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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 145 records · Page 8

Hermetic Seal Leak Detection Apparatus with Variable Size Test Chamber

The present invention is a versatile hermetic seal leak detection apparatus for testing hermetically sealed containers and devices for leaks without the need to create a custom or specially manufactured testing chamber conforming to the dimensions of the specific object under test. The size of the testing chamber may be mechanically adjusted by the novel use of bellows to reduce and optimize the amount of gas space in a test chamber which surrounds the hermetically sealed object under test. The present invention allows the size of the test chamber to be selectively adjusted during testing to provide an optimum test chamber gas space. The present invention may be further adapted to isolate and test specific portions of the hermetically sealed object under test for leaks.

Kelley, Anthony R.↗

International Space Station (ISS) Environmental Control and Life Support System (ECLSS) Vent Flow Reflection and Detection by Robotic External Leak Locator (RELL)

On-orbit Robotic External Leak Locator (RELL) (i.e., mass spectrometer and ion gauge) measurements on the International Space Station (ISS) are presented to show the detection of recurring Environmental Control and Life Support System (ECLSS) vents at multiple ISS locations and RELL pointing directions. The path of ECLSS effluents to the RELL detectors is not entirely obvious at some locations, but the data indicates that diffuse gas-surface reflection or scattering resulting from plume interaction with vehicle surfaces is responsible. RELL was also able to confirm the ISS ECLSS constituents and distinguish them from the ammonia leak based on the ion mass spectra and known venting times during its operation to locate a leak in the ISS port-side External Active Thermal Control System (EATCS) coolant loop.

Gas/Surface Reflections or Scattering↗

Natural and Induced Environment around the International Space Station (ISS) as Observed during On-Orbit Operations of the Robotic External Leak Locator (RELL)

Final Document is attached. The Robotic External Leak Locator (RELL) was deployed to the International Space Station (ISS) with the goal of detecting and locating on-orbit leaks around the ISS. Three activities to investigate and corroborate the background natural and induced environment of ISS were performed with RELL as part of the on-orbit validation and demonstration conducted in November – December 2016. The first demonstration activity pointed RELL directly in the ram and wake directions for one orbit each. The ram facing measurements showed high partial pressure for mass-to-charge ratio 16, corresponding to atomic oxygen (AO), as well as the presence of mass-to-charge ratio 17. RELL™s view in the wake-facing direction included more ISS structure and several Environmental Control and Life Support System (ECLSS) on-orbit vents were detected, including the Carbon Dioxide Removal Assembly (CDRA), Russian segment ECLSS, and Sabatier vents. The second demonstration activity pointed RELL at three faces of the P1 Truss segment. Effluents from ECLSS and European Space Agency (ESA) Columbus module on-orbit vents were detected by RELL. The partial pressures of mass-to-charge ratios 17 and 18 remained consistent with the first on-orbit activity of characterizing the natural environment. The third demonstration activity involved RELL scanning an Active Thermal Control System (ATCS) radiator. Three locations along the radiator were scanned and the angular position of RELL with respect to the radiator was varied. Mass-to-charge ratios 16 and 17 both had upward shifts in partial pressure when pointing toward the Radiator Beam Valve Modules (RBVMs), likely corresponding to a known, small ammonia leak.

International Space Station↗

Natural and Induced Environment Around the International Space Station (ISS) as Observed During On-Orbit Operations of the Robotic External Leak Locator (RELL)

The Robotic External Leak Locator (RELL) was deployed to the International Space Station (ISS) with the goal of detecting and locating on-orbit leaks around the ISS. Three activities to characterize the background natural and induced environment of ISS were performed with RELL as part of the on-orbit validation and demonstration conducted in November and December 2016. The first demonstration activity pointed RELL directly in the ram (+X) and wake (-X) directions for one orbit each. The ram facing measurements showed high partial pressure for mass-to-charge ratio 16, corresponding to atomic oxygen (AO), as well as the presence of mass-to-charge ratio 17. RELL's view in the wake-facing direction included more ISS structure and several Environmental Control and Life Support System (ECLSS) on-orbit vents were detected, including the Carbon Dioxide Removal Assembly (CDRA), Russian segment ECLSS, and Sabatier vents. The second demonstration activity pointed RELL at three faces of the P1 Truss segment. Effluents from ECLSS and European Space Agency (ESA) Columbus module on-orbit vents were detected by RELL. The partial pressures of mass-to-charge ratios 17 and 18 remained consistent with the first on-orbit activity of characterizing the natural environment. The third demonstration activity involved RELL scanning an Active Thermal Control System (ATCS) radiator. Three locations along the radiator were scanned and the angular position of RELL with respect to the radiator was varied. Mass-to-charge ratios 16 and 17 both had upward shifts in partial pressure when pointing toward the Radiator Beam Valve Modules (RBVMs), likely corresponding to a known, small ammonia leak.

Fox, Katie L.↗

International Space Station (ISS) Environmental Control and Life Support System (ECLSS) Vent Flow Reflection and Detection by Robotic External Leak Locator (RELL)

On-orbit Robotic External Leak Locator (RELL) (i.e., mass spectrometer and ion gauge) measurements on the International Space Station (ISS) are presented to show the detection of recurring Environmental Control and Life Support System (ECLSS) vents at multiple ISS locations and RELL pointing directions. The path of ECLSS effluents to the RELL detectors is not entirely obvious at some locations, but the data indicates that diffuse gas-surface reflection or scattering resulting from plume interaction with vehicle surfaces is responsible. RELL was also able to confirm the ISS ECLSS constituents and distinguish them from the ammonia leak based on the ion mass spectra and known venting times during its operation to locate a leak in the ISS port-side External Active Thermal Control System (EATCS) coolant loop.

Gas/Surface Reflections or Scattering↗

Annular Air Leaks in a Liquid Hydrogen Storage Tank

Large liquid hydrogen (LH2) storage tanks are vital infrastructure for NASA, the DOD, and industrial users. Over time, air may leak into the evacuated, perlite filled annular region of these tanks. Once inside, the extremely low temperatures will cause most of the air to freeze. If a significant mass of air is allowed to accumulate, severe damage can result from nominal draining operations. Collection of liquid air on the outer shell may chill it below its ductility range, resulting in fracture. Testing and analysis to quantify the thermal conductivity of perlite that has nitrogen frozen into its interstitial spaces and to determine the void fraction of frozen nitrogen within a perlite-frozen nitrogen mixture is presented. General equations to evaluate methods for removing frozen air, while avoiding fracture, are developed. A hypothetical leak is imposed on an existing tank and a full analysis of that leak is detailed. This analysis includes a thermal model of the tank and a time-to-failure calculation. Approaches to safely remove the frozen air are analyzed, leading to the conclusion that the optimal approach is to allow the frozen air to melt and use a water stream to prevent the outer shell from chilling.

Krenn, A. G.↗

Finding and Fixing a Small Low Temperature Leak - A Case Study on XRISM/Resolve

The Resolve instrument on the X-Ray Imaging and Spectroscopy Mission (XRISM) uses an Adiabatic Demagnetization Refrigerator (ADR) to cool extremely sensitive x-ray microcalorimeters to 50 mK. A 40-liter superfluid helium dewar and a 4.5 K Joule Thomson (JT)/Stirling cryocooler serve as heat sinks for the ADR and staged cooling for the dewar. The superfluid helium lifetime is required to last at least 3 years on orbit with margin. The superfluid helium dewar developed a small leak (~5e-7 Pa m^3/s) at low temperature which compromised the dewar vacuum in two days of ground testing. It turns out that this leak disappears completely at room temperature (<5e-13 Pa m^3/s). This presentation describes the lengthy process of characterizing, isolating, and ultimately, repairing this leak.

Michael DiPirro↗

Ground-Based Cryogenic Leak Test of Fittings for Cryogenic Fluid Management

Mechanically connected fluid joints are virtually unavoidable in complex cryogenic system designs. In the case of spacecraft, the performance of these joints is critical to mission success. This is especially true for long-duration space missions where even very low leak rates can eventually lead to significant propellant losses or failure of vital cryogenic cooling systems. NASA has recently undertaken an effort to quantify the leak rate of Vacuum Coupling Radiation (VCR) fittings over the temperature range from ambient to 20 K, both before and after exposure to a launch vibration profile. A test apparatus employing a cryocooler and a calibrated helium mass spectrometer was developed, validated, and used to obtain quantifiable leak rates at a fitting test pressure of 31 bar (450 psig). Three different fitting sizes were tested, 25.4 mm (¼ inch), 12.7 mm (½ inch), and 6.35 mm (1 inch) and two gasket materials, stainless steel, and silver-plated nickel. Each fitting configuration (size/seal material) was subjected to two consecutive cryogenic thermal cycles/measurement tests, followed by a launch vibration test profile at ambient temperature, and then two additional cryogenic thermal cycles/measurement tests. The design and development of the test apparatus, and test data are presented and discussed in detail.

G J Tamasy↗

Evaluation of an Accident Tolerant Fuel Leak in the Advanced Test Reactor

Accident Tolerant Fuels (ATF), which are nuclear fuel sources designed to withstand operational irregularities and incidents, have been a topic of interest in the nuclear industry for several decades. Interest in ATF technology surged following the 2011 accident at Fukushima Daiichi in Japan. At the Advanced Test Reactor (ATR), one of Idaho National Laboratory’s (INL) four operating nuclear reactors, the ATF program is a collaborative effort between the national laboratory and various stakeholders within the nuclear industry. This program focuses on the research and development of novel fuel compositions, cladding, and component materials with enhanced accident-resistant properties. During one of ATR’s 60-day operating cycles in 2024, the reactor experienced five unplanned shutdowns. Following the fifth shutdown, radiation monitors detected an increase in radiation levels coming from the loop piping. Subsequent water samples confirmed the cause was a leak of fission products from the ATF experiment, designated as ATF-2C. The source of the leak was identified as the instrumented section of the test train. The primary discussions in this paper are 1) the design of the ATF test train, 2) the operating parameters leading up to and following the detection of the leak, and 3) the quantification and characterization of the released fission products.

Accident Tolerant Fuels↗

Evaluation of an Accident Tolerant Fuel Leak in the Advanced Test Reactor

Accident Tolerant Fuels (ATF), which are nuclear fuel sources designed to withstand operational irregularities and incidents, have been a topic of interest in the nuclear industry for several decades. Interest in ATF technology surged following the 2011 accident at Fukushima Daiichi in Japan. At the Advanced Test Reactor (ATR), one of Idaho National Laboratory’s (INL) four operating nuclear reactors, the ATF program is a collaborative effort between the national laboratory and various stakeholders within the nuclear industry. This program focuses on the research and development of novel fuel compositions, cladding, and component materials with enhanced accident-resistant properties. During one of ATR’s 60-day operating cycles in 2024, the reactor experienced five unplanned shutdowns. Following the fifth shutdown, radiation monitors detected an increase in radiation levels coming from the loop piping. Subsequent water samples confirmed the cause was a leak of fission products from the ATF experiment, designated as ATF-2C. The source of the leak was identified as the instrumented section of the test train. The primary discussions in this presentation are 1) the design of the ATF test train, 2) the operating parameters leading up to and following the detection of the leak, and 3) the quantification and characterization of the released fission products.

11 - NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Solid-State Mixed-Potential Electrochemical Sensors for Natural Gas Leak Detection and Quality Control (Final Technical Report)

Mitigation of methane emissions are a critical factor to limiting the impact of the natural gas industry on global climate change. Throughout the period of 2020-2024, the University of New Mexico and its commercialization partner and subcontractor, SensorComm Technologies, Inc. (SCT), have worked together to develop a low-cost Artificial Intelligence (AI)-driven Internet of Things (IoT)-based multi-gas sensor platform for methane emissions detection. In the final year of the project, we extended this work to include hydrogen detection in support of a transition to a hydrogen economy where hydrogen could be transported through existing natural gas infrastructure. Mixed potential electrochemical sensors were first prototyped by ceramic additive manufacturing and then transitioned to conventional ceramic manufacturing tape casting and screen-printing technologies in preparation for mass production. Demonstrated limits of detection of 5 ppm of methane in natural gas and 1 ppm of hydrogen were measured. These limits of detection are among the lowest of solid-state electrochemical sensors that have been reported in the literature or available in the industry. Machine learning algorithms were developed to identify natural gas mixtures with > 98% accuracy level and quantify methane concentrations at 97% accuracy. The presence of hydrogen could also be identified, and its concentration quantified at these accuracy levels. These algorithms were optimized for running on portable computing hardware which enabled > 1 Hz processing rates. A portable packaged IoT system was integrated with the electrochemical sensor in collaboration with SCT. The package consists of readout electronics with < 1 mV resolution, sensor temperature control, and data transmission over cellular wireless and/or Wi-Fi networks. Field testing was performed in two rounds at Colorado State University’s Methane Emissions Technology Evaluation Center (CSU METEC). The first round of testing demonstrated successful measurements of methane from an underground natural gas leak of 20 standard liters per minute (SLPM), which agreed with previously published literature using more sophisticated and expensive analytical equipment. The second round of testing showed that an above ground leak of 2 SLPM of hydrogen could be detected at 32 ft. This project has resulted in six published peer reviewed journal articles, over ten presentations at professional conferences, and one full patent application filed in 2023. Future work on this project includes increased sensitivity, higher production yields, and applications in the hydrogen safety and flare emissions monitoring spaces.

03 NATURAL GAS↗

Capacitive system detects and locates fluid leaks

Electronic monitoring system automatically detects and locates minute leaks in seams of large fluid storage tanks and pipelines covered with thermal insulation. The system uses a capacitive tape-sensing element that is adhesively bonded over seams where fluid leaks are likely to occur.

Source record↗

Silver plating technique seals leaks in thin wall tubing joints

Leaks in thin wall tubing joints are sealed by cleaning and silver plating the hot gas side of the joint in the leakage area. The pressure differential across the silver during hydrostatic test and subsequent use forces the ductile silver into the leak area and seals it.

Blenderman, W. H.↗

Proceedings of the Conference on the Design of Leak-tight Fluid Connectors

These technical papers were prepared for presentation at the Conference on Design of Leak-tight Fluid Connectors sponsored by the Society of Automotive Engineers and NASA/George C. Marshall Space Flight Center. This conference was planned to promote the direct exchange of technical information concerning separable, semipermanent and permanent leak-tight fluid connectors for space vehicle use. A conference emphasizing design of separable connectors was previously held on March 24 and 25, 1964. The papers represent a cross section of significant topics on design, testing and instrumentation. This exchange of technical information between government agencies and private industry is certain to benefit the nation's space effort and other fields of technology. The sponsors of the conference extend their thanks to all companies and individuals who have contributed toward this meeting.

Connector↗

Portable detector set discloses helium leak rates

Portable helium detector measuring helium leak rates makes possible the use of the inert gas helium as a tracer. This helps solve safety and contamination problems in detecting leaks in closed fluid systems.

Anderson, G. E.↗

Burst diaphragm leak detector

New method replaces flowmeter approach with readily available burst diaphragm leak detector assembly mounted to all drain ports. This allows simultaneous leak detection of all flange seals under operating conditions.

Pascolla, J. A.↗

Leak detector-measurer

Detector locates leaks from inside pressurized cabins. Head is placed flush against area being tested. Should leak be present, most air inside detector housing will escape. Diaphragm will then flex into chamber and push electrical contact together, closing circuit and turning on warning light.

Sawyer, J. T.↗