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NASA NTRS2020

Lunar Dust Simulant Particle Adhesion on Copolyimide Alkyl Ethers

Mitigation of lunar dust contamination is one of the greatest challenges to be overcome to realize a sustained lunar presence. Likely solutions will integrate active mitigation strategies, requiring the input of external energy, and passive materials, exhibiting an intrinsic resistance to lunar dust adhesion. In this work, a series of copolyimide alkyl ethers containing per fluorinated side-chains were generated to evaluate the influence surface modification agents have on surface chemical, topographical, and mechanical properties. An expanded testing protocol to characterize the adhesion interaction between lunar dust simulant and the copolyimide substrate was carried out. The interfacial adhesion strength was in-situ measured by a custom-built particulate adhesion instrument, utilizing a sonic wand. Surface mechanical properties were characterized by nanoindentation, utilizing the continuous stiffness measurement approach. A nominal presence of surface modifying agents, 1 wt%, resulted in a six-fold reduction in adhesion strength of the interface. A strong inverse correlation between the adhesion strength and Young’s modulus of the substrate was identified. The reduction was attributed to a synergistic interaction between the surface energy, surface roughness, and modulus of the copolyimide alkyl ethers film.

Lunar Dust, Particulate Adhesion, Surface Migratio↗

NASA NTRS2000

International Agreement on Planetary Protection

The maintenance of a NASA policy, is consistent with international agreements. The planetary protection policy management in OSS, with Field Center support. The advice from internal and external advisory groups (NRC, NAC/Planetary Protection Task Force). The technology research and standards development in bioload characterization. The technology research and development in bioload reduction/sterilization. This presentation focuses on: forward contamination - research on the potential for Earth life to exist on other bodies, improved strategies for planetary navigation and collision avoidance, and improved procedures for sterile spacecraft assembly, cleaning and/or sterilization; and backward contamination - development of sample transfer and container sealing technologies for Earth return, improvement in sample return landing target assessment and navigation strategy, planning for sample hazard determination requirements and procedures, safety certification, (liaison to NEO Program Office for compositional data on small bodies), facility planning for sample recovery system, quarantine, and long-term curation of 4 returned samples.

Source record↗

NASA NTRS1999

Simple model for the reconstruction of radionuclide concentrations and radiation exposures along the Techa River

The Techa River (Southern Urals, Russia) was contaminated in 1949-1956 by liquid radioactive wastes from the Mayak complex, the first Russian facility for the production of plutonium. The measurements of environmental contamination were started in 1951. A simple model describing radionuclide transport along the free-flowing river and the accumulation of radionuclides by bottom sediments is presented. This model successfully correlates the rates of radionuclide releases as reconstructed by the Mayak experts, hydrological data, and available environmental monitoring data for the early period of contamination (1949-1951). The model was developed to reconstruct doses for people who lived in the riverside communities during the period of the releases and who were chronically exposed to external and internal irradiation. The model fills the data gaps and permits reconstruction of external gamma-exposure rates in air on the river bank and radionuclide concentrations in river water used for drinking and other household needs in 1949-1951.

Non-NASA Center↗

NASA NTRS2022

Environmental Testing of Contamination Sensitive Instruments and Optics in Non-Cleanliness Controlled Facilities

The James Webb Space Telescope (JWST) Optical Telescope Element + Integrated Science Instrument Module (OTIS) went through environmental testing at the Goddard Space Flight Center. The vibration and acoustic tests occurred outside of cleanrooms. These areas are typically around ISO Class 8, far out of specifications for JWST. Through collaboration between the OTIS Mechanical and Contamination Engineering teams, a portable clean enclosure was designed, built, and verified to prevent contamination of the sensitive OTIS assembly. This manuscript describes the process of designing and building this enclosure, including materials selection and High Efficiency Particle Air (HEPA) filtration. This enclosure also provided environmental control with a portable air conditioning unit to control the relative humidity level enabling personnel to work within it. The manuscript emphasizes working in a systematic order to maintain cleanliness and integrity. “Clean as you go” during construction was a top priority to ensure that this critical Ground Support Equipment (GSE) was acceptable. The process of installing the walls and then sealing their internal and external surfaces with approved films was critical to maintaining OTIS integrity. This proved important because OTIS was in the enclosure for months longer than originally planned. This manuscript concludes by reviewing the process used to verify that the OTIS clean enclosure could achieve acceptable contamination level fallout accumulation for use during the vibration and acoustic testing and then verifying that the predicted performance was achieved after testing was complete.

Contamination Control, James Webb Space Telescope,↗

NASA NTRS1974

External insulation systems for cryogenic storage systems. Volume 1: Optical properties of Kapton and report of process variable study

Investigations are conducted into the optical properties of the glass and Kapton substrate materials, and three variables were chosen: deposition rate, sputter gas pressure, and film contamination time. Substrate tests have shown that fabrication of an dielectric broadband reflector would require an extremely complex and expensive filter design.

Frank, A. M.↗

NASA NTRS2011

Discovery and Identification of Dimethylsilanediol as a Contaminant in ISS Potable Water

In September 2010, analysis of ISS potable water samples was undertaken to determine the contaminant(s) responsible for a rise of total organic carbon (TOC) in the Water Processor Assembly (WPA) product water. As analysis of the routine target list of organic compounds did not reveal the contaminant, efforts to look for unknown compounds were initiated, resulting in discovery of an unknown peak in the gas chromatography/mass spectrometry (GC/MS) analysis for glycols. A mass spectrum of the contaminant was then generated by concentrating one of the samples and analyzing it by GC/MS in full-scan mode. Although a computer match of the compound identity could not be obtained with the instrument database, a search with a more up-to-date mass spectral library yielded a good match with dimethylsilanediol (DMSD). Inductively coupled plasma/mass spectrometry (ICP/MS) analyses showed abnormally high silicon levels in the samples, confirming that the unknown compound(s) contained silicon. DMSD was then synthesized to confirm the identification and provide a standard to develop a calibration curve. Further confirmation was provided by external direct analysis in real time time of flight (DART TOF) mass spectrometry. To routinely test for DMSD in the future, a quantitative method was needed. A preliminary GC/MS method was developed and archived samples from various locations on ISS were analyzed to determine the extent of the contamination and provide data for troubleshooting. This paper describes these events in more detail as well as problems encountered in routine GC/MS analyses and the subsequent development of high performance liquid chromatography and LC/MS/MS methods for measuring DMSD.

Rutz, Jeffrey A.↗

NASA NTRS2018

A Prototype Tool for Assessing Forward Contamination from Space Suits

Crewed exploration missions dramatically increase the capability for large-scale sample collection and return activities, but they also increase the possibility and likelihood of forward contamination. Systematic research on forward contamination from uncrewed spacecraft has steadily progressed since the Viking missions, but parallel research on contamination from space suits has not. Current space suits have leakage rates as high as 100 cc gas/min., but it is unclear how many or what types of microbes are exiting the suits along with this gas. The Human Forward Contamination Assessment team at NASA's Johnson Space Center (JSC) has developed a prototype swab tool that is capable of maintaining sterility during pressure changes associated with entering and exiting vacuum. The primary objective of recent Extravehicular Activity (EVA) Swab Kit testing is to characterize the type of microorganisms typically found on spacesuit external surfaces under suit differential pressure conditions. Most human-associated microorganisms can fit through a 0.5 to 1.0 μm gap. Understanding potential leak paths will inform future hardware design decisions. Knowing which types of microorganisms may leak from EVA suits provides a basis for subsequent studies to characterize the viability of those organisms under destination conditions, as well as how far they might spread through natural or human-influenced processes. The results of EVA suit molecular microbial community analyses will inform NASA exploration mission operations and hardware design, and help close Strategic Knowledge Gap B5, Forward Contamination to Mars.

Rucker, M.↗

NASA NTRS1966

Bio-Medical Factors and External Hazards in Space Station Design

The design of space-station configurations is influenced by many factors. Probably the most demanding and critical are the biomedical and external hazards requirements imposed to provide the proper environment and supporting facilities for the crew and the adequate protective measures necessary to provide a configuration'in which the crew can live and work efficiently in relative comfort and safety. The major biomedical factors, such as physiology, psychology, nutrition, personal hygiene, waste management, and recreation, all impose their own peculiar requirements. The commonality and integration of these requirements demand the utmost ingenuity and inventiveness be exercised in order to achieve effective configuration compliance. The relationship of biomedical factors for the internal space-station environment will be explored with respect to internal atmospheric constituency, atmospheric pressure levels, oxygen positive pressure, temperature, humidity, CO2 concentration, and atmospheric contamination. The range of these various parameters and the recommended levels for design use will be analyzed. Requirements and criteria for specific problem areas such as zero and artificial gravity and crew private quarters will be reviewed and the impact on the design of representative solutions will be presented. In the areas of external hazards, the impact of factors such as meteoroids, radiation, vacuum, temperature extremes, and cycling on station design will be evaluated. Considerations with respect to operational effectiveness and crew safety will be discussed. The impact of such factors on spacecraft design to achieve acceptable launch and reentry g levels, crew rotation intervals, etc., will be reviewed.

Olling, E. H.↗

NASA NTRS1966

Bio-Medical Factors and External Hazards in Space Station Design

The design of space-station configurations is influenced by many factors, Probably the most demanding and critical are the biomedical and external hazards requirements imposed to provide the proper environment and supporting facilities for the crew and the adequate protective measures necessary to provide a configuration in which the crew can live and work efficiently in relative comfort and safety. The major biomedical factors, such as physiology, psychology, nutrition, personal hygiene, waste management, and recreation, all impose their own peculiar requirements. The commonality and integration of these requirements demand the utmost ingenuity and inventiveness be exercised in order to achieve effective configuration compliance. The relationship of biomedical factors for the internal space-station environment will be explored with respect to internal atmospheric constituency, atmospheric pressure levels, oxygen positive pressure, temperature, humidity, CO2 concentration, and atmospheric contamination. The range of these various parameters and the recommended levels for design use will be analyzed. Requirements and criteria for specific problem areas such as zero and artificial gravity and crew private quarters will be reviewed and the impact on the design of representative solutions will be presented. In the areas of external hazards, the impact of factors such as meteoroids, radiation, vacuum, temperature extremes, and cycling on station design will be evaluated. Considerations with respect to operational effectiveness and crew safety will be discussed. The impact of such factors on spacecraft design to achieve acceptable launch and reentry g levels, crew rotation intervals, etc., will be reviewed. Examples of configurations, subsystems, and internal a arrangement and installations to comply with such biomedical factor requirements will ber presented. The effects of solutions to certain biomedical factors on configuration weight, operational convenience, and program costs will be compared.

Olling, Edward H.↗

NASA NTRS1995

Ices on the Satellites of Jupiter, Saturn, and Uranus

Three satellites of Jupiter, seven satellites of Saturn, and five satellites of Uranus show spectroscopic evidence of H2O ice on their surfaces, although other details of their surfaces are highly diverse. The icy surfaces contain contaminants of unknown composition in varying degrees of concentration, resulting in coloration and large differences in albedo. In addition to H2O, Europa has frozen SO2, and Ganymede has O2 in the surface; in both of these cases external causes are implicated in the deposition or formation of these trace components. Variations in ice exposure across the surfaces of the satellites are measured from the spectroscopic signatures. While H2O ice occurs on the surfaces of many satellites, the range of bulk densities of these bodies shows that its contribution to their overall compositions is highly variable from one object to another.

Cruikshank, Dale P.↗

NASA NTRS1999

Review of historical monitoring data on Techa River contamination

The Mayak Production Association was the first Russian site for the production and separation of plutonium. The extensive increase in plutonium production during 1948-1955, as well as the absence of reliable waste-management technology, resulted in significant releases of liquid radioactive effluent into the rather small Techa River. This resulted in chronic external and internal exposure of about 30,000 residents of riverside communities; these residents form the cohort of an epidemiologic investigation. Analysis of the available historical monitoring data indicates that the following reliable data sets can be used for reconstruction of doses received during the early periods of operation of the Mayak Production Association: Temporal pattern of specific beta activity of river water for several sites in the upper Techa region since July 1951; average annual values of specific beta activity of river water and bottom sediments as a function of downstream distance for the whole river since 1951; external gamma-exposure rates near the shoreline as a function of downstream distance for the whole Techa River since 1952; and external gamma-exposure rate as a function of distance from the shoreline for several sites in the upper and middle Techa since 1951.

NASA Discipline Radiation Health↗

NASA NTRS1997

An OSEE Based Portable Surface Contamination Monitor

Many industrial and aerospace processes involving the joining of materials, require sufficient surface cleanliness to insure proper bonding. Processes as diverse as painting, welding, or the soldering of electronic circuits will be compromised if prior inspection and removal of surface contaminants is inadequate. As process requirements become more stringent and the number of different materials and identified contaminants increases, various instruments and techniques have been developed for improved inspection. One such technique based on the principle of Optically Stimulated Electron Emission (OSEE) has been explored for a number of years as a tool for surface contamination monitoring. Some of the benefits of OSEE are: it's non-contacting; requires little operator training; and has very high contamination sensitivity. This paper describes the development of a portable OSEE based surface contamination monitor. The instrument is suitable for both hand-held and robotic inspections with either manual or automated control of instrument operation. In addition, instrument output data is visually displayed to the operator and may be output to an external computer for archiving or analysis.

Perey, Daniel F.↗

NASA NTRS1996

A Portable Surface Contamination Monitor Based on the Principle of Optically Stimulated Electron Emission (OSEE)

Many industrial and aerospace processes involving the joining of materials, require sufficient surface cleanliness to insure proper bonding. Processes as diverse as painting, welding, or the soldering of electronic circuits will be compromised if prior inspection and removal of surface contaminants is inadequate. As process requirements become more stringent and the number of different materials and identified contaminants increases, various instruments and techniques have been developed for improved inspection. One such technique, based on the principle of Optically Stimulated Electron Emission (OSEE), has been explored for a number of years as a tool for surface contamination monitoring. Some of the benefits of OSEE are: it is non-contacting; requires little operator training; and has very high contamination sensitivity. This paper describes the development of a portable OSEE based surface contamination monitor. The instrument is suitable for both hand-held and robotic inspections with either manual or automated control of instrument operation. In addition, instrument output data is visually displayed to the operator and may be sent to an external computer for archiving or analysis.

Perey, D. F.↗

NASA NTRS2011

External Surface Changes Observed on the International Space Station (ISS) Through 2010

Some worse-than-expected materials degradation effects have been observed, but none have created any operational issues and some hardware (as with the anodized aluminum labels) appear to be recovering. Inadvertent materials substitutions have been observed, but none have created any operational issues. Hardware handling contamination effects have been observed, and although none have created operational issues, there is clearly room for improvement in this regard. Even with robust materials selections, space environmental effects will be observed. Be cautious when interpreting on-orbit photography, as lighting conditions and the space environment affect imaging.

Golden, J. L.↗

NASA NTRS1990

Dissociation phenomena in electron-beam sustained carbon dioxide lasers

A number of applications are emerging requiring efficient, long pulse, long-life sealed CO2 lasers. Examples include the proposed NASA and ESA wind lidars. Electron-beam sustained discharge devices are strong contenders. Unlike self-sustained discharges, e-beam sustenance readily provides efficient performance from large volume discharges and offers pulse lengths well in excess of the microsecond or so generally associated with self-sustained devices. In the case of the e-beam sustained laser, since the plasma is externally maintained and operated at electric field strengths less than that associated with the glow to arc transition, the discharges can be run even in the presence of strongly attacking species such as O2. Build up of large levels of attacking contaminants is nevertheless undesirable as their presence reduces the current drawn by the plasma and thus the pumping rate to the upper laser level. The impedance rise leads to a mismatch of the pulse forming network with a consequent loss of control over energy deposition, operating E/N, and gain. Clearly CO2 dissociation rates, the influence of dissociation products on the discharge and gain, and tolerance of the discharge to these products need to be determined. This information can then be used to assess co-oxidation catalyst requirements for sealed operation.

Harris, Michael R.↗

NASA NTRS2010

Examination of Icing Induced Loss of Control and Its Mitigations

Factors external to the aircraft are often a significant causal factor in loss of control (LOC) accidents. In today s aviation world, very few accidents stem from a single cause and typically have a number of causal factors that culminate in a LOC accident. Very often the "trigger" that initiates an accident sequence is an external environment factor. In a recent NASA statistical analysis of LOC accidents, aircraft icing was shown to be the most common external environmental LOC causal factor for scheduled operations. When investigating LOC accident or incidents aircraft icing causal factors can be categorized into groups of 1) in-flight encounter with super-cooled liquid water clouds, 2) take-off with ice contamination, or 3) in-flight encounter with high concentrations of ice crystals. As with other flight hazards, icing induced LOC accidents can be prevented through avoidance, detection, and recovery mitigations. For icing hazards, avoidance can take the form of avoiding flight into icing conditions or avoiding the hazard of icing by making the aircraft tolerant to icing conditions. Icing detection mitigations can take the form of detecting icing conditions or detecting early performance degradation caused by icing. Recovery from icing induced LOC requires flight crew or automated systems capable of accounting for reduced aircraft performance and degraded control authority during the recovery maneuvers. In this report we review the icing induced LOC accident mitigations defined in a recent LOC study and for each mitigation describe a research topic required to enable or strengthen the mitigation. Many of these research topics are already included in ongoing or planned NASA icing research activities or are being addressed by members of the icing research community. These research activities are described and the status of the ongoing or planned research to address the technology needs is discussed

Reehorst, Andrew L.↗

NASA NTRS1985

Detecting supernova remnants in external galaxies

Identification of supernova remnants (SNR) in external galaxies through the combined use of radio, optical and X-ray surveys is discussed. Some 24 likely distant galaxy SNR have been found in the past six years, though confirmation is often difficult. Radio surveys of other galaxies are restricted by background object contamination in the field, and confirmation of these candidates requires other techniques. Optical measurement of the ratio of the forbidden SII doublet at .6717 and .6731 microns to H-alpha, followed by spectroscopic or radio confirmation, has successfully identified SNR in the LMC and other galaxies, though few in number. Most of the SNR in the Magellanic Clouds have been detected as X-ray emitters, but towards M31 there are no coincidences between the lists of optical SNR and X-ray sources. An increase in SNR identifications should result from use of the Space Telescope and continued use of the VLA.

Dickel, J. R.↗

NASA NTRSDate not supplied

ISS External Microorganisms: A Payload to Close Planetary Protection Knowledge Gaps for Crewed Missions

Before NASA or COSPAR is able to set planetary protection requirements for crewed missions to locations like Mars there are a number of critical knowledge gaps that must be addressed (1). One of the most important knowledge gaps is an understanding of microbial leakage from crewed habitats and space suits. Current ECLSS (Environmental Control and Life Support System) and PLSS (Portable Life Support System) requirements do not include any provisions to control microbes that may escape along with vented or leaked gasses. The current generation of NASA space suits can leak at rates as high as 100 cm2 /min. during nominal operation (2). ISS (International Space Station) intentionally vents atmospheric gases like CO2 to maintain habitable conditions for the crew. Furthermore, every time an airlock is used for EVA (extravehicular activity)there is an accompanying release of internal atmosphere. Since it is not possible to sterilize a crewed mission, it is important that we understand what if any microbes are entrained in these vented and leaked products. It is also important to understand if these microbes can survive on exterior surfaces. Recent sampling of the Russian segments of ISS suggest that bacteria and fungi from inside ISS may be capable of surviving on external surfaces(3). NASA is developing an aseptic sampling tool for use during EVA and plans to collect samples from vents on ISS to build on these results. The results of this work will be used to develop planetary protection requirements for vented and leaked gasses from crewed volumes. NASA has developed and tested a tool kit for collecting microbiological samples during EVA(4). This tool kit contains eight commercially available, 23 mm. diameter, foam swabs that can be used to aseptically collect samples while at vacuum. The swabs are individually housed in aluminum canisters that are equipped with 0.2 μm Teflon filters. These filters allow the canisters to equilibrate to pressure changes while preventing microbiological contamination. The canisters will be cleaned and sterilized before flight. Results from ground-based testing indicate that this tool kit is capable of aseptically collecting microbes while at vacuum without becoming contaminated during pressure changes(5). Based on the results of this ground testing we have modified the tool kit to meet NASA safety requirements and improve the ergonomics. We added additional mounting points to the tool kit to give astronauts more options for securing it during use. We also changed the opening mechanism to improve the precision with which swabs can be extracted from the tool kit. We plan to use this kit on an upcoming EVA to collect samples from non-propulsive vents and areas near the U.S. airlock on ISS. These samples will be frozen at -80 ̊C and stored on station until they can be returned to Earth. We will analyze these returned samples using next generation DNA sequencing to determine the community composition and function of external ISS environments. The results of this study will close planetary protection knowledge gaps for crewed missions and will help NASA determine appropriate planetary protection requirements for life support systems. The tool kit will also be useful for collecting aseptic samples on upcoming crewed or robotic missions and could easily be modified to collect samples with organic contamination control requirements as well.

A B Regberg↗