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At least 145 records · Page 8

Deep trap, laser activated image converting system

Receiving an optical image on the surface of a photoconducting semiconductor is presented, storing the image in deep traps of the semiconductor, and later scanning the semiconductor with a laser beam to empty the deep traps, thereby producing a video signal. The semiconductor is illuminated with photons of energy greater than the band gap producing electron-hole pairs in the semiconductor which subsequently fill traps in energy from the band edges. When the laser beam of low energy photons excites the trapped electrons and holes out of the traps into the conduction and valence bands, a photoconductivity can be observed.

Maserjian, J.↗

Optical properties of ion beam textured metals

Copper, silicon, aluminum, titanium and 316 stainless steel were textured by 1000 eV xenon ions from an 8 cm diameter electron bombardment ion source. Simultaneously sputter-deposited tantalum was used to facilitate the development of the surface microstructure. Scanning electron microscopy of the ion textured surfaces revealed two types of microstructure. Copper, silicon, and aluminum developed a cone structure with an average peak-to-peak distance ranging from 1 micron for silicon to 6 microns for aluminum. Titanium and 316 stainless steel developed a serpentine ridge structure. The average peak-to-peak distance for both of these materials was 0.5 micron. Spectral reflectance was measured using an integrating sphere and a holraum reflectometer. Total reflectance for air mass 0 and 2, solar absorptance and total emittance normalized for a 425 K black body were calculated from the reflectance measurements.

Hudson, W. R.↗

Antiphase boundaries in epitaxially grown beta-SiC

When the surface of beta-SiC, grown epitaxially on (001) silicon by chemical vapor deposition, is chemically etched, boundaries appear which may be observed by optical or scanning electron microscopy. Examination by plan-view and cross-sectional transmission electron microscopy shows boundaries in the film which exhibit line or fringe contrast. Convergent beam electron diffraction has been used to show that these boundaries separate domains that are in an antiphase relationship to each other. A model is presented which discusses the formation of these domains from independent nucleation on a stepped substrate surface.

Pirouz, P.↗

Holographic Optical Elements as Scanning Lidar Telescopes

We have developed and investigated the use of holographic optical elements (HOEs) and holographic transmission gratings for scanning lidar telescopes. For example, rotating a flat HOE in its own plane with the focal spot on the rotation axis makes a very simple and compact conical scanning telescope. We developed and tested transmission and reflection HOEs for use at the first three harmonic wavelengths of Nd:YAG lasers. The diffraction efficiency, diffraction angle, focal length, focal spot size and optical losses were measured for several HOEs and holographic gratings, and found to be suitable for use as lidar receiver telescopes, and in many cases could also serve as the final collimating and beam steering optic for the laser transmitter. Two lidar systems based on this technology have been designed, built, and successfully tested in atmospheric science applications. This technology will enable future spaceborne lidar missions by significantly lowering the size, weight, power requirement and cost of a large aperture, narrow field of view scanning telescope.

Schwemmer, Geary K.↗

Multispectral scanner optical system

An optical system for use in a multispectral scanner of the type used in video imaging devices is disclosed. Electromagnetic radiation reflected by a rotating scan mirror is focused by a concave primary telescope mirror and collimated by a second concave mirror. The collimated beam is split by a dichroic filter which transmits radiant energy in the infrared spectrum and reflects visible and near infrared energy. The long wavelength beam is filtered and focused on an infrared detector positioned in a cryogenic environment. The short wavelength beam is dispersed by a pair of prisms, then projected on an array of detectors also mounted in a cryogenic environment and oriented at an angle relative to the optical path of the dispersed short wavelength beam.

Stokes, R. C.↗

C-Coupon Studies of CMCS: Fracture Behavior and Microstructural Characterization

A curved beam 'C-coupon' was used to assess fracture behavior in a Sylramic(tm)/melt infiltration (MI) SiC matrix composite. Failure stresses and fracture mechanisms, as determined by optical and scanning electron microstructural analysis, are compared with finite element stress calculations to analyze failure modes. Material microstructure was found to have a strong influence on mechanical behavior. Fracture occurs in interlaminar tension (ILT), provided that the ratio of ILT to tensile strength for the material is less than the ratio of radial to hoop stresses for the C-coupon geometry. Utilization of 3D architectures to improve interlaminar strength requires significant development efforts to incorporate through thickness fibers in regions with high curvatures while maintaining uniform thickness, radius, and microstructure.

Hurwitz, Frances I.↗

Eucrite Impact Melt NWA 5218 - Evidence for a Large Crater on Vesta

Northwest Africa (NWA) 5218 is a 76 g achondrite that is classified as a eucrite [1]. However, an initial classification [2] describes it as a "eucrite shock-melt breccia...(in which) large, partially melted cumulate basalt clasts are set in a shock melt flow...". We explore the petrology of this clast-bearing impact melt rock (Fig. 1), which could be a characteristic lithology at large impact craters on asteroid Vesta [3]. Methods: Optical microscopy, scanning electronmicroscopy, and Raman spectroscopy were used on a thin section (Fig. 1) for petrographic characterization. The impact melt composition was determined by 20 m diameter defocused-beam analyses with a Cameca SX-100 electron microprobe. The data from 97 spots were corrected for mineral density effects [4]. Constituent mineral phases were analyzed with a focusedbeam. Bidirectonal visible and near-infrared (VNIR) and biconical FT-IR reflectance spectra were measured on the surface of a sample slab on its central melt area and on an eucrite clast, and from 125-500 m and <125 m powders of melt. Results: General petrography: The sample specimen is a coherent, medium dark-grey (N4), melt rock. The thin section captures a central, subophitic-textured melt that contains ~1 cm to tens of m-size subangular to rounded, variably-shocked eucrite clasts. Clasts >100 m are coarse-grained with equigranular ~1 mm size plagioclase, quartz, and clinopyroxene (Fig. 1). Single crystals of chromite, ilmenite, zircon, Ca-Mg phosphate, Fe-metal, and troilite are embedded in the melt. Polymineralic clasts are mostly compositionally similar to the above mentioned larger clasts but scarce granulitic fragments are observed as well.

Wittmann, Axel↗

Structural and optical characterization of dilute Bi-doped GaN nanostructures grown by molecular beam epitaxy

We have carried out detailed studies on the epitaxy and characterization of dilute Bi-doped GaN nanostructures. A comprehensive investigation of Bi-doped GaN nanowires and quasi-film epitaxial growth conditions has been performed. Scanning electron microscopy studies show that lowering the GaBiN growth temperature causes gradual changes in top c-plane nanowire morphology due to the incremental incorporation of foreign Bi atoms. This trend is further substantiated by the secondary ion mass spectroscopy analysis of a multi-layer Bi-doped GaN quasi-film. However, it is also found that the amount of Bi incorporation into the GaN lattice is relatively independent of the N2 flow rate variation under the growth conditions investigated. Furthermore, room-temperature micro-Raman spectra show that there are additional peaks near 530, 650, and 729 cm−1 wave numbers in the Bi-doped GaN samples, which can primarily be attributed to Bi local vibrational modes, indicative of a small amount of Bi incorporation in the GaN lattice. Moreover, phonon calculations with density functional theory indicate that Bi replacing the N sites is the likely origin of the experimentally measured Raman modes. X-ray photoelectron spectroscopy measurements have also been obtained to deduce the electronic interaction between the Bi dopant atom and the GaN nanostructure. Such one-dimensional nanowires permit the synthesis of dislocation-free highly mismatched alloys due to strain relaxation, allowing efficient light absorption and charge carrier extraction that is relevant for solar energy harvesting and artificial photosynthesis.

Materials Science↗

Zone Refining by Laser

System developed for studying use of laser beam for zone-refining semiconductors and metals. Specimen scanned with focused CO2 laser beam in such way that thin zone of molten material moves along specimen sweeps impurities with it. Zone-melting system comprises microcomputer, laser, electromechanical and optical components for beam control, vacuum chamber that holds specimen, and sensor for determining specimen temperature.

Griner, D. B.↗

Rectangular Relief Diffraction Gratings for Coherent Lidar Beam Scanning

The application of specialized rectangular relief transmission gratings to coherent lidar beam scanning is presented. Two types of surface relief transmission grating approaches are studied with an eye toward potential insertion of a constant thickness, diffractive scanner where refractive wedges now exist. The first diffractive approach uses vertically oriented relief structure in the surface of an optical flat; illumination of the diffractive scanner is off-normal in nature. The second grating design case describes rectangular relief structure slanted at a prescribed angle with respect to the surface. In this case, illumination is normal to the diffractive scanner. In both cases, performance predictions for 2.0 micron, circularly polarized light at beam deflection angles of 30 or 45 degrees are presented.

Cole, H. J.↗

Prototype Holographic Atmospheric Scanner for Environmental Remote Sensing (PHASERS)

A ground-based atmospheric lidar system that utilizes a Holographic Optical Telescope and Scanner has been developed and successfully operated to obtain atmospheric backscatter profiles. The Prototype Holographic Atmospheric Scanner for Environmental Remote Sensing is built around a volume phase reflection Holographic Optical Element. This single optical element both directs and collimates the outgoing laser beam as well as collects, focuses, and filters the atmospheric laser backscatter, while offering significant weight savings over existing telescope mirror technology. Conical scanning is accomplished as the HOE rotates on a turntable sweeping the 1.2 mrad field of view around a 42deg cone. During this technology demonstration, atmospheric aerosol and cloud return signals have been received in both stationary and scanning modes. The success of this program has led to the further development of this technology for integration into airborne and eventually satellite earth observing scanning lidar telescopes.

Guerra, David V.↗

Proposed Definitions of Some Technical Terms Frequently Used in Microwave Radiometry for Remote Sensing

The use of microwave radiometry for remote sensing is a relatively young field. As a result, there are no standard definitions of many frequently used technical terms; a lot of which are conventional usages carried-over from optical remote sensing, and a lot more are shared with electrical or microwave engineering. Sometimes the divergent notions and assumptions originating from a different field may cause ambiguity or confusions. It is proposed that we establish a list of frequently used terms, together with their 'standard' definitions and hope that they will gradually gain general acceptance by the remote sensing community. It would be even more useful if the IEEE community can set up a standard committee of sort to develop and maintain the standards. To minimize the effort, the existing terms should be kept or reinterpreted as much as possible. For example, the term 'Instantaneous Field of View' (IFOV), originally coming from the optical remote sensing field, is now appearing in microwave remote sensing literature frequently. The IFOV refers to the 'beam width' or the 'diameter' of the beam's geometrical projection on earth surface. Since the definition of 'beam width' is different for an optical system versus a microwave antenna, the use of IFOV in microwave radiometry needed to be clarified. Also, the meaning of the IFOV will be different depending upon whether the beam is scanning or not, and how the scanning takes place, e.g. 'continuous scanning' vs 'stare-and-step scan.' From this one term alone, it is clear that more subtle meanings must be spell out in detail and a 'standard' definition would help in understanding and comparing systems and data in the literature. A selected list of terms with their suggested definitions will be discussed in this presentation.

Shiue, James C.↗

Experimental Characterization of Photoemission from Plasmonic Nanogroove Arrays

Metal photocathodes are an important source of high-brightness electron beams, ubiquitous in the operation of both large-scale accelerators and table-top microscopes. When the surface of a metal is nanoengineered with patterns on the order of the optical wavelength, it can lead to the excitation and confinement of surface-plasmon-polariton waves that drive nonlinear photoemission. In this work, we aim to evaluate gold plasmonic nanogrooves as a concept for producing bright electron beams for accelerators via nonlinear photoemission. Here, we do this by first comparing their optical properties to numerical calculations from first principles to confirm our ability to fabricate these nanoscale structures. Their nonlinear photoemission yield is found by measuring emitted photocurrent as the intensity of their driving laser is varied. Finally, the mean transverse energy of this electron source is found using the solenoid-scan technique. Our data demonstrate the ability of these cathodes to provide a tenfold enhancement in the efficiency of photoemission over flat metals driven with a linear process. We find that these cathodes are robust and capable of reaching sustained average currents over 100 nA at optical intensities larger than 2 GW cm –2 with no degradation of performance. The emittance of the generated beam is found to be highly asymmetric, a fact we can explain with calculations involving the also asymmetric roughness of the patterned surface. These results demonstrate the use of nanoengineered surfaces as enhanced photocathodes, providing a robust air-stable source of high-average-current electron beams hopefully with great potential for industrial and scientific applications.

47 OTHER INSTRUMENTATION↗

Final Technical Report - Rapid Surface Microanalysis using a Low Temperature Plasma

This project focused on improving our current understanding and scientific knowledge in the area of plasma-surface interactions and plasma assisted material synthesis related to advanced microelectronics and nanotechnology. Current challenges include: controlling the interaction of Low Temperature Plasma (LTP) with a single layer of atoms to manufacture integrated circuits, continued miniaturization of integrated circuits, LTP processing of material surfaces and thin films to enable industrial scale fabrication of advanced microelectronics, synthesis of new materials, nanomaterials, nanotubes, and complex materials, Technology developed in this subtopic is of value to either (i) enable scans of surfaces (~1 sq. cm area) using various microscopies (electron, optical, other) at high resolution (micron or sub-micron resolution) rapidly (hours or days rather than years to complete a high-resolution scan of such a large surface area), or (ii) enable scans of surfaces (~1 sq. cm area) using various microscopies (electron, optical, other) at relatively low resolution rapidly, then apply algorithms to select spots for micron-scale imaging. Sputtering occurs when particles of a solid material are ejected from its surface by energetic particles from a plasma. While the degradation of the solid material and the subsequent deposition of the ejected material onto vulnerable surfaces are the usual subjects of sputtering studies, plasma science has yet to be combined with sputtering to create new diagnostics devices and systems. Small changes in the design of the plasma discharge device make it possible to create broad plasma beams for rapid scanning or small plasma beams to obtain the distribution of ejected elements with micron resolution. In the high-resolution use, the ion flux is extracted from the gas-discharge plasma and focused by a spherical emission surface to micron sizes onto the target specimen, providing very local sputtering and local elemental analysis. We call this “self-focusing”. The radiation from the excited and ionized sputtered atoms is recorded by a spectrometer through a window and fiberglass cable and analyzed with standard software packages used for optical glow discharge spectroscopy. Computer simulations of beam formation were used to verify and optimize the designs to be tested. A prototype was designed, constructed, and used to start experiments of beam formation.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Recycled polyethylene and crumb rubber composites modified asphalt with improved aging resistance and thermal stability

Crumb rubbers (CR) and recycled Polyethylene (PE) are commonly used as modifiers to improve the asphalt properties. However, the addition of these modifiers individually may result in phase separation of PE and inadequate degradation of CR, which may not simultaneously satisfy the rheological and aging resistance of the binder blends. In this study, a type of CR/PE composites manufactured through melt extrusion procedures was adopted for the improvement of the modified binder blends. The modified binder blends after short-term (RTFO) and long-term (PAV) aging were collected for dynamic shear rheometer and bending beam rheometer tests. FTIR tests were also used to quantify the aging resistance, while differential scanning calorimetry (DSC) and thermogravimetric analysis (TGA) were applied to evaluate the thermal behaviors of the binder blends. Optical microscopy tests were used to explore the modification mechanism and visualize the microstructures of original and PAV aged binder blends. Test results showed that CR/PE composites could significantly improve the aging resistance of the binder blends. The dispersed PE particles still interacted with each other and meanwhile worked with the diffused rubbery phase, which could form a similar TPEs network. The oxidation and high-temperature aging of such binder blends would strengthen the network that resisted the aging severity of the binder blends. Furthermore, it was also revealed that CR/PE modified asphalt could sustain more heat before a rapid degradation and the well-dispersed PE particles could interact with the diffused CR particles to form a network to resist aging.

02 PETROLEUM↗

Electronic heterodyne recording of interference patterns

An electronic heterodyne technique is being investigated for video (i.e., television rate and format) recording of interference patterns. In the heterodyne technique electro-optic modulation is used to introduce a sinusoidal phase shift between the beams of an interferometer. For phase modulation frequencies between 0.1 and 15 MHz an image dissector camera may be used to scan the resulting temporally modulated interference pattern. Heterodyne detection of the camera output is used to selectively record the interference pattern. An advantage of such synchronous recording is that it permits recording of low-contrast fringes in high ambient light conditions. The application of this technique to the recording of holograms is discussed.

Merat, F. L.↗

Development and applications of optical interferometric micrometrology in the Angstrom and subangstrom range

The characteristics of the scanning tunneling microscope and atomic force microscope (AFM) are briefly reviewed, and optical methods, mainly interferometry, of sufficient resolution to measure AFM deflections are discussed. The methods include optical resonators, laser interferometry, multiple-beam interferometry, and evanescent wave detection. Experimental results using AFM are reviewed.

Lauer, James L.↗

Method for Measuring the Volume-Scattering Function of Water

The volume scattering function (VSF) of seawater affects visibility, remote sensing properties, in-water light propagation, lidar performance, and the like. Currently, it s possible to measure only small forward angles of VSF, or to use cumbersome, large, and non-autonomous systems. This innovation is a method of measuring the full range of VSF using a portable instrument. A single rapid-sensing photosensor is used to scan a green laser beam, which delivers the desired measurement. By using a single sensor, inter-calibration is avoided. A compact design is achieved by using drift-free detector electronics, fiber optics, and a new type of photomultiplier. This provides a high angular resolution of 1 or better, as well as the ability to focus in on a VSF region of particular interest. Currently, the total scattering of light is measured as a difference from the other two parts of the light budget equation. This innovation will allow the direct calculation of the total scattering of light by taking an integral of the VSF over all angles. This directly provides one of the three components of the light budget equation, allowing greater versatility in its calculation.

Agrawal, Yogesh C.↗