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At least 145 records · Page 8

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NASA NTRS1979

Graphite fiber reinforced glass matrix composites for aerospace applications

The graphite fiber reinforced glass matrix composite system is described. Although this composite is not yet a mature material, it possesses low density, attractive mechanical properties at elevated temperatures, and good environmental stability. Properties are reported for a borosilicate glass matrix unidirectionally reinforced with 60 volume percent HMS graphite fiber. The flexural strength and fatigue characteristics at room and elevated temperature, resistance to thermal cycling and continuous high temperature oxidation, and thermal expansion characteristics of the composite are reported. The properties of this new composite are compared to those of advanced resin and metal matrix composites showing that graphite fiber reinforced glass matrix composites are attractive for aerospace applications.

Prewo, K. M.↗

NASA NTRS1980

High Temperature Resin Matrix Composites for Aerospace Structures

Accomplishments and the outlook for graphite-polyimide composite structures are briefly outlined. Laminates, skin-stiffened and honeycomb sandwich panels, chopped fiber moldings, and structural components were fabricated with Celion/LARC-160 and Celion/PMR-15 composite materials. Interlaminar shear and flexure strength data obtained on as-fabricated specimens and specimens that were exposed for 125 hours at 589 K indicate that epoxy sized and polyimide sized Celion graphite fibers exhibit essentially the same behavior in a PMR-15 matrix composite. Analyses and tests of graphite-polyimide compression and shear panels indicate that utilization in moderately loaded applications offers the potential for achieving a 30 to 50 percent reduction in structural mass compared to conventional aluminum panels. Data on effects of moisture, temperature, thermal cycling, and shuttle fluids on mechanical properties indicate that both LARC-160 and PMR-15 are suitable matrix materials for a graphite-polyimide aft body flap. No technical road blocks to building a graphite-polyimide composite aft body flap are identified.

Davis, J. G., Jr.↗

NASA NTRS1980

State-of-the-art SiAlON materials

The state of the art of SiAlONs is examined. The review includes work on phase relations, crystal structure, synthesis, fabrication, and properties of various SiAlONs. The essential features of compositions, fabrication methods, and microstructure are reviewed. High temperature flexure strength, creep, fracture toughness, oxidation, and thermal shock resistance are discussed. These data are compared to those for some currently produced silicon nitride ceramics to assess the potential of SiAlON materials for use in advanced gas turbine engines.

Dutta, S.↗

NASA NTRS1979

State-of-the-art of SiAlON materials

The state of the art of 'SiAlONs' is reviewed, noting that the term has become a generic one applied to Si3N4 based materials. Attention is given to work on phase relations, crystal structure, synthesis, fabrication, and properties of various SiAlONs. Also discussed are the essential features of compositions, fabrication methods, and microstructures. In addition, consideration is given to high temperature flexure strength, creep, fracture toughness, oxidation, and thermal shock resistance. Finally, these data are compared to those for some currently produced silicon nitride ceramics to assess the potential of SiAlON materials for use in advanced gas turbine engines.

Dutta, S.↗

NASA NTRS1980

Effect of High Energy Radiation on Mechanical Properties of Graphite Fiber Reinforced Composites

The flexural strength and average modulus of graphite fiber reinforced composites were tested before and after exposure to 0.5 Mev electron radiation and 1.33 Mev gamma radiation by using a three point bending test (ASTM D-790). The irradiation was conducted on vacuum treated samples. Graphite fiber/epoxy (T300/5208), graphite fiber/polyimide (C6000/PMR 15) and graphite fiber/polysulfone (C6000/P1700) composites after being irradiated with 0.5 Mev electron radiation in vacuum up to 5000 Mrad, show increases in stress and modulus of approximately 12% compared with the controls. Graphite fiber/epoxy (T300/5208 and AS/3501-6), after being irradiated with 1.33 Mev gamma radiation up to 360 Mrads, show increases in stress and modulus of approximately 6% at 167 Mrad compared with the controls. Results suggest that the graphite fiber composites studied should withstand the high energy radiation in a space environment for a considerable time, e.g., over 30 years.

Naranong, N.↗

NASA NTRS1981

Imide modified epoxy matrix resins

High char yield epoxy using novel bisimide amines (BIA's) as curing agents with a state of the art epoxy resin was developed. Stoichiometric quantities of the epoxy resin and the BIA's were studied to determine the cure cycle required for preparation of resin specimens. The bisimide cured epoxies were designated IME's (imide modified epoxy). The physical, thermal and mechanical properties of these novel resins were determined. The levels of moisture absorption exhibited by the bisimide amine cured expoxies (IME's) were considerably lower than the state of the art epoxies. The strain-to-failure of the control resin system was improved 25% by replacement of DDS with 6F-DDS. Each BIA containing resin exhibited twice the char yield of the control resin MY 720/DDS. Graphite fiber reinforced control (C) and IME resins were fabricated and characterized. Two of the composite systems showed superior properties compared to the other Celion 6000/IME composite systems and state of the art graphite epoxy systems. The two systems exhibited excellent wet shear and flexural strengths and moduli at 300 and 350 F.

Scola, D. A.↗

NASA NTRS1980

Environmental effects on graphite fiber reinforced PMR-15 polyimide

Studies were conducted to establish the effects of thermo-oxidative and hydrothermal exposure on the mechanical properties of T300 graphite fabric reinforced PMR-15 composites. The effects of hydrothermal exposure on the mechanical properties of HTS-2 continuous graphite fiber composites were also investigated. The thermo-oxidative stability characteristics of T300 fabric and T300 fabric/PMR-15 composites were determined. Flexural strengths of specimens were determined. The useful lifetime of T300 fabric/PMR-15 composites in air at 316 C was found to be about 100 hours. The useful lifetimes in air at 228 and 260 C were determined to be 500 and 1000 hours, respectively. Absorbed moisture was found to reduce the elevated temperature properties of both the T300 fabricate and HTS-2 continuous fiber composites. The moisture effect was found to be reversible.

Serafini, T. T.↗

NASA NTRS1980

Thermal decomposition of a Si3N4-22 wt% Al2O3 alloy

It is pointed out that materials near the Si3N4 corner of the Si3N4-AlN-Al2O3-SiO2 quaternary, termed sialons are candidate materials for high performance applications. Hot pressed alloys in this system are useful because they possess high flexure strengths and good oxidation and creep resistance. The results of the thermal decomposition studies conducted indicate that dissociation and resulting weight loss lead to inhomogeneous specimens. Material loss comes primarily from near the surface (at least initially) thus causing differences between the composition of the surface material and the bulk. In these specimens, the O-prime phase was found to be the least stable to dissociation and the beta-prime phase the most stable. This result is in accord with the conclusions of Mitomo et al. (1979) that Si2N2O has a larger equilibrium SiO partial pressure than either the X phase or the beta-prime phase.

Ditchek, B. M.↗

NASA NTRS1982

On isostasy at Atlantic-type continental margins

The concept of isostasy describes the manner in which topographic features on the earth's surface are compensated at depth. The present investigation is concerned with the isostatic mechanism at Atlantic-type continental margins. Particular attention is given to the question whether the flexure model of isostasy, which has successfully been used at other geological features in oceans, is applicable at margins. Cross-spectral techniques are used to analyze the relationship between free air gravity and topography at Atlantic-type continental margins. The relatively old eastern North America is found to be associated with the highest value of the effective elastic thickness in the range 10-20 km, while the relatively young Coral Sea/Lord Howe rise is associated with the lowest value of less than 5 km. The differences in estimates of effective elastic thickness between margins can be explained by a simple model in which the flexural strength of the basement increases with age.

Karner, G. D.↗

NASA NTRS1982

Oxidation stability of advanced reaction-bonded Si3N4 materials

Four slip-cast, injection-molded and isostatically-pressed specimens of reaction-bonded silicon nitride (RBSN) were subjected to static oxidation tests at 900 C for 10 hours. Specimens containing 8-10% interconnected open porosity of size greater than one micron exhibited a 20-30% decrease in average room temperature four-point flexure strength, while those with 10% open porosity of magnitudes much smaller than one micron as well as those with 2-4% interconnected open porosity of about one micron did not decrease in strength after 900 C exposure. It was determined that preoxidation treatment at 1350 C prevents the 20-30% strength degradation due to internal oxidation, and evidence is presented which suggests that surface pit formation in some RBSN may result from contamination by the furnace environment rather than any intrinsic material properties.

Lindberg, L. J.↗

NASA NTRS1982

Progress in ceramic component fabrication technology

Net shape techniques have been used in the production of rotating and static vehicular engine high-temperature components composed of sintered Alpha-SiC (SASC). Injection-molded rotors have been cold spin tested, as well as a slip-cast combustor assembly hot rig. SASC pistons and cylinder liners have also been constructed for an opposed piston, two-cycle diesel test rig while test results are presented. An uncooled, minimum-friction internal combustion engine with multi-fuel capability due to its elevated combustion temperatures appears to be achievable in the near term by means of SASC techniques. The flexural strength of SASC at 1500 C is 446 MPa, identical to that at room temperature, and excellent strength retention has been demonstrated after 3500 hours of cyclic exposure.

Storm, R. S.↗

NASA NTRS1981

Development and demonstration of manufacturing processes for fabricating graphite/Larc-160 polyimide structural elements, part 4, paragraph B

Progress in the development of processes for production of Celion/LARC-160 graphite-polyimide materials, quality control, and the fabrication of Space Shuttle composite structure components is reported. Liquid chromatographic analyses of three repeatibility batches were performed and are compared to previous Hexcel standard production and to variables study LARC-160 intermediate resins. Development of processes for chopped fiber molding are described and flexural strength, elastic modulus, and other physical and mechanical properties of the molding are presented.

Source record↗

NASA NTRS1983

SEASAT observations of lithospheric flexure seaward of trenches

Lithospheric flexure seaward of deep ocean trenches in SEASAT altimeter observations of the marine geoid. In fact, mechanical models of lithospheric flexure can be tested directly on the SEASAT altimeter data. A simple elastic model was used for the oceanic lithosphere and, after least squares adjustments, estimates of model parameters were recovered including Outer Rise (OR) amplitude, OR wavelength, and effective lithospheric thickness. Effective lithospheric thickness was recovered for five regions: the Mariana, the Kuril, the Philippine, the Aleutian and the Middle America OR. These results support the suggestion of Bodine et al. (1981) that effective thickness, T, increased with age of lithosphere in approximate accord with the relation T approximately equals x age to the 1/2 power where C approximately equals 4 km x my to the -1/2 power. Altimetric results agree more closely with this relation than do published results based on bathymetric data. The close agreement with the thickness-age relation suggests that there is no longer any need to assume that significant horizontal compression acts across the Kuril, Marianas and Izo-Bonin trenches. This thickness-age relation implies that flexural strength of the oceanic lithosphere is temperature controlled.

Mcadoo, D. C.↗

NASA NTRS1982

Environmental effects on graphite fiber reinforced PMR-15 polyimide

Serafini, T. T.↗

NASA NTRS1983

Cobalt ion-containing epoxies

Varying concentrations of an organometallic cobalt complex were added to an epoxy system currently used by the aerospace industry as a composite matrix resin. Methods for combining cobalt (III) acetylacetonate with a tetraglycidyl 4,4 prime - diaminodiphenylmethane-based epoxy were investigated. The effects of increasing cobalt ion concentration on the epoxy cure were demonstrated by epoxy gel times and differential scanning calorimetry cure exotherms. Analysis on cured cobalt-containing epoxy castings included determination of glass transition temperatures by thermomechanical analysis, thermooxidative stabilities by thermogravimetric analysis, and densities in a density gradient column. Flexural strength and stiffness were also measured on the neat resin castings.

Stoakley, D. M.↗

NASA NTRS1983

Polyfunctional epoxies - Different molecular weights of brominated polymeric additives as flame retardants in graphite composites

The imparting of flame retardancy to graphite-reinforced composites without incurring mechanical property deterioration is investigated for the case of an experimental, trifunctional epoxy resin incorporating brominated polymeric additives (BPAs) of the diglycidyl type. Such mechanical properties as flexural strength and modulus, and short beam shear strength, were measured in dry and in hot/wet conditions, and the glass transition temperature, flammability, and water absorption were measured and compared with nonbromilated systems. Another comparison was made with a tetrafunctional epoxy system. The results obtained are explained in terms of differences in the polymeric backbone length of the bromine carrier polymer. BPAs are found to be a reliable bromine source for fire inhibition in carbon-reinforced composites without compromise of mechanical properties.

Nir, Z.↗

NASA NTRS1984

Seasat observations of lithospheric flexure seaward of trenches

Lithospheric flexure seaward of deep ocean trenches is evident in Seasat altimeter observations of the marine geoid. In fact, mechanical models of lithospheric flexure can be tested directly on the Seasat altimeter data. A simple elastic model has been used for the oceanic lithosphere and, after least squares adjustments, estimates have been recovered of model parameters including outer rise (OR) amplitude, OR wavelength, and effective lithospheric thickness. Effective lithospheric thicknesses have been recovered for six regions: the Mariana, the Kuril, the Philippine, the Aleutian, the Izu-Bonin, and the Middle America OR's. These results support the proposition that effective thickness Te increases with age of lithosphere in approximate accord with the relation Te approximately C x square root of age where C approximately 4 km/square root of (m.y.). In fact, altimetric results agree more closely with this relation than do published results based on bathymetric data. The close agreement with the thickness-age relation suggests that there is no longer any need to assume that significant horizontal compression acts across the Kuril, Marianas, and Izu-Bonin trenches. This thickness-age relation implies that flexural strength of the oceanic lithosphere is temperature controlled.

Mcadoo, D. C.↗

NASA NTRS1983

Development of new and improved polymer matrix resin systems, phase 1

Vinystilbazole (vinylstryrylpyridine) and vinylpolystyrulpyridine were prepared for the purpose of modifying bismaleimide composite resins. Cure studies of resins systems were investigated by differential scanning calorimetry. The vinylstyrylpyridine-modified bismaleimide composite resins were found to have lower cure and gel temperatures, and shorter cure times than the corresponding unmodified composite resins. The resin systems were reinforced with commercially avialable satin-weave carbon cloth. Prepregs were fabricated by solvent or hot melt techniques. Thermal stability, flammability, moisture absorption, and mechanical properties of the composites (such as flexural strength, modulus, tensile and short beam shear strength) were determined. Composite laminates showed substantial improvements in both processability and mechanical properties compared to he bismaleimide control systems. The vinylstyrylpyridine modified bismaleimide resins can be used as advanced matrix resins for graphite secondary structures where ease of processing, fireworthiness, and high temperature stability are required for aerospace applications.

Hsu, M. S.↗