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DOE OSTI2025

Design of an Out-Of-Pile Experimental Facility to Demonstrate the Feasibility of In Situ Thermal Conductivity Measurements of Nuclear Fuels Under Irradiation

There is substantial merit in quantifying nuclear fuel performance under irradiation. At Oak Ridge National Laboratory (ORNL), the MiniFuel irradiation platform has become the primary test vehicle for conducting separate-effects fuel performance irradiation experiments. The MiniFuel experiment is a passively controlled capsule design deployed in the High Flux Isotope Reactor (HFIR) through which fuel performance data is collected post-irradiation. Separate effects fuels irradiation capabilities are being expanded at ORNL by developing instrumented capsule designs that aim to capture fuel performance phenomena in-situ. One such capsule will specifically target fuel specimen thermal conductivity changes as a function of fuel burnup. Due to the complexity of making this measurement on nuclear fuel in-pile, this paper describes the necessary out-of-pile testing conducted on the thermal conductivity capsule (TCC) design. The measurement is ascertained via a thermopile system with heat transferred unidirectionally through a surrogate fuel specimen sandwiched between two conductive materials. The capsules investigated in this study are representative of the in-pile design, with the primary departure from irradiation conditions being the distribution of heat generation within the capsule. In the out-of-pile experiment, an external heater was used to drive heat through the conductive slug materials and into the specimen. This paper expounds the design of the out-of-pile experimental system and the thermal conductivity measurement technique. Predictive models used to determine the sensitivity of the measurement to variables governing thermal contact conductance between the specimen and slug materials and to predict experimental results are also described. Data from the out-of-pile experiment will be used to validate the readiness of the design for insertion into HFIR for irradiation.

Parker, Trevor [ORNL]↗

DOE OSTI2024

Accelerated Irradiation and Qualification of Ceramic Nuclear Fuels

Accelerated irradiation efforts are an important topic in accelerated qualification of new nuclear fuel concepts for light water reactor (LWRs), microreactors, and other special purpose reactors. Accelerated fuel qualification combines both experimental and modeling work to expedite the total qualification time from approximately 20-25 years to 5-10 years timeframe. The scope covered under the current work package focuses on the experimental contributions for the neutron irradiations. Accelerated irradiation aims to reduce the total time needed for neutron irradiation to achieve targeted burnup, which is timely using conventional irradiation profiles. The purpose of this report is to detail the samples preparation for such irradiations, which contain standard, medium, and large grain undoped UO 2 , as well as large grain, Cr 2 O 3 -doped UO 2 . The data that will be generated from the irradiation of these samples will yield important information regarding fission gas retention as a function of grain size and the effect that Cr dopants have on diffusivity of fission gases.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

DOE OSTI2024

Final Report on Characterization of Irradiated Sensors and Coupling Adhesive Bonds

This report summarizes characterization via scanning/transmission electron microscopy of the microstructures of the unirradiated and irradiated piezoelectric ultrasonic sensor/aluminum substrate assemblies using four commercially available inorganic coupling adhesives to bond two types of piezoelectric crystals to the substrates. The sample assemblies were irradiated in the PULSTAR reactor at NC State University and ultrasonic data was collected in-situ. ORNL LAMDA Laboratory capabilities were utilized to perform pre- and post-irradiation examination of the sensor assemblies. This document summarizes the PIE performed at the ORNL LAMDA laboratory. The results of the PIE described in this report are consistent with the ultrasonic data collected during irradiation – in particular, high temperature epoxy adhesive seemed to provide the best coupling as compared to the refractory ceramic adhesives. It was determined that the quality of the sensor-adhesive-substrates governed the ultrasonic performance of the sensors. It was also apparent that irradiation did not significantly affect bond quality, which is also supported by the ultrasonic data collected during irradiation. A more comprehensive DOE NSUF Final Report including details of materials selection, sample fabrication, initial ultrasonic testing, irradiation and in-situ ultrasonic testing, positron annihilation lifetime spectroscopy and doppler broadening spectroscopy performed at EPRI and NC State University will be published at the conclusion of the project.

36 MATERIALS SCIENCE↗

DOE OSTI2024

ROADRUNNER MiniFuel Experiment: Irradiation Target Design and Sample Characterization

High-density uranium nitride (UN) is a fuel candidate for several advanced nuclear reactor designs currently under development. Because there are limited UN performance data relative to fuel fabrication impurity and density variation, an irradiation campaign has been developed as part of a collaborative effort among the University of Texas at San Antonio (UTSA), Westinghouse Electric Company, Oak Ridge National Laboratory (ORNL), and Los Alamos National Laboratory (LANL) under the Nuclear Science User Facilities program. This project, entitled ROADRUNNER, or Research On ADvancing the peRformance of UraNium Nitrides in Extreme enviRonments, aimsto support UN fuel qualification for advanced reactors by investigating the impact of density and impurity variations on UN performance as a function of irradiation temperature and burnup. The MiniFuel experiment vehicle developed by ORNL, which leverages the High Flux Isotope Reactor, was selected to perform this accelerated separate-effects irradiation testing. The experiment test matrix consists of six MiniFuel targets containing miniature UN fuel disks, and targets three distinct burnup levels (37.5, 60, and 75 MWd/kg U) and three distinct temperatures (600, 900, and 1200°C). Neutronics and thermal analyses were performed to determine the experimental parameters needed to meet the desired irradiation conditions and to predict the experiment components temperatures. UN pellets were fabricated at LANL with tightly controlled parameters to produce specimens with three distinct densities and three levels of carbon content. The pellets were then thinned down by UTSA to the experiment-required thickness. The pre-characterization of the specimens includes density measurements, carbon and oxygen contents, microstructure analysis, and x-ray computed tomography. The selected specimens will be assembled into the MiniFuel experiment, and the first ROADRUNNER MiniFuel targets are intended for HFIR insertion during the Fall of 2024. After irradiation, the targets will be shipped to ORNL’s hot cell facility for disassembly. The post-irradiation examination on the fuel specimens includes fission gas release measurements, visual inspection, fuel swelling measurements, gamma spectroscopy, and microstructure analysis. The data collected post-irradiation will be used to develop fuel performance models.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

DOE OSTI2025

Ion irradiation testing of 14YWT ODS and HT-9

Ion irradiations were performed to compare a new generation of 14YWT, NFA-2, to the prior generation NFA-1. Irradiations were performed at 450 °C and to a peak dose of 500 dpa. The irradiation condition was chosen as a relevant temperature for scoping for an upcoming JOYO neutron irradiation, and the high dose was chosen to evaluate the exceptional microstructural stability to irradiation induced changes of 14YWT. For comparison, HT-9 was irradiated as the benchmark. Irradiation induced changes to the microstructures were limited for the 14YWT samples and extensive for the HT-9 benchmark.

36 MATERIALS SCIENCE↗

DOE OSTI2026

AMMT Round Robin 316H HFIR Irradiation Test Matrix and Readiness for Insertion

The Round Robin 316H HFIR-2 irradiation campaign, conducted under the Advanced Materials and Manufacturing Technologies (AMMT) Program, is designed to evaluate the variability in irradiation response of laser powder bed fusion (LPBF) stainless steel (SS)-316H across multiple national laboratories, powder heats, and processing conditions, with comparison to wrought counterparts. A total of 11 materials are intended for irradiation in the High Flux Isotope Reactor (HFIR), targeting two irradiation temperatures (400°C and 600°C) and one level of irradiation damage (2 dpa). This irradiation campaign utilizes the standardized general tensile (GENTEN) capsule design to accommodate subsized tensile specimens of these materials. Thermal analyses were performed to ensure appropriate temperature control by design and uniformity within the capsules. All the capsules for this irradiation except one have been successfully assembled, welded, and tested and are ready for HFIR insertion. The last capsule requires re-build following a failed weld. All eight capsules are intended to be inserted in HFIR cycle 517, which is scheduled to start September 8, 2026. This report summarizes the design, material selection, and readiness for insertion of the capsules.

36 MATERIALS SCIENCE↗

DOE OSTI2026

High-Temperature SiC Cladding End Plug Irradiation Design and HFIR Readiness

This report documents the design of a High Flux Isotope Reactor (HFIR) irradiation experiment intended to evaluate irradiation effects on the hermeticity of silicon carbide (SiC) end plug specimens under a radial fast neutron flux gradient at representative light-water reactor (LWR) temperatures of approximately 300 °C. The overarching goal of this work is to statistically evaluate SiC end plug hermeticity and mechanical properties following irradiation using the high-throughput irradiation capability discussed here. Each specimen consists of a short section of SiC fiber–reinforced SiC (SiC/SiC) tube with a single monolithic SiC end plug joined to one end. The experiment allows up to 66 specimens to be irradiated in six different stacks within a dry, sealed irradiation capsule derived from the previously developed high-temperature SiC/SiC cladding bowing experiment. The neutronics basis, thermal analysis, and HFIR readiness of the experiment are discussed in this report for two possible design cases. The first design case is based on existing approval documentation and components that are on hand and approved for use, so the experiment insertion would require only specimen receipt, specimen pre-irradiation characterization, experiment assembly, and final fabrication package approval. The second design case provides improved thermal robustness and the preferred end plug geometry but requires fabrication of a modified holder and revisions to the HFIR approval documentation, in addition to the other activities required for the first design case, before insertion.

Hott, Daniel [Oak Ridge National Laboratory (ORNL)↗

NASA NTRS1978

Solar spectral irradiance at ground level

Available quantitative data on solar total and spectral irradiance is examined in the context of utilization of solar irradiance for terrestrial applications of solar energy. A brief review is given on the extraterrestrial solar total and spectral irradiance values. Computed values of solar spectral irradiance at ground level for different air mass values and various levels of atmospheric pollution or turbidity are also presented. Wavelengths are given for computation of solar absorptance, transmittance and reflectance by the 100-selected-ordinate method and by the 50-selected-ordinate method from air mass two solar spectral irradiance for the four degrees of atmospheric pollution. Total solar spectral irradiance measured with a prism monochromator is examined to evaluate the direct solar spectral irradiance for a surface normal to the sun's rays and to compare the computed spectrum with the experimentally observed one.

Mecherikunnel, A. T.↗

NASA NTRS1982

Solar irradiance variations and solar activity

A mean value for the 1 AU total solar irradiance of 1368.2 W/sq m and a downward trend of 0.05% per year were derived from measurements by the Active Cavity Radiometer Irradiance Monitor (ACRIM) experiment on the Solar Maximum Mission during 1980. Distinct temporary solar irradiance decreases associated with solar activity maxima were observed with a series of nine dips from April to October recurring at fairly regular intervals averaging 24 days. The decreases correlate inversely with sunspot area, 2800-MHz flux, and Zurich sunspot number. Dominant periods common to the irradiance and sunspot area power spectra link the irradiance decreases to sunspot flux deficit in solar active regions. Evidence of significant total irradiance modulation by facular flux excess is cited. A persistent radiative cycle of active regions consistent with the ACRIM irradiance results and the morphology of solar active regions was found. The pattern of regularly recurrent active region maxima between April and October suggests an asymmetry in solar activity generation during this period.

Willson, R. C.↗

NASA NTRS1987

The calculated influence of atmospheric conditions on solar cell ISC under direct and global solar irradiances

Calculations of the influence of atmospheric conditions on solar cell short-circuit current (Isc) are made using a recently developed computer model for solar spectral irradiance distribution. The results isolate the dependence of Isc on changes in the spectral irradiance distribution without the direct influence of the total irradiance level. The calculated direct normal irradiance and percent diffuse irradiance are given as a reference to indicate the expected irradiance levels. This method can be applied to the calibration of photovoltaic reference cells. Graphic examples are provided for amorphous silicon and monocrystalline silicon solar cells under direct normal and global normal solar irradiances.

Mueller, Robert L.↗

NASA NTRS1992

Variations in solar Lyman alpha irradiance on short time scales

Variations in solar UV irradiance at Lyman alpha are studied on short time scales (from days to months) after removing the long-term changes over the solar cycle. The SME/Lyman alpha irradiance is estimated from various solar indices using linear regression analysis. In order to study the nonlinear effects, Lyman alpha irradiance is modeled with a 5th-degree polynomial as well. It is shown that the full-disk equivalent width of the He line at 1083 nm, which is used as a proxy for the plages and active network, can best reproduce the changes observed in Lyman alpha. Approximately 72 percent of the solar-activity-related changes in Lyman alpha irradiance arise from plages and the network. The network contribution is estimated by the correlation analysis to be about 19 percent. It is shown that significant variability remains in Lyman alpha irradiance, with periods around 300, 27, and 13.5d, which is not explained by the solar activity indices. It is shown that the nonlinear effects cannot account for a significant part of the unexplained variation in Lyman alpha irradiance. Therefore, additional events (e.g., large-scale motions and/or a systematic difference in the area and intensity of the plages and network observed in the lines of Ca-K, He 1083, and Lyman alpha) may explain the discrepancies found between the observed and estimated irradiance values.

Pap, J. M.↗

NASA NTRS1994

Observed solar UV irradiance variations of importance to middle atmosphere energetics and photochemistry

Absorption of solar UV irradiance in the spectral interval 120-420 nm is chiefly responsible for radiative heating and photodissociation of important atmospheric constituents (e.g., O2, O3, H2O, NO2, etc.) in the stratosphere, mesosphere, and lower thermosphere. Thus, the absolute value and time perturbations of the UV irradiance could significantly affect the energetics, photochemistry, and subsequent dynamics of these regions. Analysis of preliminary data from the SOLSTICE (UARS) observations for a period of 244 days (3 Oct 1991-2 Jun 1992) is discussed in this paper. The data provide mean daily values of the spectral distribution of the observed irradiances at 1-nm resolution and their solar rotation and semirotation variations. The average amplitudes of the 27-day irradiance oscillations for the 244-day data period were 5.7% at Lyman-alpha (121 nm), 1% at 200 nm, 0.5% at 210 nm, and generally less than 0.2% at wavelengths longer than 280 nm. The average amplitudes of 13.5-day oscillations were, by and large, about half of these values. Solar irradiance variations at 10.7 cm are highly correlated with those at Ly-alpha and other chromospheric emission lines (r = 0.7 to 0.8) and only moderately correlated with irradiances at wavelengths of 180-208 nm (r = 0.5). The correlation decreases as the source region of the irradiance gets closer to the base of the photosphere. At the 2-nm interval 279-281 nm, however, which contains the cores of the Mg II h and k lines, the correlation is again approximately 0.8.

London, Julius↗

NASA NTRS1995

Response of the upper atmosphere to variations in the solar soft x-ray irradiance

Terrestrial far ultraviolet (FUV) airglow emissions have been suggested as a means for remote sensing the structure of the upper atmosphere. The energy which leads to the excitation of FUV airglow emissions is solar irradiance at extreme ultraviolet (EUV) and soft x-ray wavelengths. Solar irradiance at these wavelengths is known to be highly variable; studies of nitric oxide (NO) in the lower thermosphere have suggested a variability of more than an order of magnitude in the solar soft x-ray irradiance. To properly interpret the FUV airflow, the magnitude of the solar energy deposition must be known. Previous analyses have used the electron impact excited Lyman-Birge-Hopfield (LBH) bands of N2 to infer the flux of photoelectrons in the atmosphere and thus to infer the magnitude of the solar irradiance. This dissertation presents the first simultaneous measurements of the FUV airglow, the major atmospheric constituent densities, and the solar EUV and soft x-ray irradiances. The measurements were made on three flights of an identical sounding rocket payload at different levels of solar activity. The linear response in brightness of the LBH bands to variations in solar irradiance is demonstrated. In addition to the N2 LBH bands, atomic oxygen lines at 135.6 and 130.4 nm are also studied. Unlike the LBH bands, these emissions undergo radiative transfer effects in the atmosphere. The OI emission at 135.6 nm is found to be well modeled using a radiative transfer calculation and the known excitation processes. Unfortunately, the assumed processes leading to OI 130.4 nm excitation are found to be insufficient to reproduce the observed variability of this emission. Production of NO in the atmosphere is examined; it is shown that a lower than previously reported variability in the solar soft x-ray irradiance is required to explain the variability of NO.

Bailey, Scott Martin↗

NASA NTRS1999

Global Mapping of Underwater UV Irradiances and DNA-Weighted Exposures using TOMS and SeaWiFS Data Products

The global stratospheric ozone-layer depletion results In an increase in biologically harmful ultraviolet (UV) radiation reaching the surface and penetrating to ecologically significant depths in natural waters. Such an increase can be estimated on a global scale by combining satellite estimates of UV irradiance at the ocean surface from the Total Ozone Mapping Spectrometer (TOMS) satellite instrument with the SeaWIFS satellite ocean-color measurements in the visible spectral region. In this paper we propose a model of seawater optical properties in the UV spectral region based on the Case I water model in the visible range. The inputs to the model are standard monthly SeaWiFS products: chlorophyll concentration and the diffuse attenuation coefficient at 490nm. Penetration of solar UV radiation to different depths in open ocean waters is calculated using the RT (radiative transfer) quasi-single scattering approximation (QSSA). The accuracy of the QSSA approximation in the water is tested using more accurate codes. The sensitivity study of the underwater UV irradiance to atmospheric and oceanic optical properties have shown that the main environmental parameters controlling the absolute levels of the UVB (280-320nm) and DNA-weighted irradiance underwater are: solar-zenith angle, cloud transmittance, water optical properties, and total ozone. Weekly maps of underwater UV irradiance and DNA-weighted exposure are calculated using monthly-mean SeaWiFS chlorophyll and diffuse attenuation coefficient products, daily SeaWiFS cloud fraction data, and the TOMS-derived surface UV irradiance daily maps. The final products include global maps of weekly-average UVB irradiance and DNA-weighted daily exposures at 3m and 10m, and depths where the UVB irradiance and DNA-weighted dose rate at local noon are equal to 10% of their surface values.

Vasilkov, Alexander↗

NASA NTRS2003

Future Satellite Observations of Solar Irradiance

Required solar irradiance measurements for climate studies include those now being made by the Total Irradiance Monitor (TIM) and the Spectral Irradiance Monitor (SIM) onboard the SORCE satellite, part of the Earth Observing System fleet of NASA satellites. Equivalent or better measures of Total Solar Irradiance (TSI) and Spectral Solar Irradiance (SSI, 200 to 2000 nm) are planned for the post-2010 satellites of the National Polar-orbiting Operational Environmental Satellite System ("OESS). The design life of SORCE is 5 years, so a "Solar Irradiance Gap Filler" EOS mission is being planned for launch in the 2007 time frame, to include the same TSI and SSI measurements. Besides avoiding any gap, overlap of the data sources is also necessary for determination of possible multi-decadal trends in solar irradiance. We discuss these requirements and the impacts of data gaps, and data overlaps, that may occur in the monitoring of the critical solar radiative forcing.

Cahalan, R. F.↗

NASA NTRS2012

Late Effects of Heavy Ion Irradiation on Ex Vivo Osteoblastogenesis and Cancellous Bone Microarchitecture

Prolonged spaceflight causes degeneration of skeletal tissue with incomplete recovery even after return to Earth. We hypothesize that heavy ion irradiation, a component of Galactic Cosmic Radiation, damages osteoblast progenitors and may contribute to bone loss during long duration space travel beyond the protection of the Earth's magnetosphere. Male, 16 week old C57BL6/J mice were exposed to high LET (56 Fe, 600MeV) radiation using either low (5 or 10cGy) or high (50 or 200cGy) doses at the NASA Space Radiation Lab and were euthanized 3 - 4, 7, or 35 days later. Bone structure was quantified by microcomputed tomography (6.8 micron pixel size) and marrow cell redox assessed using membrane permeable, free radical sensitive fluorogenic dyes. To assess osteoblastogenesis, adherent marrow cells were cultured ex vivo, then mineralized nodule formation quantified by imaging and gene expression analyzed by RT PCR. Interestingly, 3 - 4 days post exposure, fluorogenic dyes that reflect cytoplasmic generation of reactive nitrogen/oxygen species (DAF FM Diacetate or CM H2DCFDA) revealed irradiation (50cGy) reduced free radical generation (20-45%) compared to sham irradiated controls. Alternatively, use of a dye showing relative specificity for mitochondrial superoxide generation (MitoSOX) revealed an 88% increase compared to controls. One week after exposure, reactive oxygen/nitrogen levels remained lower(24%) relative to sham irradiated controls. After one month, high dose irradiation (200 cGy) caused an 86% decrement in ex vivo nodule formation and a 16-31% decrement in bone volume to total volume and trabecular number (50, 200cGy) compared to controls. High dose irradiation (200cGy) up regulated expression of a late osteoblast marker (BGLAP) and select genes related to oxidative metabolism (Catalase) and DNA damage repair (Gadd45). In contrast, lower doses (5, 10cGy) did not affect bone structure or ex vivo nodule formation, but did down regulate iNOS by 0.54 - 0.58 fold. Thus, both low and high doses of heavy ion irradiation cause time dependent, adaptive changes in redox state within marrow cells but only high doses (50, 200cGy) inhibit osteoblastogenesis and cause cancellous bone loss. We conclude space radiation has the potential to cause persistent damage to bone marrow derived stem and progenitor cells for osteoblasts despite adaptive changes in cellular redox state.

Tran, Luan Hoang↗

NASA NTRS2019

Estimating Residual Uncertainties for Lunar Irradiance Measurements Due to Imaging Acquisition Parameters

Lunar calibration is a commonly used method to track a climate satellite sensor's long-term radiometric stability. We present a modeling approach to examine the satellite sensor lunar observation uncertainties due to several important aspects related to the lunar image acquisition by the satellite sensor: lunar pixel shift, point spread function (PSF), lunar orientation, pitch, and oversampling rates. Our analyses can be summarized as follows: (1) The sensor observed lunar irradiance can vary due to small lunar pixel shift if the PSF is less than ideal; (2) During lunar calibration, an unstable oversampling rate due to spacecraft control will result in errors in observed lunar irradiance. A drift in oversampling rate would result in a bias in observed lunar irradiance and a random variation in oversampling rate would cause random error in lunar irradiance. Increasing the overall oversampling rates can reduce random error in observed lunar irradiance but would not change the biases in the observation; (3) Furthermore, the biases can vary when the Moon is observed at different orientations. Our results show impacts on observed lunar irradiance are on the order of 0.1 percent, which is a significant part of the overall uncertainty for a lunar irradiance measurement of a climate satellite sensor.

Oversampling↗

NASA NTRS2020

Examining Biases in Diurnally-Integrated Shortwave Irradiances due to Two- and Four-Stream Approximations in Cloudy Atmosphere

Shortwave irradiance biases due to two- and four-stream approximations have been studied for the last couple of decades, but biases in estimating Earth’s radiation budget have not been examined in earlier studies. In order to quantify biases in diurnally-averaged irradiances, we integrate the two- and four-stream biases using realistic diurnal variations of cloud properties from Clouds and the Earth’s Radiant Energy System (CERES) synoptic (SYN) hourly product. Three approximations are examined in this study, delta-two-stream-Eddington (D2strEdd), delta- two-stream-quadrature (D2strQuad), and delta-four-stream-quadrature (D4strQuad). Irradiances computed by the Discrete Ordinates Radiative Transfer (DISORT) and Monte Carlo (MC) methods are used as references. The MC noises are further examined by comparing with DISORT results. When the biases are integrated with a one-day of solar zenith angle variation, regional biases of D2strEdd and D2strQuad reach up to 8 W/sq.m, while biases of D4strQuad reach up to 2 W/sq.m. When the biases are further averaged monthly or annually, regional biases of D2strEdd and D2strQuad can reach –1.5 W/sq.m in SW top-of-atmosphere (TOA) upward irradiances and +3 W/sq.m in surface downward irradiances. In contrast, regional biases of D4strQuad are within +0.9 for TOA irradiances and –1.2 W/sq.m for surface irradiances. Except for polar regions, monthly and annual global mean biases are similar, suggesting that the biases are nearly independent to season. Biases in SW heating rate profiles are up to –0.008 K/d for D2strEdd and –0.016 K/d for D2strQuad, while the biases of the D4strQuad method are negligible.

Ham, Seung-Hee↗