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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 145 records · Page 8
All sourcesNASA NTRSDOE OSTI
DOE OSTI2018

A peridynamic failure analysis of fiber-reinforced composite laminates using finite element discontinuous Galerkin approximations

Here, this paper presents a discontinuous Galerkin weak form for bond-based peridynamic models to predict the damage of fiber-reinforced composite laminates. To represent the anisotropy of a laminate in a peridynamic model, a lamina is simplified as a transversely isotropic medium under a plane stress condition. The laminated structure is modeled by stacking the surface mesh layers along the thickness direction according to the laminate sequence. To avoid a mesh dependence on either the fiber orientation or the discretization, the spherical harmonic expansion theory is employed to construct a function for the micro-elastic modulus in terms of the bond-fiber angle. The laminate material is decomposed into an isotropic matrix material part and a transversely isotropic material part. The bond stiffness can be evaluated using the engineering material constants, based on the equivalence between the elastic energy density in the peridynamic theory and the elastic energy density in the classic continuum mechanics theory. Benchmark tests are conducted to verify the proposed model. Numerical results illustrate that the convergence of simulations with different horizon sizes and meshes can be achieved. In terms of damage analysis, the proposed model can capture the dynamic process of the complex coupling of the inner-layer and delamination damage modes.

42 ENGINEERING↗
DOE OSTI2023

In-Situ X-Ray Imaging High Strain Rate Compression of Laminate Al-Graphene Composite and Mechanical Property Characterization

Owing to the opaque nature of the laminated structures, traditional high-speed optical camera cannot be used to detect the dynamic process of sub-surface deformation. In this article, we report a study of using high speed X-ray imaging to study the high strain rate deformation in laminated Al structures. We used a Kolsky bar apparatus to apply dynamic compression and a high-speed synchrotron X-ray phase contrast imaging (PCI) setup to conduct the in situ X-ray imaging study. The in situ X-ray imaging captures the shock wave propagation in the laminated structures. After shock compression, we characterized the microstructures by using transmission electron microscopy (TEM), which demonstrates an increase of dislocation density. In conclusion, the micro-pillar compression tests show that the yield strength at 0.2% offset of laminated Al-graphene composite has a significant increase of 67%, from 30 to 50 MPa, compared to laminate Al after shock loading.

36 MATERIALS SCIENCE↗
DOE OSTI2024

Self-healing carbon fiber/epoxy laminates with particulate interlayers of a low-melting-point alloy

In order to prolong the service life of fiber-reinforced polymer composites, the implementation of self-healing ability with the micro-encapsulated healing agent has been extensively studied. However, such microcapsule-based self-healing composites typically suffer from degraded mechanical properties due to the liquid-phase inclusions, thereby limiting their proliferation. Here, in this study, a low-melting-point alloy is utilized as the particulate inclusions of carbon fiber/epoxy laminated composites. Field's Metal particles (melting point: 62 °C) are distributed between woven carbon fiber preforms followed by the resin impregnation to realize laminated composites with a Field's Metal-enhanced interlayer(s). The resulting laminated composites demonstrate the autonomic repair of interlaminar failure with a 40 % of healing efficiency. Most of all, the mechanical properties of these self-healing laminated composites are comparable to the conventional laminated composites attributed to the rigid inclusions that can be compressed to increase the fiber volume. Since the Field's Metal particle inclusions can bestow polymer composites with self-healing ability and the potential increase in mechanical properties, Field's Metal-enhanced fiber-reinforced polymer composites are expected to unlock the practical utility of self-healing composites.

A. polymer-matrix composites (PMCs)↗
DOE OSTI2014

Wettability of graphene-laminated micropillar structures

The wetting control of graphene is of great interest for electronic, mechanical, architectural, and bionic applications. In this study, the wettability of graphene-laminated micropillar structures was manipulated by changing the height of graphene-laminated structures and employing the trichlorosilane (HDF-S)-based self-assembly monolayer. Graphene-laminated micropillar structures with HDF-S exhibited higher hydrophobicity (contact angle of 129.5°) than pristine graphene thin film (78.8°), pristine graphene-laminated micropillar structures (97.5°), and HDF-S self-assembled graphene thin film (98.5°). Wetting states of the graphene-laminated micropillar structure with HDF-S was also examined by using a urea solution, which flowed across the surface without leaving any residues.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2015

Lamination of organic solar cells and organic light emitting devices: Models and experiments

In this paper, a combined experimental, computational, and analytical approach is used to provide new insights into the lamination of organic solar cells and light emitting devices at macro- and micro-scales. First, the effects of applied lamination force (on contact between the laminated layers) are studied. The crack driving forces associated with the interfacial cracks (at the bi-material interfaces) are estimated along with the critical interfacial crack driving forces associated with the separation of thin films, after layer transfer. The conditions for successful lamination are predicted using a combination of experiments and computational models. Guidelines are developed for the lamination of low-cost organic electronic structures.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2015

A large genomic deletion leads to enhancer adoption by the lamin B1 gene: a second path to autosomal dominant adult-onset demyelinating leukodystrophy (ADLD)

Chromosomal rearrangements with duplication of the lamin B1 (LMNB1) gene underlie autosomal dominant adult-onset demyelinating leukodystrophy (ADLD), a rare neurological disorder in which overexpression of LMNB1 causes progressive central nervous system demyelination. However, we previously reported an ADLD family (ADLD-1-TO) without evidence of duplication or other mutation in LMNB1 despite linkage to the LMNB1 locus and lamin B1 overexpression. By custom array-CGH, we further investigated this family and report here that patients carry a large (~660 kb) heterozygous deletion that begins 66 kb upstream of the LMNB1 promoter. Lamin B1 overexpression was confirmed in further ADLD-1-TO tissues and in a postmortem brain sample, where lamin B1 was increased in the frontal lobe. Through parallel studies, we investigated both loss of genetic material and chromosomal rearrangement as possible causes of LMNB1 overexpression, and found that ADLD-1-TO plausibly results from an enhancer adoption mechanism. The deletion eliminates a genome topological domain boundary, allowing normally forbidden interactions between at least three forebrain-directed enhancers and the LMNB1 promoter, in line with the observed mainly cerebral localization of lamin B1 overexpression and myelin degeneration. Finally, this second route to LMNB1 overexpression and ADLD is a new example of the relevance of regulatory landscape modifications in determining Mendelian phenotypes.

59 BASIC BIOLOGICAL SCIENCES↗
DOE OSTI2026

Extended Accelerated Stress Testing of Lamination-Free Edge-Sealed Photovoltaic Minimodules

Lamination-free minimodules are constructed with silicon solar cells between glass sheets and an edge seal of polyisobutylene and silicone. These samples are stressed using a repeated sequential testing sequence including ultraviolet-containing simulated solar spectrum light exposure at elevated temperature, damp heat, humidity freeze, and thermal cycling adapted from the International Electrotechnical Commission (IEC) TS 63209-2:2022. The minimodule performance throughout the stressing is characterized by flash testing and electroluminescence imaging. Results are compared to conventional laminated minimodules using the same type of solar cells. The lamination-free minimodules experience up to 8% power loss compared to roughly 3% for the laminated versions. However, those losses, dominated by current and fill factor, are caused by glass soiling and busbar ribbon separation on the cells. When glass is replaced and the stressed cells are contacted with probes bypassing the delaminated ribbons, the initial performance is recovered, and overall losses of the lamination-free samples become negligible.

14 SOLAR ENERGY↗
DOE OSTI2014

A Quantitative Assessment of Advanced NDI Techniques for Detecting Flaws in Composite Laminate Aircraft Structures. Draft

The aircraft industry continues to increase its use of composite materials, most noteworthy in the arena of principle structural elements. This expanded use, coupled with difficulties associated with damage tolerance analysis of composites, has placed greater emphasis on the application of accurate nondestructive inspection (NDI) methods. Traditionally, a few ultrasonic-based inspection methods have been used to inspect solid laminate structures. Recent developments in more advanced NDI techniques have produced a number of new inspection options. Many of these methods can be categorized as wide area techniques that produce two-dimensional flaw maps of the structure. An experiment has been developed to assess the ability of both conventional and advanced NDI techniques to detect voids, disbonds, delaminations, and impact damage in adhesively bonded composite aircraft structures. A series of solid laminate, carbon composite specimens with statistically relevant flaw profiles are being inspected using conventional, hand-held pulse echo UT and resonance, as well as, new NDI methods that have recently been introduced to improve sensitivity and repeatability of inspections. The primary factors affecting flaw detection in laminates are included in this study: material type, flaw profiles, presence of complex geometries like taper and substructure elements, presence of fasteners, secondarily bonded joints, and environmental conditions. One phase of this effort utilized airline personnel to study Probability of Detection (POD) in the field and to formulate improvements to existing inspection techniques. In addition, advanced NDI methods for laminate inspections — such as thermography, shearography, laser ultrasonics, microwave, and phased/linear array UT — were applied to quantify the improvements achievable through the use of more sophisticated NDI. This report presents the composite laminate experiment design and the POD results for advanced NDI with comparisons to results achieved by airline inspectors using conventional UT methods. A companion report provides the full set of results from the conventional NDI testing.

36 MATERIALS SCIENCE↗
NASA NTRS1974

A method for determining local elastoplastic stress and strain in metallurgically bonded notched laminates subjected to a loading cycle

A semianalytical method was developed for determining elastoplastic cyclic stresses and strains at notch roots in metallurgically bonded metal laminates. The method is based on the Neuber equation, which was used with an effective stress-strain curve for the laminate. It was applied to laminates containing a circular hole which were subjected to one cycle of reversed loading. The laminates consisted of two elasto-perfectly-plastic materials with different yield strengths and with either equal or different Young's moduli. A laminate of high-strength titanium alloy with alternate layers of commercially pure titanium was also analyzed. The accuracy of the method was evaluated by comparing the stresses and strains with those calculated from a finite-element analysis. The results estimated by the simple method based on the Neuber equation agreed closely with the results computed from the more elaborate finite-element analysis.

Sova, J. A.↗
NASA NTRS1975

Lamination residual stresses in fiber composites

An experimental investigation was conducted to determine the magnitude of lamination residual stresses in angle-ply composites and to evaluate their effects on composite structural integrity. The materials investigated were boron/epoxy, boron/polyimide, graphite/low modulus epoxy, graphite/high modulus epoxy, graphite/polyimide and s-glass/epoxy. These materials were fully characterized. Static properties of laminates were also determined. Experimental techniques using embedded strain gages were developed and used to measure residual strains during curing. The extent of relaxation of lamination residual stresses was investigated. It was concluded that the degree of such relaxation is low. The behavior of angle-ply laminates subjected to thermal cycling, tensile load cycling, and combined thermal cycling with tensile load was investigated. In most cases these cycling programs did not have any measurable influence on residual strength and stiffness of the laminates. In the tensile load cycling tests, the graphite/polyimide shows the highest endurance with 10 million cycle runouts at loads up to 90 percent of the static strength.

Daniel, I. M.↗
NASA NTRS1976

A limiting analysis for edge effects in angle-ply laminates

A zeroth order solution for edge effects in angle ply composite laminates using perturbation techniques and a limiting free body approach was developed. The general method of solution for laminates is developed and then applied to the special case of a graphite/epoxy laminate. Interlaminar stress distributions are obtained as a function of the laminate thickness to width ratio h/b and compared to existing numerical results. The solution predicts stable, continuous stress distributions, determines finite maximum tensile interlaminar normal stress for two laminates, and provides mathematical evidence for singular interlaminar shear stresses.

Hsu, P. W.↗
NASA NTRS1976

Effect of laminate construction on residual stresses in composites

The effects of ply stacking sequence and ply orientation on the magnitude of lamination residual stresses in graphite/polyimide angle-ply laminates was studied. Embedded strain gage techniques were used to measure thermal strains in laminates of different layup, and residual strains were determined by comparing thermal strains in the angle-ply laminates with those of a unidirectional laminate. The ply stacking sequence did not have an effect on the magnitude of residual strains.

Daniel, I. M.↗
NASA NTRS1978

Preliminary investigation of crack arrest in composite laminates containing buffer strips

The mechanical properties of some hybrid buffer strip laminates and the crack arrest potential of laminates containing buffer strips were determined. The hybrid laminates consisted of graphite with either S-glass, E-glass, or Kevlar. Unnotched tensile coupons and center-cracked fracture coupons were tested. Elastic properties, complete stress/strain curves, and critical stress intensity values are given. The measured elastic properties compare well with those calculated by classical lamination theory for laminates with linear stress/strain behavior. The glass hybrids had more delamination and higher fracture toughness than the all-graphite or the Kevlar hybrid.

Goree, J. G.↗
NASA NTRS1977

Edge effects in angle-ply composite laminates

This paper presents the results of a zeroth-order solution for edge effects in angle-ply composite laminates obtained using perturbation techniques and a limiting free body approach. The general solution for edge effects in laminates of arbitrary angle ply is applied to the special case of a (+ or - 45)s graphite/epoxy laminate. Interlaminar stress distributions are obtained as a function of the laminate thickness-to-width ratio and compared to finite difference results. The solution predicts stable, continuous stress distributions, determines finite maximum tensile interlaminar normal stress and provides mathematical evidence for singular interlaminar shear stresses in (+ or - 45) graphite/epoxy laminates.

Hsu, P. W.↗
NASA NTRS1977

Fatigue damage of notched boron/epoxy laminates under constant-amplitude loading

Fatigue damage in (0, plus or minus 45) and (0, plus or minus 45, 90) boron/epoxy laminates was studied with X-ray radiography and scanning electron microscopy. In addition, limited tests for residual strength and stiffness were performed. Initially, fatigue damage in both (0, plus or minus 45) and (0, plus or minus 45, 90) laminates occurred as intralaminar cracks around the edge of the hole. Then, whenever further damage developed, intralaminar cracks in the plus or minus 45-deg plies began to propagate from the edge of the hole. Finally, in both types of laminates, primarily plus or minus 45-deg fibers broke (prior to two-piece failure) where intralaminar cracks in the plus or minus 45-deg plies had occurred. In the (0, plus or minus 45) laminates, the 45-deg plies developed intralaminar and transthickness cracks along lines parallel to the loading axis and tangent to the hole in the test specimen. This damage, which was most pronounced under compressive loads, had little effect on either strength or stiffness. In contrast, in the (0, plus or minus 45, 90) laminates, the plus or minus 45-deg plies developed intralaminar cracks transverse to the loading axis.

Roderick, G. L.↗
NASA NTRS1978

A temperature dependent fatigue failure criterion for graphite/epoxy laminates

A fatigue failure criterion applicable to composite materials is developed and applied to predict the fatigue behavior of graphite/epoxy laminates with particular emphasis on the influence of temperature. Tensile stress-strain curves and tension-tension fatigue curves for various unidirectional, angle-ply and symmetrically balanced laminates were developed at test temperatures of 25 C, 74 C, and 114 C. For most laminates a reduction in both static strength and fatigue strength is observed with increasing temperature. This reduction appeared more severe in fatigue loading than in static tensile loading and most severe where the shear stress in the lamina is the dominate failure mode. Through an analytical formulation of shifting functions for the influences of temperature, all fatigue data are shown to be capable of being reduced to a single reference curve at some temperature. Examples are given which demonstrate the capability of the fatigue failure criterion to predict failure of complex symmetrically balanced laminates from relevant parameters obtained from the observed behavior of unidirectional and angle-ply laminates.

Rotem, A.↗
NASA NTRS1979

A temperature dependent fatigue failure criterion for graphite/epoxy laminates

A fatigue failure criterion applicable to composite materials is developed and applied to predict the fatigue behavior of graphite/epoxy laminates with particular emphasis on the influence of temperature. Tensile stress-strain curves and tension-tension fatigue curves for various unidirectional, angle-ply and symmetrically balanced laminates were developed at test temperatures of 25 C, 74 C and 114 C. In general for most laminates a reduction in both static strength and fatigue strength is observed with increasing temperature. This reduction appeared more severe in fatigue loading than in static tensile loading and most severe where the shear stress in the lamina is the dominant failure mode. Through an analytical formulation of shifting functions for the influences of temperature, all fatigue data are shown to be capable of being reduced to a single reference curve at some temperature. Additionally, examples are given which demonstrate the capability of the fatigue failure criterion to predict failure of complex symmetrically balanced laminates from relevant parameters obtained from the observed behavior of unidirectional and angle-ply laminates.

Rotem, A.↗
NASA NTRS1979

Characterization of graphite/epoxy laminates for aeroelastic tailoring

A study of interaction between wing bending and twist by graphite/epoxy anisotropic laminates used in aircraft wing skins is presented. The laminates were used as covers for subscale box beams supported as a cantilever and tested in tip shear and tip torque, measuring beam response with a reflected light technique. The results indicated that the in-plane stiffness properties of anisotropic laminates can be predicted if the layer properties of the composite materials are known; thus, the coupled bending/twist response of wing type structures made from these laminates can be determined provided the limits of the laminate linear behavior are not significantly exceeded.

Shyprykevich, P.↗