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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 145 records · Page 8

Importance of Sample Handling and Preparation for Surface Analysis: A Summary of ISO Standard 20579 Part 1, Documenting and Reporting the Handling of Specimens Prior to Analysis

Reliable and reproducible analysis of surfaces is critically dependent on how samples have been collected, handled, and prepared before analysis. Although there are important, well-established general guidelines to minimize unintended alteration of the surfaces to be analyzed, specific handling steps depend on the nature of the samples and information desired. Assessments of the validity and reliability of the results require adequate information about sampling, handling, and processing. ISO standard 20579 part 1 describes the information to be recorded and reported for samples that are prepared or submitted for surface analysis. This paper summarizes elements of the standard, which includes annexes that justify and inform the sample handling processes. Also included is a checklist of information that needs to be recorded and reported and an appendix containing an example of a form that might be used to report the information.

AES↗

Autoignition study of binary blends of n- dodecane/1-methylnaphthalene and iso- cetane/1-methylnaphthalene

An experimental study on autoignition of two binary blends, n-dodecane/1-methylnaphthalene and iso-cetane/1-methylnaphthalene, has been conducted using a rapid compression machine. Specifically, the ignition delays of the stoichiometric blend+air mixtures were measured at elevated pressures of P C = 15 bar and 30 bar, compressed temperatures of T C = 626–944 K, and varying blending ratios of the constituents. For a given set of P C and T C , a nonlinear response of the blend reactivity with respect to the relative amount of the constituents was observed. Since a comprehensive chemical kinetic model for the blends investigated here is under development, the current ignition delay datasets serve as the needed targets for model validation. For selected conditions, ignition delay simulations were conducted to highlight and discuss the deficiencies of the literature models and the potential areas for model improvements, especially at low temperatures. In conclusion, further chemical kinetic analyses were conducted to gain understanding of the blending behavior predicted by the available model.

1-methylnaphthalene↗

Effect of nitric oxide and exhaust gases on gasoline surrogate autoignition: iso-octane experiments and modeling

Exhaust gas recirculation (EGR) is widely used in advanced internal combustion engines to reduce engine emissions as well as control combustion phasing. Among various species present in EGR gases, CO 2 and H 2 O are two major components that can thermally and chemically affect fuel autoignition. It is of fundamental interest to isolate the thermal and chemical effects of CO 2 and H 2 O on fuel autoignition, especially as such an effort has not been reported in the literature. Moreover, nitric oxide (NO) is known to exhibit strong chemical effects on fuel autoignition, which in turn affects engine combustion phasing. The effects of ultra-low NO addition (< 100 ppm) on fuel autoignition at low temperatures are also not well understood. Recognizing these problems, autoignition experiments of iso-octane (a major gasoline surrogate component) in air are performed in this study using a rapid compression machine at varying compressed pressures, equivalence ratios, dilution levels with an EGR gas analogue (consisting of CO 2 , H 2 O, O 2 , and N 2 ) and N 2 only, and varying amounts of NO addition. Furthermore, the thermal and chemical effects of the EGR gas analogue are isolated and evaluated by comparing the ignition delay time datasets of EGR and N2-only diluted cases.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

Consensus statement for stability assessment and reporting for perovskite photovoltaics based on ISOS procedures

Improving the long-term stability of perovskite solar cells is critical to the deployment of this technology. Despite the great emphasis laid on stability-related investigations, publications lack consistency in experimental procedures and parameters reported. It is therefore challenging to reproduce and compare results and thereby develop a deep understanding of degradation mechanisms. Here, we report a consensus between researchers in the field on procedures for testing perovskite solar cell stability, which are based on the International Summit on Organic Photovoltaic Stability (ISOS) protocols. We propose additional procedures to account for properties specific to PSCs such as ion redistribution under electric fields, reversible degradation and to distinguish ambient-induced degradation from other stress factors. These protocols are not intended as a replacement of the existing qualification standards, but rather they aim to unify the stability assessment and to understand failure modes. Finally, we identify key procedural information which we suggest reporting in publications to improve reproducibility and enable large data set analysis.

14 SOLAR ENERGY↗

New requirements for digital radiographic testing of welds according to ISO standards

Users of EN 14784-2 (general principles for computed radiography with phosphor imaging plates) reported about difficulties to achieve testing class B in weld testing with imaging plates. One of the reasons is the insufficient consideration of the inherent detector unsharpness (u{sub i}) in the minimum requirements. Digital detectors have a higher inherent unsharpness compared to film, which can even exceed the geometrical unsharpness (u{sub g}) of the typical contact technique. In EN 444 and ISO 5579 (general principles for film radiography) u{sub i} is neglected for the calculation of the minimum source-to-object distance (SOD), because it is small compared to the geometric unsharpness (u{sub g}). Considering u{sub i} for digital detectors results in a new equation for SOD (see ISO/FDIS 17636-2). Therefore, the increase in total image unsharpness requires the compensation by a larger SOD to reduce u{sub g}. This contribution discusses the need for change of the SOD for different setups (detectors, focal spots, etc.) and explains the difference in image quality, achieved on basis of the extended equation of ISO/FDIS 17636-2. Furthermore, the detection of image quality indicators depends on the achieved Contrast-to-Noise ratio (CNR) and total image unsharpness. Both of them are essential parameters, which influence the contrast sensitivity. Additionally, new compensation principles (e.g. compensation of missing spatial resolution by enhanced contrast sensitivity) allow to widen the application range of digital detectors for radiographic weld testing.

42 ENGINEERING↗

A high-resolution single-molecule sequencing-based Arabidopsis transcriptome using novel methods of Iso-seq analysis

Accurate and comprehensive annotation of transcript sequences is essential for transcript quantification and differential gene and transcript expression analysis. Single-molecule long-read sequencing technologies provide improved integrity of transcript structures including alternative splicing, and transcription start and polyadenylation sites. However, accuracy is significantly affected by sequencing errors, mRNA degradation, or incomplete cDNA synthesis. We present a new and comprehensive Arabidopsis thaliana Reference Transcript Dataset 3 (AtRTD3). AtRTD3 contains over 169,000 transcripts—twice that of the best current Arabidopsis transcriptome and including over 1500 novel genes. Seventy-eight percent of transcripts are from Iso-seq with accurately defined splice junctions and transcription start and end sites. We develop novel methods to determine splice junctions and transcription start and end sites accurately. Mismatch profiles around splice junctions provide a powerful feature to distinguish correct splice junctions and remove false splice junctions. Stratified approaches identify high-confidence transcription start and end sites and remove fragmentary transcripts due to degradation. AtRTD3 is a major improvement over existing transcriptomes as demonstrated by analysis of an Arabidopsis cold response RNA-seq time-series. AtRTD3 provides higher resolution of transcript expression profiling and identifies cold-induced differential transcription start and polyadenylation site usage. AtRTD3 is the most comprehensive Arabidopsis transcriptome currently. It improves the precision of differential gene and transcript expression, differential alternative splicing, and transcription start/end site usage analysis from RNA-seq data. The novel methods for identifying accurate splice junctions and transcription start/end sites are widely applicable and will improve single-molecule sequencing analysis from any species.

transcription start and end sites↗

Comparison of ISO and ANSI/ANS Nuclear Criticality Safety Standards

This paper provides a high-level comparison between the international and domestic Nuclear Criticality Safety (NCS) standards, as requested by members of the Nuclear Criticality Safety Division. Currently, there are 18 enacted American National Standards Institute (ANSI)/American National Standards (ANS) and 1 ANSI/ANS standard in progress. There are 11 NCS standards from the International Organization for Standardization (ISO), Technical Committee 85 (TC85) on Nuclear Energy, Subcommittee 5 (SC5) on Nuclear Fuel Cycle, Working Group 8 (WG8). There are NCS standard revisions in progress for both standards organizations.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗

ISO 14001:2015 Environmental Management System Management Assessment Internal Review Assessing Organization: EPC-ES LANL-ASMT-2022-0289 (Spring 2023)

The Environmental Protection and Compliance Division-Environmental Stewardship Group of Los Alamos National Laboratory conducted a management assessment that supports the implementation of the Los Alamos National Laboratory Environmental Management System according to International Organization for Standardization (ISO) 14001:2015, Environmental Management System. The assessment resulted in zero findings of nonconformity, five opportunities for improvement, four noteworthy practices, and three observations.

54 ENVIRONMENTAL SCIENCES↗

The ISO-IRAS Faint Galaxy Survey: ISOCAM Results

The ISO-IRAS Faint Galaxy Survey (IIFGS) is a program designed to produce one of the largest and deepest samples of luminous galaxies possible with present facilities.

galaxies infrared ISO IRAS↗

ISO 191* Revisions and Amendments

ISO standards have changed recently in response to new requirements from introduced by NASA, NOAA, and other ESIP members. These changes address important uses cases related to identification, parameter metadata, and platform/instrument/sensor metadata. Each change will be described along with discussion of how they may be used.

data quality↗

Grid Enhancing Technologies in ISO-NE

Assess Grid Enhancing Technologies in transmission planning by coupling economic and reliability analysis over an entire time horizon rather than a few dispatch conditions for ISO-NE.

24 POWER TRANSMISSION AND DISTRIBUTION↗

Summary of ISO/TC 201 Standard: ISO 29081: 2010, Surface Chemical Analysis - Auger Electron Spectroscopy - Reporting of Methods Used for Charge Control and Charge Correction

This international standard specifies the minimum amount of information required for describing the methods of charge control in measurements of Auger electron transitions from insulating specimens by electron-stimulated Auger electron spectroscopy to be reported with the analytical results. Information is provided in an Annex on methods that have been found useful for charge control prior to or during AES analysis. The Annex also includes a summary table of methods or approaches, ordered by simplicity of approach. A similar international standard has been published for x-ray photoelectron spectroscopy (ISO 19318: 2003(E), Surface chemical analysis - X-ray photoelectron spectroscopy - Reporting of methods used for charge control and charge correction).

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

Application of Surface Analysis Methods to Nanomaterials: Summaryof ISO/TC 201 Technical Report: ISO 14187:2011 -Surface Chemical Analysis- Characterization of Nanomaterials

ISO Technical Report (TR) 14187 provides an introduction to (and examples of) the information that can be obtained about nanostructured materials using surface-analysis tools. In addition, both general issues and challenges associated with characterising nanostructured materials and the specific opportunities and challenges associated with individual analytical methods are identified. As the size of objects or components of materials approaches a few nanometres, the distinctions among 'bulk', 'surface' and 'particle' analysis blur. This Technical Report focuses on issues specifically relevant to surface chemical analysis of nanostructured materials. The report considers a variety of analysis methods but focuses on techniques that are in the domain of ISO/TC 201 including Auger electron spectroscopy, X-ray photoelectron spectroscopy, secondary ion mass spectrometry, and scanning probe microscopy. Measurements of nanoparticle surface properties such as surface potential that are often made in a solution are not discussed.

36 MATERIALS SCIENCE↗

Importance of standard terminology in surface chemical analysis: ISO 18115-1:2023, general terms and terms used in spectroscopy

The International Standard ISO 18115-1 on terminology in surface chemical analysis has been revised with clarifications, modifications, and deletions to more than 70 terms and with the addition of more than 50 terms in response to trends, issues, and needs identified by the surface analysis community. This revision adds terminology and concepts associated with emerging methods such as atom probe tomography, near ambient pressure XPS, and hard X-ray photoelectron spectroscopy. It includes 25 new and revised terms to ensure that the description of resolution is consistent across all surface analysis methods. The 630 terms in the document cover words or phrases used in describing the samples, instruments, and concepts involved in surface chemical analysis. Here, the terms have been collated into subject specific sections to ensure that related terms can be found easily.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

New AdS4 vacua in dyonic ISO(7) gauged supergravity

We identify 219 AdS 4 solutions in four-dimensional dyonically gauged ISO(7) N = 8 supergravity and present some of their properties. One of the new solutions preserves N = 1 supersymmetry and provides a rare explicit example of an AdS 4 vacuum dual to a 3d SCFT with no continuous global symmetry. There are also two new non-supersymmetric solutions for which all 70 scalar fields in the supergravity theory have masses above the BF bound. All of these AdS 4 solutions can be uplifted to massive type IIA supergravity. Motivated by this we present the low lying operator spectra of the dual 3d CFTs for all known supersymmetric AdS 4 solutions in the theory and organize them into superconformal multiplets.

79 ASTRONOMY AND ASTROPHYSICS↗

Short-term administration of iso-α-acids increases transthyretin transcription in the hippocampus

Cognitive decline and dementia are currently recognized as major problems in the aging population; however, there is still no promising treatment for these conditions. Previously, our group reported that iso-α-acids (IAAs), which are hop-derived bitter components present in beer, prevent inflammation and cognitive impairment in an Alzheimer's disease model mice (5xFAD mice) and yield significant reduction in amyloid β (Αβ) in the brain. However, data on the molecular mechanisms underlying these physiological effects of IAAs remain limited. Here, we used transcriptome analysis and found that oral administration of IAAs to 5xFAD mice for 7 days induces a 58.9-fold increase in the expression of transthyretin (TTR; Ttr) in the hippocampus compared with controls. In addition, real-time quantitative PCR showed that oral administration of IAAs significantly increased Ttr transcription in the hippocampi of wild type C57BL/6J mice but not in the cerebral cortex. TTR is an Αβ protein scavenger; thus, an increase in its expression could prevent amyloid aggregate formation. These results indicate that IAAs reduce Αβ in the brain by elevating TTR levels.

60 APPLIED LIFE SCIENCES↗

LES of HCCI combustion of iso-octane/air in a flat-piston rapid compression machine

Homogeneous Charge Compression Ignition (HCCI) engines promise better efficiency and cleaner emissions than conventional piston engines, but can be challenging to control. Rapid compression machines (RCM) provide a simplified configuration for investigating HCCI combustion behavior, which is necessary for effective control of engine ignition timing and peak pressures. Here, in this study, we assess the utility of large eddy simulations (LES) for predicting HCCI combustion in a 3-D configuration. To this end, LES with finite-rate chemistry employing a 99-species iso-octane/air mechanism of two RCM operating conditions are performed. The RCM configuration under consideration was designed by Strozzi et al. with a flat piston to introduce large amounts of thermal stratification representative of realistic HCCI engine conditions, through the generation of corner vortices. It is shown that the simulation provides reasonable agreement with temperature fluctuations (7% difference), as well as ignition delay in the short ignition case (1 ms difference), while the long ignition case (35 ms difference) highlights more substantial deficiencies that are still within the expected uncertainty from the employed chemical mechanism. Flame propagation modes predicted by LES agree with experimental observations: spontaneous ignition is seen in the short ignition case, while deflagration is more prominent in the long ignition case. Analysis of global and local quantities classify the short ignition case in a mixed ignition regime, and the long ignition case in the mild ignition regime. These results demonstrate the utility of FRC-LES for investigations of multimode combustion regimes of HCCI combustion in a 3-D configuration.

33 ADVANCED PROPULSION SYSTEMS↗