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NASA NTRSDate not supplied

Simulation-Aided Design and Interpretation of Results of Microgravity-Based Solidification Experiments

The preparation and interpretation of microgravity experiments conducted on the International Space Station (ISS) can be challenging because of the remote location of the equipment. Although a “ground unit” is typically available on Earth, it is not located in the laboratory of the principal investigator. Furthermore, test experiments in the ground unit cannot fully duplicate heat transfer conditions of the weightless environment, and thus be a reliable reference for experiment design. Under such conditions, numerical simulations are a valuable tool both for preparing the experiments and interpreting the results obtained under terrestrial and micro-gravity conditions. In this work, we developed a detailed 3D model of the “SUBSA” furnace located at the ISS, and demonstrate its use in our present investigation which includes melt growth and vapor growth of InI crystals on the ISS. In 2002, the SUBSA furnace was designed and built for the growth of InSb crystals in the Microgravity Science Glovebox (MSG) at the ISS. The SUBSA furnace features a transparent section without heating elements, where the axial temperature gradient is high. In our present investigation, we have used the same furnace to grow four InI crystals from the melt, and two InI crystals from the vapor phase (2018-2021). InI crystals have ~20 times lower thermal conductivity than InSb crystals. As a result, during melt growth, the InI crystals were exposed to extremely high temperature gradients. To reduce the axial temperature gradient, we added external jackets made from high thermal conductivity material to the growth ampoules. The SUBSA furnace could not be modeled as asymmetric because of its rectangular shape and right-angled transparent section, which contains a convoluted geometry. The rectangular shape of the transparent section further complicates modelling of radiative heat transfer, which dominates in the zone. At present, numerical simulations are being conducted to resolve an apparent discrepancy between the readings of the 5 thermocouples located in the SUBSA furnace, and the observed position of the solid and molten material. The 3D simulation will be presented, along with the calibration and growth experiment results conducted in microgravity and in the SUBSA ground unit. The developed model should be useful for upcoming microgravity investigations planned to be conducted in the SUBSA facility.

V Riabov↗

NASA NTRS1993

The Structure and Stability of Laminar Flames

This review paper on the structure and stability of laminar flames considers such phenomena as heterogeneous mixtures, acoustic instabilities, flame balls and related phenomena, radiation effects, the iodate oxidation of arsenous acid and 'liquid flame fronts', approximate kinetic mechanisms and asymptotic approximations, and tribrachial or triple flames. The topics examined here indicate three themes that may play an important role in laminar flame theory in the coming years: microgravity experiments, kinetic modeling, and turbulence modeling. In the discussion of microgravity experiments it is pointed out that access to drop towers, the Space Shuttle and, in due course, the Space Station Freedom will encourage the development of experiments well designed to isolate the fundamental physics of combustion.

Buckmaster, John↗

NASA NTRS1989

Non-contact temperature measurements in support of microgravity combustion experiments

Recent conceptual advances in the understanding of combustion science fundamentals in the context of microgravity processes and phenomenology have resulted in an increased demand for diagnostic systems of greater sophistication. Owing primarily to the severe operational constraints that accompany the space flight environment, measurement systems to date remain fairly primative in nature. Qualitative pictures provided by photographic recording media comprise the majority of the existing data, the remainder consisting of the output of conventional transducers, such as thermocouples, hot wires, and pressure transducers. The absence of the rather strong influence of buoyant convection renders microgravity combustion phenomena more fragile than their 1-G counterparts. The emphasis was placed on nonperturbing optical diagnostics. Other factors such as limited supplies of expendable reactants, and periods of microgravity time of sufficient duration, coupled with more fundamental questions regarding inherent length and time scales and reproducibility have favored multipoint or multidimensional techniques. While the development of optical diagnostics for application to combustion science is an extremely active area at present, the peculiarities of space flight hardware severely restrict the feasibility of implementing the majority of techniques which are being utilized in terrestrial applications. The additional requirements for system reliability and operational simplicity have tended to promote somewhat less commonly emphasized techniques such as refractive index mapping and molecular Rayleigh scattering, which are briefly discussed.

Greenberg, Paul S.↗

NASA NTRS2000

Testing the BUNDLE Experiment for Microgravity Disturbance Characterization

A primary objective of the International Space Station is to provide a premier facility for microgravity research. There are many disturbances on board the Station that can disturb the quality of the microgravity environment, including disturbances caused by both system and payload hardware. Disturbances within experiments themselves can also affect the quality of their own environment. The primary functions of the Bridgman Unidirectional Dendrites in Liquids Experiment (BUNDLE) are to melt, directionally solidify, and perform in-situ quench of metallic alloys, providing data to aid in understanding the effects of the microgravity environment on the characteristics of these processed metals. Quenching of the samples in the BUNDLE furnace is accomplished by rapidly introducing high pressure helium into the furnace chamber. This type of quench will induce sample vibrations which may be large enough to adversely affect sample quality. The primary objective of the test described in this presentation was to determine the acceleration imparted on the BUNDLE sample during helium quench. From this information, the science community can better assess whether this method of quench will allow them to obtain the data they need. Utilizing breadboard hardware, the sample quench sequence was conducted. Data was collected from accelerometers located on the breadboard hardware and inside the sample cartridge. The test data indicated that the maximum acceleration achieved by the sample was 0.325 g, which is much higher than the desired microgravity (10(exp -6) g) environment. However, this acceleration level occurred over a time period of less than 0.1 second. Because this time period is so short, there should be no detrimental effects to dendrite growth. This result was consistent with the observations of the experiment scientists, who are satisfied with the results of previous dendrite growth in this breadboard unit.

Gattis, Christy↗

NASA NTRS2018

GeneLab: "Omics" Data System for Space Biology Research

Determining the biological impact of spaceflight through novel approaches is essential to reduce the health risks to astronauts for long-term space missions. The current established health risks due to spaceflight are only reflecting known symptomatic and physiologic responses and do not reflect early onset of other potential diseases. There are many unknown variables which still need to be identified to fully understand the health impacts due to the environmental factors in space. One method to uncover potential novel biological mechanisms responsible for health risks in astronauts is by utilizing NASA's GeneLab Data Systems (genelab.nasa.gov). GeneLab is public repository that hosts multiple omics datasets generated from space biology experiments that include experiments flown in space, simulated cosmic radiation experiments, and simulated microgravity experiments. This presentation will provide an overview of GeneLab and examples of analysis that are being done with GeneLab datasets. These example will include novel data and work being generated with various scientists around the world involved with GeneLab's Analysis Working Groups (AWG) that are assisting with the development of pipelines and advancing GeneLab to the next phase, a publication from GeneLab discovering novel Carbon Dioxide impact due to rodent habitats, another publication from GeneLab discovering a potential master regulator responsible for health risk associated due to spaceflight, and potential cardiovascular risk from space radiation.

microgravity↗

NASA NTRS2018

GeneLab: "Omics" Data Systems for Spaceflight and Simulated Spaceflight Environment

spaceflight↗

NASA NTRS1998

Measurement of Critical Contact Angle in a Microgravity Space Experiment

Mathematical theory predicts that small changes in container shape or in contact angle can give rise to large shifts of liquid in a microgravity environment. This phenomenon was investigated in the Interface Configuration Experiment on board the USML-2 Space Shuttle flight. The experiment's "double proboscis" containers were designed to strike a balance between conflicting requirements of sizable volume of liquid shift (for ease of observation) and abruptness of the shift (for accurate determination of critical contact angle). The experimental results support the classical concept of macroscopic contact angle and demonstrate the role of hysteresis in impeding orientation toward equilibrium.

Concus, P.↗

NASA NTRS1998

Measurement of Critical Contact Angle in a Microgravity Space Experiment

Mathematical theory predicts that small changes in container shape or in contact angle can give rise to large shifts of liquid in a microgravity environment. This phenomenon was investigated in the Interface Configuration Experiment on board the USMT,2 Space Shuttle flight. The experiment's "double proboscis" containers were designed to strike a balance between conflicting requirements of sizable volume of liquid shift (for ease of observation) and abruptness of the shift (for accurate determination of critical contact angle). The experimental results support the classical concept of macroscopic contact angle and demonstrate the role of hysteresis in impeding orientation toward equilibrium.

Concus, P.↗

NASA NTRS1998

NASA's Microgravity Fluid Physics Program: Tolerability to Residual Accelerations

An overview of the NASA microgravity fluid physics program is presented. The necessary quality of a reduced-gravity environment in terms of tolerable residual acceleration or g levels is a concern that is inevitably raised for each new microgravity experiment. Methodologies have been reported in the literature that provide guidance in obtaining reasonable estimates of residual acceleration sensitivity for a broad range of fluid physics phenomena. Furthermore, a relatively large and growing database of microgravity experiments that have successfully been performed in terrestrial reduced gravity facilities and orbiting platforms exists. Similarity of experimental conditions and hardware, in some cases, lead to new experiments adopting prior experiments g-requirements. Rationale applied to other experiments can, in principle, be a valuable guide to assist new Principal Investigators, PIs, in determining the residual acceleration tolerability of their flight experiments. The availability of g-requirements rationale from prior (mu)g experiments is discussed. An example of establishing g tolerability requirements is demonstrated, using a current microgravity fluid physics flight experiment. The Fluids and Combustion Facility (FCF) which is currently manifested on the US Laboratory of the International Space Station (ISS) will provide opportunities for fluid physics and combustion experiments throughout the life of the ISS. Although the FCF is not intended to accommodate all fluid physics experiments, it is expected to meet the science requirements of approximately 80% of the new PIs that enter the microgravity fluid physics program. The residual acceleration requirements for the FCF fluid physics experiments are based on a set of fourteen reference fluid physics experiments which are discussed.

Skarda, J. Raymond↗

NASA NTRSDate not supplied

Mitochondria Dysfunction Central in Driving Health Risks Associated with Spaceflight

Background: Determining the biological impact of spaceflight through novel approaches is essential to reduce the health risks to astronauts for long-term space missions. The current established health risks due to spaceflight are only reflecting known symptomatic and physiologic responses and do not reflect early onset of other potential diseases. There are many unknown variables which still need to be identified to fully understand the health impacts due to the environmental factors in space. Materials and Methods: One method to uncover potential novel biological mechanisms responsible for health risks in astronauts is by utilizing NASA’s GeneLab platform (genelab.nasa.gov). GeneLab is public repository that hosts multiple omics datasets generated from space biology experiments that include experiments flown in space, simulated cosmic radiation experiments, and simulated microgravity experiments. This presentation will provide an example of analysis and novel hypothesis generation that is being produced with GeneLab datasets. A comprehensive multi-omics approach was implemented correlating transcriptomics, proteomics, metabolomics, and methylation analysis. Results: We found that cells have stronger overall biological response than the tissues to spaceflight, with mitochondrial activity and innate immunity pathways being heavily impacted. NASA Twin Study results are consistent with a specific alteration in mitochondrial ATP production. Our results indicate that the space environment can directly induce mitochondrial damage, with mitochondrial dysfunctions being a cause for chronic inflammation and both being involved in the development of metabolic disorders that cause changes in lipid metabolism. We also found biological changes occurring during spaceflight with cell cycle, circadian rhythm and olfactory activity pathways can also influence and be influenced by alterations on mitochondrial activity

Afshin Beheshti↗

NASA NTRS1990

Space Station Based Microacceleration Experiment Platform

Normal Space Station Freedom activities, such as docking, astronauts' movement, equipment vibrations, and space station reboosts, exert forces on the structure, resulting in static or transient accelerations greater than many microgravity experiments can tolerate. A solution to this problem is to isolate experiments on a separate platform free from such disturbances. The Space Station Based Microacceleration Experiment Platform, a proposed solution to the Space Station microgravity experiment problem is described. It is modular in design and can be telerobotically assembled and operated. The Microacceleration Experiment Platform (MEP) consists of a minimum configuration platform to which power, propulsion, propellant, and experiment modules are added. The platform's layout is designed to take maximum advantage of the microgravity field structure in orbit.

Barber, Katy↗

NASA NTRS1991

Electrophoresis experiments in microgravity

The use of the microgravity environment to separate and purify biological cells and proteins has been a major activity since the beginning of the NASA Microgravity Science and Applications program. Purified populations of cells are needed for research, transplantation and analysis of specific cell constituents. Protein purification is a necessary step in research areas such as genetic engineering where the new protein has to be separated from the variety of other proteins synthesized from the microorganism. Sufficient data are available from the results of past electrophoresis experiments in space to show that these experiments were designed with incomplete knowledge of the fluid dynamics of the process including electrohydrodynamics. However, electrophoresis is still an important separation tool in the laboratory and thermal convection does limit its performance. Thus, there is a justification for electrophoresis but the emphasis of future space experiments must be directed toward basic research with model experiments to understand the microgravity environment and fluid analysis to test the basic principles of the process.

Snyder, Robert S.↗

NASA NTRS2000

Current Experiments in Microgravity

The Materials Science program within NASA's Microgravity Research Division will be outlined. Particular emphasis will be placed on those experiments slated for the International Space Station which pertain to high temperature materials. These include experiments designed to examine theories pertaining to solidification and pattern selection, coarsening and phase transformation.

Gillies, Donald C.↗

NASA NTRS1999

Effect of Marangoni Convection Generated by Voids on Segregation During Low-G and 1-G Solidification

Solidification experiments, especially microgravity solidification experiments are often hampered by the evolution of unwanted voids or bubbles in the melt. Although these voids and/or bubbles are highly undesirable, there are currently no effective means of preventing their formation or eliminating their adverse effects, particularly, during low-g experiments. Marangoni Convection caused by these voids can drastically change the transport processes in the melt and, therefore, introduce enormous difficulties in interpreting the results of the space investigations. Recent microgravity experiments by Matthiesen, Andrews, and Fripp are all good examples of how the presence of voids and bubbles affect the outcome of costly space experiments and significantly increase the level of difficulty in interpreting their results. In this work we examine mixing caused by Marangoni convection generated by voids and bubbles in the melt during both 1-g and low-g solidification experiments. The objective of the research is to perform a detailed and comprehensive combined numerical-experimental study of Marangoni convection caused by voids during the solidification process and to show how it can affect segregation and growth conditions by modifying the flow, temperature, and species concentration fields in the melt. While Marangoni convection generated by bubbles and voids in the melt can lead to rapid mixing that would negate the benefits of microgravity processing, it could be exploited in some terrestrial processing to ensure effective communication between a melt/solid interface and a gas phase stoichiometry control zone. Thus we hope that this study will not only aid us in interpreting the results of microgravity solidification experiments hampered by voids and bubbles but to guide us in devising possible means of minimizing the adverse effects of Marangoni convection in future space experiments or of exploiting its beneficial mixing features in ground-based solidification.

Kassemi, M.↗

NASA NTRS1984

Rationale for two phase polymer system microgravity separation experiments

The two-phase systems that result when aqueous solutions of dextran and poly(ethylene glycol) are mixed at concentrations above a few percent are discussed. They provide useful media for the partition and isolation of macromolecules and cell subpopulations. By manipulating their composition, separations based on a variety of molecular and surface properties are achieved, including membrane hydrophobic properties, cell surface charge, and membrane antigenicity. Work on the mechanism of cell partition shows there is a randomizing, nonthermal energy present which reduces separation resolution. This stochastic energy is probably associated with hydrodynamic interactions present during separation. Because such factors should be markedly reduced in microgravity, a series of shuttle experiments to indicate approaches to increasing the resolution of the procedure are planned.

Brooks, D. E.↗

NASA NTRS1977

Surface tension induced convection in encapsulated liquid metals in a microgravity environment. Experiment MA-041

The experiment was designed to detect possible convection caused by a steplike compositional variation in a liquid metal in a microgravity environment. Wetting and nonwetting ampoules were used to try to determine the extent of the stirring effects if they were present. Since stirring effects can be caused by temperature gradients, the temperature gradients were minimized. Steplike compositional variation was created by pressure bonding a lead-0.05 atom percent gold alloy to pure lead. Two diffusion temperatures (923 K and 723 K) were used; if no stirring effects were present, it was hoped that the liquid diffusion parameters for gold in lead could be obtained. Two identifical experimental arrangements were used to compare the transport mechanisms of gold in liquid lead in unit gravity and microgravity environments.

Reed, R. E.↗

NASA NTRS1993

Ground-based experiments complement microgravity flight opportunities in the investigation of the effects of space flight on the immune response: is protein kinase C gravity sensitive?

This manuscript briefly reviews ground-based and flight experiments, discusses how those experiments complement each other, and details how those experiments lead us to speculate about the gravity-sensitive nature of protein kinase C.

Review↗

NASA NTRS1992

A 6 degree-of-freedom Lorentz force vibration isolator with nonlinear controller

This program demonstrated the technical feasibility of constructing large-stroke magnetic suspensions that can meet the active vibration isolation requirements of Space Station. These requirements include: (1) strokes over 1 cm in all directions, (2) actuator bandwidths over 100 Hz, (3) isolator roll-off frequencies below 10(exp -2) Hertz, and (4) force capability over 1 Newton in all axes. The 100 Hz actuator bandwidth allows the suspension to reject any direct force disturbances that act on the microgravity experiment, for example forces created by cable connections. The low isolator roll-off frequency and large stroke allow the magnetic suspension to isolate the microgravity experiment from Space Station vibrations above the roll-off frequency. The capability to meet these requirements was demonstrated by designing, constructing and testing a six-degree-of-freedom, prototype magnetic suspension system that featured high-performance, Lorentz-force actuators and full multi-input, multi-output control. This prototype suspension is designed to isolate large orbiter locker experiments under typical spacecraft constraints of size, weight, and power. Suspension in the full six-degrees-of-freedom was successfully demonstrated in this program while using a gravity-force unload mechanism to simulate a space environment. The prototype isolator is capable of space-based isolation service with relatively minor modification. The use of advanced, nonlinear control algorithms were investigated on a specially designed single-degree-of-freedom testbed. This low acceleration test facility simulates the Space Station vibration isolation problem in a single horizontal axis with low-friction, air-slide support. This allowed testing at the desired microgravity levels, without the gravity bias effects that are seen in a full six-degrees-of-freedom suspension. Precision components were used to reduce residual accelerations to microgravity levels so that the effects of sensor, actuator, and electronic noise could be evaluated. During the Phase 2 program, this testbed was used to demonstrate the advantages of nonlinear control algorithms to provide increased vibration isolation performance.

Fenn, Ralph↗