, including the gyroid, octet, Schwarz D, and rhombic dodecahedron, under impact velocities from 0.25 to 2.25 km/s. Shock Hugoniots for each lattice topology are generated and compared, suggesting that above a critical velocity, distinctions between architectures may not persevere and compacted lattices behave similarly. Here, to investigate the transition between topology-dependent quasistatic compression and the topology-independent regime above the critical velocity, a one-dimensional elastic-linear hardening plasticity-densified solid (E-LHP-DS) shock model for lattice materials was developed that relies upon confined compression to link the quasistatic and shock mechanics. Unlike similar works, the model does not assume rigid behavior prior to yield or locking behavior at densification, allowing a richer exploration of lattice mechanics. With only six parameters, the analytical model simultaneously fit quasistatic confined compression simulations for relative densities 0.1 $≤ \bar{ρ} ≤$ 0.9 and predicted dynamic compaction behavior to traverse several distinct shock modes, each defined by a critical impact speed (equivalently, critical stresses). Comparing the numerical results to the one-dimensional E-LHP-DS shock model predictions suggests that the topology-independence under strong shocks is linked to the onset of densification, which can be predicted based on quasistatic confined compression results.

Cellular material↗
NASA NTRS1972

Elastic velocity and Q factor measurements on Apollo 12, 14, and 15 rocks.

The Rayleigh wave velocities (vR) in one Apollo 12, one Apollo 15, and two Apollo 14 rocks were measured by the impulse technique. For 14310 vR = 1.20 km/sec; for 14321 vR = 0.9 km/sec; for 12063, on which the orientation dependence was studied, vR = 1.16-1.59 km/sec; for 15555 vR = 0.32 km/sec; and for synthetic rock 10017 analogue vR = 2.26 km/sec. This represents a larger spread by a factor of 3 than previously reported on lunar igneous rock. Absolute Q factor measurements were performed on one Apollo 14 rock by the vibrating bar technique. Under exposure to high vacuum and low temperatures, the Q factor is shown to increase towards values approaching the low end of the range of estimates from seismic data.

Tittmann, B. R.↗
DOE OSTI2021

Dynamic flow stress of pure polycrystalline aluminum: Pressure-shear plate impact experiments and extension of dislocation-based modeling to large strains

The dynamic thermo-mechanical behavior of pure aluminum has attracted renewed interest lately due to experimental observations of an anomalous increase in Hugoniot Elastic Limit (HEL) at incipient plasticity and elevated temperatures in polycrystalline pure metals. In context of current dislocation-mediated plasticity models for metals, this increase in dynamic strength is indicative of a transition in the rate controlling mechanism for dislocation glide from being thermally assisted to phonon-drag restricted due to increase in phonon viscosity at elevated temperatures. Though these studies have helped to shed light on these important mechanisms operative in FCC metals at incipient plasticity, the extent to which they contribute to flow stress, particularly at larger strains, remains unclear. Here, we address these questions through a combined experimental and modeling effort focused on investigating the evolution of dynamic flow stress in polycrystalline aluminum using experimental data gathered from a series of combined pressure-and-shear plate impact (PSPI) experiments designed to reveal the flow stress of pure aluminum at strain rates ~ 10 5 /s, plastic strains of up to 40% and temperatures ranging from room to 866 K. In all cases, the flow stress of aluminum, as inferred from the measured transverse particle velocity histories at the free surface of an elastic tungsten carbide target plate, reveals saturation with increasing plastic strains at stress levels that decrease with increasing test temperatures. Numerical simulations are performed to correlate the experimentally observed temperature and strain rate dependence of flow stress at small and large plastic strains using the Austin-McDowell dislocation-mediated plasticity model parametrized to normal plate impact experiments conducted in an earlier study by Zaretsky and Kanel (2012). Extensions to the model are made to better represent dynamic behavior of pure aluminum at larger plastic strains as observed in elevated temperature split Hopkinson Pressure bar (SPHB) experiments of Samanta (1971) and Lindholm and Yeakly (1965), and the combined pressure-and-shear plate-impact experiments conducted in the present study. The main theoretical extension to the Austin-McDowell model made in this paper is the introduction of a new rate- and temperature- dependent dynamic recovery function, which can potentially allow for an effective reduction in the rate of accumulation of dislocations at large plastic strains. The numerical predictions of the revised and re-calibrated plasticity model are brought into agreement with the experimental observations, correlating sufficiently well with dynamic yield stress at incipient plasticity and the flow stress levels at larger plastic strains, plastic strain rates in the range 10 3 – 10 6 /s, and elevated temperatures up to near melt. The model, in concert with the experimental measurements, suggests that at incipient plasticity the rate governing mechanism for plastic flow is phonon-drag restricted dislocation glide, whereas, at higher magnitudes of plastic strain, it transitions to stress-assisted thermally activated glide. The transition between these two rate governing mechanisms is controlled by the evolution of dislocations throughout the deformation process.

36 MATERIALS SCIENCE↗
NASA NTRS1994

Ultrasonic Measurement Of Elastic Constants Of Composites

Ultrasonic testing system yields data on elastic constants of matrix/fiber laminated composite material. Related to one described in "Ultrasonic System Measures Elastic Properties of Composites" (NPO-18729). Tests performed nondestructive, and involve access by ultrasonic probes to only one side of material specimen. In comparison with other available ultrasonic testing systems, this system relatively inexpensive, and based on testing technique that is simpler and rapidly yields more-accurate results.

Bar-Cohen, Yoseph↗
NASA NTRS1995

Low Frequency Guided Plate Waves Propagation in Fiber Reinforced Composites

Conventional destructive techniques for the determination of the elastic stiffness constants of composite materials can be costly and often inaccurate. Reliable nondestructive evaluation methods for monitoring the integrity of composite materials and structures are needed. Guided wave propagation in isotropic plate have been studied. Studies on the low frequency symmetric guide waves are presented.

applied mechanics and materials plate wave propaga↗
DOE OSTI2022

Water Mediated Proton Hopping Furazan Mechanism that Accelerates the Decomposition of TATB

The dominant initial decomposition mechanism of TATB is believed to be a dehydration reaction that forms mono- and di-furazans, although other mechanisms have been reported. In this work, a mono-furazan mechanism is discovered that involves a proton hopping process between TATB and water. A first principles nudge elastic band calculation was performed that shows the mechanism has an energy barrier of 44.1 kcal/mol, 25.4 kcal/mol lower than the monofurazan mechanism without water. The reaction rate of the proton hopping mechanism was found to be 10 7 to 10 12 times (at 300-600 K) higher than the mechanism without water. Metadynamics simulations were also performed that indicate the mechanism is qualitatively more probable at lower temperatures (near 300 K) and higher pressures (near 100 bar), although a quantitative confirmation is needed. Future work should focus on modeling the proton hopping mechanism in the condensed state at elevated temperatures (near 600 K).

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
NASA NTRS1978

Finite element modeling of stress in the Nazca plate - Driving forces and plate boundary earthquakes

The state of stress within the Nazca plate due to plate driving forces and large plate boundary earthquakes has been analyzed by applying a finite element method using the wave front solution technique to models of the intraplate stress field in a single plate using a refined grid. Although only static elastic models have been explicitly calculated, certain limiting cases of an elastic plate over a viscous asthenosphere were also treated. A state of nearly east-west compression inferred from the source mechanism of thrust earthquakes in the interior of the plate requires ridge pushing forces. The net pulling force on the oceanic plate by the subducted slab has a maximum value comparable to pushing forces. The estimated horizontal deviatoric stress in intraplate regions, based on potential forces associated with the ridge, is on the order of a few hundred bars. The intraplate stress field in the region of the 1960 earthquake may change by a few tens of bars at most once the asthenosphere has relaxed, with changes on the order of one bar occurring at greater distances into the plate. The changes in the intraplate stress field are probably not noticeable unless the lithosphere is near failure.

Richardson, R. M.↗
NASA NTRS1993

Nondestructive Characterization of the Elastic Constants of Fiber Reinforced Composites

Composite structural components may be subjected to a variety of defects resulting in a sharp reduction in their load carrying capacity or even catastrophic failure...A nondestructive method based on ultrasonics has recently been developed for the quantitative evaluation of composite structural components during service...In this paper the method is applied to determine the stiffness constants of unidirectional graphite/epoxy materials.

composites↗