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At least 145 records · Page 8

Hydrogen adsorption and diffusion, and subcritical-crack growth in high strength steels and nickel base alloys

Embrittlement, or the enhancement of crack growth by gaseous hydrogen in high strength alloys, is of primary interest in selecting alloys for various components in the space shuttle. Embrittlement is known to occur at hydrogen gas pressures ranging from fractions to several hundred atmospheres, and is most severe in the case of martensitic high strength steels. Kinetic information on subcritical crack growth in gaseous hydrogen is sparse at this time. Corroborative information on hydrogen adsorption and diffusion is inadequate to permit a clear determination of the rate controlling process and possible mechanism in hydrogen enhanced crack growth, and for estimating behavior over a range of temperatures and pressures. Therefore, coordinated studies of the kinetics of crack growth, and adsorption and diffusion of hydrogen, using identical materials, have been initiated. Comparable conditions of temperature and pressure will be used in the chemical and mechanical experiments. Inconel 718 alloy and 18Ni(200) maraging steel have been selected for these studies. Results from these studies are expected to provide not only a better understanding of the gaseous hydrogen embrittlement phenomenon itself, but also fundamental information on hydrogen adsorption and diffusion, and crack growth information that can be used directly for design.

Wei, R. P.↗

Low temperature mechanical properties, fractographic and metallographic evaluation of several alloy steels

The mechanical properties are presented of alloy steels, 4130, 4140, 4340, 6150, and 8740. Test specimens were manufactured from approximately 1.00 inch (2.54 cm) diameter bar stock which had been heat treated to two different hardness levels. The following mechanical tests were performed at temperatures of 80 F (+26.7 C), 0 F (-17.8 C), -100 F (-73 C), and -200 F (-129 C): (1) tensile test (Ultimate, yield, modulus, elongation, and reduction of area), (2) notched tensile test, (3) charpy V-notched impact test (impact energy), and (4) double shear strength test (ultimate and yield). The test data indicate excellent tensile strength, notched/unnotched tensile ratios, ductility, impact, and shear properties at all test temperatures, except at -200 F (-129 C) where the impact strength of the higher strength group of alloy steels, 4130 (Rc-37) and 4140 (Rc-44) decreased to approximately 9 ft. lbs. (12 joules) and 6 ft. lbs. (8 joules), respectively. Chemical, metallographic, and fractographic analyses were also performed to evaluate microstructure, microhardness and the effect of decrease in temperature on the ductile to brittle failure transition.

Montano, J. W.↗

Factors affecting the strength of multipass low-alloy steel weld metal

The mechanical properties of multipass high-strength steel weld metals depend upon several factors, among the most important being: (1) The interaction between the alloy composition and weld metal cooling rate which determines the as-deposited microstructure; and (2) the thermal effects of subsequent passes on each underlying pass which alter the original microstructure. The bulk properties of a multipass weld are therefore governed by both the initial microstructure of each weld pass and its subsequent thermal history. Data obtained for a high strength low alloy steel weld metal confirmed that a simple correlation exists between mechanical properties and welding conditions if the latter are in turn correlated as weld cooling rate.

Krantz, B. M.↗

Crack growth in ASME SA-105 grade 2 steel in hydrogen at ambient temperature

Cyclic-load crack growth measurements were performed on ASME SA-105 Grade 2 steel specimens exposed to 10,000- and 15,000-psi hydrogen and to 5000-psi helium, all at ambient temperatures. The cyclic-load crack growth rate was found to be faster in high-pressure hydrogen than in helium. Cyclic-load crack growth rates in this steel were not reduced by preloading in air to a stress intensity of 1.5 times the cyclic K sub max in hydrogen. There are indications that holding under load in hydrogen, and loading and unloading in helium retards hydrogen-accelerated cyclic-load crack growth. Cyclic frequency and R (ratio of K sub min/k sub max) were important variables determining crack growth rate. The crack growth rate increased as a logarithm of the cycle duration and decreased with increasing R.

Walter, R. J.↗

Fracture under combined modes in 4340 steel

An experimental investigation was conducted to study the interaction of combined modes of loading on crack instability in the presence of the opening and sliding modes of stress intensity factors, the opening and tearing modes of stress intensity factors, and all three modes of stress intensity factors. Through-cracked and surface-cracked flat and round specimens, and round notched bar specimens fabricated from high strength 4340 steel were used for the investigation. The results are evaluated to determine fracture criteria under the combined modes of stress intensity factors for the 4340 steel. These results are compared with the results of other investigators obtained for different materials.

Shah, R. C.↗

Diffusion brazing nickel-plated stainless steel

To bond parts, sandwich assembly is made up of aluminum core, aluminum face sheet with brazing alloy interface, and nickel plated stainless steel part. Sandwich is placed between bottom and top glide sheet that is placed in stainless steel retort where assembly is bonded at 580 C.

Beuyukian, C. S.↗

Experimental transient and permanent deformation studies of steel-sphere-impacted or impulsively-loaded aluminum beams with clamped ends

The sheet explosive loading technique (SELT) was employed to obtain elastic-plastic, large-deflection transient and/or permanent strain data on simple well-defined structural specimens and materials: initially-flat 6061-T651 aluminum beams with both ends ideally clamped via integral construction. The SELT loading technique was chosen since it is both convenient and provides forcing function information of small uncertainty. These data will be useful for evaluating pertinent structural response prediction methods. A second objective was to obtain high-quality transient-strain data for a well-defined structural/material model subjected to impact by a rigid body of known mass, impact velocity, and geometry; large-deflection, elastic-plastic transient response conditions are of primary interest. The beam with both ends clamped and a steel sphere as the impacting body were chosen. The steel sphere was launched vertically by explosive propulsion to achieve various desired impact velocities. The sphere/beam impact tests resulted in producing a wide range of structural responses and permanent deformations, including rupture of the beam from excessive structural response in two cases. The transient and permanent strain data as well as the permanent deflection data obtained are of high quality and should be useful for checking and evaluating methods for predicting the responses of simple 2-d structures to fragment (sphere) impact. Transient strain data very close to the point of impact were not obtained over as long a time as desirable because the gage(s) in that region became detached during the transient response.

Witmer, E. A.↗

Mechanical properties of low-nickel stainless steel

Demand for improved corrosion-resistant steels, coupled with increased emphasis on conserving strategic metals, has led to development of family of stainless steels in which manganese and nitrogen are substituted for portion of usual nickel content. Advantages are approximately-doubled yield strength in annealed condition, better resistance to stress-corrosion cracking, retention of low magnetic permeability even after severe cold working, excellent strength and ductility at cryogenic temperatures, superior resistance to wear and galling, and excellent high-temperature properties.

Montano, J. W.↗

Effect of ion-plated films of germanium and silicon on friction, wear, and oxidation of 52100 bearing steel

Friction and wear experiments were conducted with ion plated films of germanium and silicon on the surface of 52100 bearing steel both dry and in the presence of mineral oil. Both silicon and germanium were found to reduce wear, with germanium being more effective than silicon. An optimum film thickness of germanium for minimum wear without surface crack formation was found to be approximately 400 nanometers (4000 A). The presence of silicon and germanium on the 52100 bearing steel surface improved resistance to oxidation.

Buckley, D. H.↗

Oxidation and corrosion behavior of modified-composition, low-chromium 304 stainless steel alloys

The effects of substituting less strategic elements than Cr on the oxidation and corrosion resistance of AISI 304 stainless steel were investigated. Cyclic oxidation resistance was evaluated at 870 C. Corrosion resistance was determined by exposure of specimens to a boiling copper-rich solution of copper sulfate and sulfuric acid. Alloy substitutes for Cr included Al, Mn, Mo, Si, Ti, V, Y, and misch metal. A level of about 12% Cr was the minimum amount of Cr required for adequate oxidation and corrosion resistance in the modified composition 304 stainless steels. This represents a Cr saving of at least 33%. Two alloys containing 12% Cr and 2% Al plus 2% Mo and 12% Cr plus 2.65% Si were identified as most promising for more detailed evaluation.

Stephens, J. R.↗

Evaluation and control of environmental corrosion for aluminum and steel alloys

Corrosion protection systems for aerospace application and the effects of surface treatments and methods of controlling stress corrosion are evaluated. Chromate pigmented systems were found to be most effective for aluminum alloys; zinc-rich coatings gave the greatest protection to steel alloys. Various steel and aluminum alloys are rated for stress corrosion resistance.

Franklin, D. B.↗

Cross sections for He and Ne isotopes in natural Mg, Al, and Si, He isotopes in CaF2, Ar isotopes in natural Ca, and radionuclides in natural Al, Si, Ti, Cr, and stainless steel induced by 12- to 45-MeV protons

Stacks of thin Mg, Al, Si, Ca, CaF2, Ti, and stainless steel foils were bombarded in twelve irradiations by a variable energy cyclotron. Cross sections are reported for He and Ne in natural Mg, Al, and Si, and for He in CaF2, and for Ar in natural Ca, as determined from mass spectrometer analysis of the inert gases. In addition, cross sections of Na-22 in natural Al and Si, of V-48 in natural Ti, and of Cr-51, Mn-52, and Co-57 in stainless steel are reported. From these were deduced Cr-51 and Mn-52 cross sections in natural Cr.

Walton, J. R.↗

Fractography of the high temperature hydrogen attack of a medium carbon steel

Results are reported for an experimental study of the microscopic fracture processes associated with hydrogen attack of a commercially produced plain carbon steel in a well-controlled high-temperature hydrogen environment of high purity. In the experiments, sheet samples were exposed to laboratory-grade hydrogen at a pressure of 3.5 MN/sq m and a temperature of 575 C. The fractography of gas-filled fissures and failed tension specimens is analyzed in an effort to identify any predominant microstructural defect associated with fissure formation, the prevalent modes of fracture, and the contribution of gas-filled fissures to the overall failure process. It is found that the tensile properties of the examined steel were significantly degraded after as few as 136 hr of exposure to a high-purity hydrogen atmosphere at 575 C; that the yield strength, ultimate strength, and elongation at fracture were all reduced progressively with increasing exposure time; and that the yield and ultimate strengths were reduced more than 40% after 408 hr while elongation was reduced to less than 2%.

Nelson, H. G.↗

Wear formulation for aircraft brake material sliding against steel

Predictions of wear on contemporary copper-based brake material sliding against 17-22 AS grade steel, wear testing equipment, formulation of wear, and test results are discussed. An initial investigation of worn surfaces of the brake material and a mating steel rotor was carried out. A wear model proposed suggests initiation of cracks at a hard particle inclusion site in the surface layer of the brake material; crack propagation allows particles to be removed by intersection of cracks. Mutual relations between sliding variables, load, time, hardness, and surface temperature are studied. Empirical formulas are exhibited.

Ho, T. L.↗

Low-chromium stainless steels

Two modified stainless-steel formulations, with only two-thirds chromium content found in conventional type 304, have mechanical and chemical properties comparable to type 304. Low-chromium stainless steels have potential uses in heat exchangers, transfer lines for chemicals, automobile trim, and other applications.

Barrett, C. A.↗

High-temperature brazing of stainless steel

Prevention of iron contamination of platens is eliminated by placing alumina/silica ceramic-fiber blankets between platens and carbon-steel plate. Carbon-steel plates provide rigidity and improve heat transfer.

Beuyukian, C. S.↗

Forming "dynamic" membranes on stainless steel

"Dynamic" zirconium polyacrylic membrane is formed directly on stainless steel substrate without excessive corrosion of steel. Membrane is potentially useful in removal of contaminated chemicals from solution through reversed osmosis. Application includes use in filtration and desalination equipment, and in textile industry for separation of dyes from aqueous solvents.

Brandon, C. A.↗

Nine percent nickel steel heavy forging weld repair study

The feasibility of making weld repairs on heavy section 9% nickel steel forgings such as those being manufactured for the National Transonic Facility fan disk and fan drive shaft components was evaluated. Results indicate that 9% nickel steel in heavy forgings has very good weldability characteristics for the particular weld rod and weld procedures used. A comparison of data for known similar work is included.

Young, C. P., Jr.↗