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Results for “materials analysis”

Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 145 records · Page 8
All sourcesNASA NTRSDOE OSTI
NASA NTRS1984

Engine cyclic durability by analysis and material testing

The problem of calculating turbine engine component durability is addressed. Nonlinear, finite-element structural analyses, cyclic constitutive behavior models, and an advanced creep-fatigue life prediction method called strainrange partitioning were assessed for their applicability to the solution of durability problems in hot-section components of gas turbine engines. Three different component or subcomponent geometries are examined: a stress concentration in a turbine disk; a louver lip of a half-scale combustor linear; and a squealer tip of a first-stage high-pressure turbine blade. Cyclic structural analyses were performed for all three problems. The computed strain-temperature histories at the critical locations of the combustor linear and turbine blade components were imposed on smooth specimens in uniaxial, strain-controlled, thermomechanical fatigue tests of evaluate the structural and life analysis methods.

Kaufman, A.↗
DOE OSTI2019

XAFS studies on battery materials: Data analysis supported by a chemometric approach

The large amount of data collected during a typical operando X-ray absorption fine structure (XAFS) experiment and the interest to thoroughly investigate and comprehend a redox process occurring in a Li-ion battery need an advanced data analysis approach. In this context, multivariate curve resolution (MCR) has gained attention as chemometric technique that allows the identification of the number of the species and their existence range without any a priori information on the studied system. Herein the call for an advanced data treatment is answered by a joint XAFS-MCR approach, able to unveil the local structural dynamics of the selected species, providing a quick and efficient data interpretation.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2018

A high-throughput data analysis and materials discovery tool for strongly correlated materials

Abstract Modeling of f -electron systems is challenging due to the complex interplay of the effects of spin–orbit coupling, electron–electron interactions, and the hybridization of the localized f -electrons with itinerant conduction electrons. This complexity drives not only the richness of electronic properties but also makes these materials suitable for diverse technological applications. In this context, we propose and implement a data-driven approach to aid the materials discovery process. By deploying state-of-the-art algorithms and query tools, we train our learning models using a large, simulated dataset based on existing actinide and lanthanide compounds. The machine-learned models so obtained can then be used to search for new classes of stable materials with desired electronic and physical properties. We discuss the basic structure of our f -electron database, and our approach towards cleaning and correcting the structure data files. Illustrative examples of the applications of our database include successful prediction of stable superstructures of double perovskites and identification of a number of physically-relevant trends in strongly correlated features of f -electron based materials.

36 MATERIALS SCIENCE↗
DOE OSTI2021

Towards Validation of Advanced Accelerated Stress Testing Protocols through Failure Analysis and Materials Characterization

As the lifetime of photovoltaic modules increases toward the goal of 50 years, accelerated stress testing is critical to assessing the viability of newer, improved, and often cheaper materials in the field. However, the validation of accelerated testing to reproduce field failure has remained elusive. The recent developments of more advanced stress testing protocols utilizing sequential and combined stressors have provided another opportunity for validation. Using a suite of mechanical, chemical, and structural characterization methods we report the development of our approach using a known bad backsheet “AAA.” We then apply this approach to PVDF-based backsheets to further confirm the generalizability of this approach. The outcome of this work is two-fold: (1) validation of advanced accelerated testing protocols which will enable the prediction of field failures in new materials, and (2) deeper insights into the degradation mechanisms observed through the extensive characterization allowing for improved materials engineering and development.

accelerated aging↗
DOE OSTI2018

Updated Erosion Analysis for Material Disposal Area G, Technical Area 54, Los Alamos National Laboratory

Material Disposal Area G (MDA G), located within Technical Area 54 (TA-54) is used to dispose radioactive waste at Los Alamos National Laboratory (LANL). Technical Area 54 is located on LANL property on the Pajarito Plateau between the communities of Los Alamos and White Rock (Figure 1-1). The MDA G disposal facility is currently in operation (Figure 1-2). Waste is generally placed in large rectangular pits, numbered 1-39, and cylindrical shafts within MDA G.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2019

Advanced In-situ Diagnostics for Multicomponent Gas Analysis and Material Aging Part 2: Compact Determination of Hydrogen Isotopes

This report has been accepted for publication in the journal Fusion Science and Technology, in the special issue associated with the Tritium 2016 conference, where the work was presented. Scanning calorimetry of a confined, reversible hydrogen sorbent material has been previously proposed as a method to determine compositions of unknown mixtures of diatomic hydrogen isotopologues and helium. Application of this concept could result in greater process knowledge during the handling of these gases. Previously published studies have focused on mixtures that do not include tritium. This paper focuses on modeling to predict the effect of tritium in mixtures of the isotopologues on a calorimetry scan. The model predicts that tritium can be measured with a sensitivity comparable to that observed for hydrogen-deuterium mixtures, and that under some conditions, it may be possible to determine the atomic fractions of all three isotopes in a gas mixture.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2023

Digital Image Correlation Strain Field Analysis of Materials for Target Systems

Many accelerator facilities are currently being limited in beam power by their target facilities. When exposed to high-energy proton beams, target systems experience radiation damage, mechanical stress, and extreme temperatures, altering their physical properties.For example, due to defects induced in materials by high-energy protons, the physical properties of materials will change during irradiation. Conducting PIEs (Post Irradiation Examinations) can help us understand how the materials can change.Analyzing the strain field across an irradiated sample can help identify where defects have been created, how the hardness of materials have changed, and where they will experience failure.

Ayyildiz, Onat↗
NASA NTRS1991

Ground and space based optical analysis of materials degradation in low-Earth-orbit

There is strong interest in being able to accurately and sensitively monitor materials degradation in both ground-based and space-based environments. Two optical techniques for sensitive degradation monitoring are reviewed: spectroscopic ellipsometry and photothermal spectroscopy. These techniques complement each other in that ellipsometry is sensitive to atomically thin surface and subsurface changes, and photothermal spectroscopy is sensitive to local defects, pin-holes, subsurface defects, and delamination. Progress in applying these spectroscopies (both ex situ and in situ) to atomic oxygen degradation of space materials is reviewed.

Woollam, John A.↗
NASA NTRS1990

Ellipsometric analysis of materials degradation in space

The fundamentals of variable angle spectroscopic ellipsometry (VASE) are reviewed, and its usefulness in studying the effect of atomic oxygen on space coatings such as indium tin oxide (ITO), silicon dioxide, and aluminum oxide is discussed. Monolayer sensitive and nondestructive VASE is found to be an effective technique for monitoring the atomic oxygen diffusion through the aluminum oxide and silicon dioxide protective overcoatings on space reflectors. Ashing of ITO/silicon samples had the net effect of annealing the film inside the plasma. The annealing effect was supported both by structural changes as verified by X-ray diffraction measurements and by increased absorbance in the spectral range below 3 eV as measured by VASE.

Woollam, John A.↗
NASA NTRS1992

LDEF materials data analysis: Representative examples

Results of measurements on silverized teflon, heat shrink tubing and nylon tie downs on the wire harness clamps, silvered hex nuts, and contamination deposits are presented. We interpret the results in terms of our microenvironments exposure model and locations on the Long Duration Exposure Facility (LDEF). Distinct changes in the surface properties of FEP were observed as a function of UV exposure. Significant differences in outgassing characteristics were detected for hardware on the interior row 3 relative to identical hardware on the interior row 3 relative to identical hardware on nearby rows. The implications for in service performance are reviewed.

Pippin, H. Gary↗
NASA NTRS1992

Material nonlinear analysis via mixed-iterative finite element method

The performance of elastic-plastic mixed-iterative analysis is examined through a set of convergence studies. Membrane and bending behaviors are tested using 4-node quadrilateral finite elements. The membrane result is excellent, which indicates the implementation of elastic-plastic mixed-iterative analysis is appropriate. On the other hand, further research to improve bending performance of the method seems to be warranted.

Sutjahjo, Edhi↗