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NASA NTRS1995

Measuring Q And f(sub r) Of A Microwave Cavity: Part I

Method of measuring quality factor (Q) and frequency of resonance (f(subr)) of microwave cavity exploits two inflection points of power-vs.-frequency resonance curve of cavity. Intended particularly for use with microwave cavity in which sample of lossy dielectric material heated to specified high temperature by microwave power at resonant frequency. Accurate measurement contributes to enhanced monitoring and control in contactless high-temperature processing of materials. Also used with small spherical sample to determine temperature dependence of complex dielectric constant.

Barmatz, Martin B.↗

DOE OSTI2025

A self-supervised robotic system for autonomous contact-based spatial mapping of semiconductor properties

Integrating robotically driven contact-based material characterization techniques into self-driving laboratories can enhance measurement quality, reliability, and throughput. While deep learning models support robust autonomy, current methods lack reliable pixel-precision positioning and require extensive labeled data. To overcome these challenges, we propose an approach for building self-supervised autonomy into contact-based robotic systems that teach the robot to follow domain expert measurement principles at high throughputs. We demonstrate the performance of this approach by autonomously driving a 4-DOF robotic probe for 24 hours to characterize semiconductor photoconductivity at 3025 uniquely predicted poses across a gradient of drop-casted perovskite film compositions, achieving throughputs of more than 125 measurements per hour. Spatially mapping photoconductivity onto each drop-casted film reveals compositional trends and regions of inhomogeneity, valuable for identifying manufacturing defects. With this self-supervised neural network–driven robotic system, we enable high-precision and reliable automation of contact-based characterization techniques at high throughputs, thereby allowing measurement of previously inaccessible yet important semiconductor properties for self-driving laboratories.

Science & Technology - Other Topics↗

NASA NTRS1993

Simulation reduction using the Taguchi method

A large amount of engineering effort is consumed in conducting experiments to obtain information needed for making design decisions. Efficiency in generating such information is the key to meeting market windows, keeping development and manufacturing costs low, and having high-quality products. The principal focus of this project is to develop and implement applications of Taguchi's quality engineering techniques. In particular, we show how these techniques are applied to reduce the number of experiments for trajectory simulation of the LifeSat space vehicle. Orthogonal arrays are used to study many parameters simultaneously with a minimum of time and resources. Taguchi's signal to noise ratio is being employed to measure quality. A compromise Decision Support Problem and Robust Design are applied to demonstrate how quality is designed into a product in the early stages of designing.

Mistree, Farrokh↗

DOE OSTI2021

Monte Carlo Simulation of Background and Source Measurements with CSG and CAD Geometries

Detecting radioactive sources in an urban environment is difficult due to the large magnitude and variability of the background radiation. To support the search mission of the National Nuclear Security Administration, a project was undertaken to determine if first-principles modeling and simulation could be used to accurately predict the response of radiation detectors in urban environments. This study demonstrates that the simulated detector responses to photon radiation from both an isotopic source and the background compare well to benchmark-quality measurements in a large urban-like test environment. Simulation results using a traditional combinatorial solid geometry and a CAD model generated from LiDAR measurements gave very similar detector responses. With this validation, further simulations could be used to predict detector responses for various situations in real urban settings.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

NASA NTRS1995

TOPEX/Poseidon Precision Orbit Determination Using Combined GPS, SLR, and DORIS

TOPEX/Poseidon (T/P) is a joint spaceborne oceanographic mission of U.W. NASA and France CNES design launched August 10, 1992. The satellite has a variety tracking systems for both operational and precision orbit determination. Three precise tracking systems: Satellite Laser Ranging (SLR), Doppler Orbitography and Radiopositioning Integrated by Satellite (DORIS), and Global Positioning System (GPS) provide high quality measurements essential for reconstructing the T/P orbital height with centimeter precision. This paper presents results of simultaneously processing all three data types to exploit the inherent strength of each in a combined solution. SLR and DORIS are routinely combined to provide orbit solutions for the T/P science team. GPS orbit solutions are produced as part of the first demonstration flight of a high quality spaceborne GPS receiver. Coordinate frame and software system differences between the combined SLR/DORIS orbits and the GPS orbits induce orbital height differences of 2 to 3 centimeters. Combining the three data types within a single software system permits removal of software system differences while obtaining coordinate frame calibration information. These calibrations will aid future spaceborne GPS missions that are not complemented with SLR and/or DORIS.

TOPEX/Poseidon↗

NASA NTRS2020

The Global Ecosystem Dynamics Investigation: High-Resolution Laser Ranging of the Earth’s Forests and Topography

Obtaining accurate and widespread measurements of the vertical structure of the Earth’s forests has been a longsought goal for the ecological community. Such observations are critical for accurately assessing the existing biomass of forests, and how changes in this biomass caused by human activities or variations in climate may impact atmospheric CO2 concentrations. Additionally, the three-dimensional structure of forests is a key component of habitat quality and biodiversity at local to regional scales. The Global Ecosystem Dynamics Investigation (GEDI) was launched to the International Space Station in late 2018 to provide high-quality measurements of forest vertical structure in temperate and tropical forests between 51.6 N & S latitude. The GEDI instrument is a geodetic-class laser altimeter/waveform lidar comprised of 3 lasers that produce 8 transects of structural information. Over its two-year nominal lifetime GEDI is anticipated to provide over 10 billion waveforms at a footprint resolution of 25 m. These data will be used to derive a variety of footprint and gridded products, including canopy height, canopy foliar profiles, Leaf Area Index (LAI), sub-canopy topography and biomass. Additionally, data from GEDI are used to demonstrate the efficacy of its measurements for prognostic ecosystem modeling, habit and biodiversity studies, and for fusion using radar and other remote sensing instruments. GEDI science and technology are unique: no other space-based mission has been created that is specifically optimized for retrieving vegetation vertical structure. As such, GEDI promises to advance our understanding of the importance of canopy vertical variations within an ecological paradigm based on structure, composition and function.

Dubayah, Ralph↗

NASA NTRS2012

Emperical Tests of Acceptance Sampling Plans

Acceptance sampling is a quality control procedure applied as an alternative to 100% inspection. A random sample of items is drawn from a lot to determine the fraction of items which have a required quality characteristic. Both the number of items to be inspected and the criterion for determining conformance of the lot to the requirement are given by an appropriate sampling plan with specified risks of Type I and Type II sampling errors. In this paper, we present the results of empirical tests of the accuracy of selected sampling plans reported in the literature. These plans are for measureable quality characteristics which are known have either binomial, exponential, normal, gamma, Weibull, inverse Gaussian, or Poisson distributions. In the main, results support the accepted wisdom that variables acceptance plans are superior to attributes (binomial) acceptance plans, in the sense that these provide comparable protection against risks at reduced sampling cost. For the Gaussian and Weibull plans, however, there are ranges of the shape parameters for which the required sample sizes are in fact larger than the corresponding attributes plans, dramatically so for instances of large skew. Tests further confirm that the published inverse-Gaussian (IG) plan is flawed, as reported by White and Johnson (2011).

White, K. Preston, Jr.↗

NASA NTRS2020

Causes and Effects of AIRS Optics Temperature Cycles

In addition to the expected orbital thermal cycle, geophysical conditions with high thermal and reflected upwelling infrared (IR) drive measurable changes in the AIRS instrument with a period of 24 hours. Especially hot and bright scenes are important, with about 30% of the variability driven by thermal IR and 70% by reflected IR. We show how these cycles manifest in the instrument telemetry for temperatures and gain and with careful analysis can even be detected in spectral shifts.Thermal cycles are an unavoidable feature of instruments observing upwelling radiances from Earth, because the signal inherently carries varying amounts of energy into the instrument. Temperature control of the optical bench, on-board calibrator blackbody, and Focal Plane Array (FPA) in AIRS reduce the impacts of temperature variability to extremely small levels. This combined with good on-board telemetry of the temperatures and including temperature variability in our calibration algorithm has resulted in an instrument that achieves ‘climate quality’ measurements. Careful instrument and algorithm design allows us to characterize and document the impact of temperature variability and limit the effects to negligible levels, helping the instrument meet important climate-quality criteria specified in Ohring 2005

Overoye, Kenneth↗

NASA NTRS2005

Intelligent Sensors: An Integrated Systems Approach

The need for intelligent sensors as a critical component for Integrated System Health Management (ISHM) is fairly well recognized by now. Even the definition of what constitutes an intelligent sensor (or smart sensor) is well documented and stems from an intuitive desire to get the best quality measurement data that forms the basis of any complex health monitoring and/or management system. If the sensors, i.e. the elements closest to the measurand, are unreliable then the whole system works with a tremendous handicap. Hence, there has always been a desire to distribute intelligence down to the sensor level, and give it the ability to assess its own health thereby improving the confidence in the quality of the data at all times. This paper proposes the development of intelligent sensors as an integrated systems approach, i.e. one treats the sensors as a complete system with its own sensing hardware (the traditional sensor), A/D converters, processing and storage capabilities, software drivers, self-assessment algorithms, communication protocols and evolutionary methodologies that allow them to get better with time. Under a project being undertaken at the NASA Stennis Space Center, an integrated framework is being developed for the intelligent monitoring of smart elements. These smart elements can be sensors, actuators or other devices. The immediate application is the monitoring of the rocket test stands, but the technology should be generally applicable to the Intelligent Systems Health Monitoring (ISHM) vision. This paper outlines some fundamental issues in the development of intelligent sensors under the following two categories: Physical Intelligent Sensors (PIS) and Virtual Intelligent Sensors (VIS).

Mahajan, Ajay↗

DOE OSTI2025

Review of High‐Speed Digital Image Correlation: Advancements and Good Practices

This paper reviews the current state of the art in high‐speed (HS) and ultrahigh‐speed (UHS) digital image correlation (DIC) techniques, emphasizing their critical role in experimental research across various scientific domains. HS and UHS DIC have evolved significantly, driven by advancements in camera systems, image processing algorithms and experimental methodologies. These developments have opened new avenues for capturing and analysing dynamic events with unprecedented temporal and spatial detail, but not without introducing challenges such as optical distortions, motion blur and lighting issues that can affect measurement quality. This review advocates for standardized reporting practices in HS/UHS DIC methodologies to improve reproducibility and reliability across studies, drawing on guidelines from the International Digital Image Correlation Society (iDICs). Through a comprehensive analysis of over 150 articles, this review identifies key advancements in imaging technology and their application in six research domains: material characterization, test development, fracture mechanics, model validation, ballistic and explosive phenomena assessment and measurement uncertainties. Distinctions between two‐dimensional (2D) and stereo‐DIC applications are explored, offering insights into their practical implementation and trade‐offs. Good practices for HS/UHS DIC applications are proposed along with suggestions for future directions for this evolving field, highlighting the indispensable role of technological innovation in expanding the capabilities of optical metrology.

experimental mechanics↗

DOE OSTI2020

Status Update on the High Precision Isotopic Measurements on High Burnup LWR Fuel in 2020

The US Department of Energy (DOE) Office of Nuclear Energy (NE) is currently investigating the feasibility of directly disposing dual-purpose (storage and transportation) canisters (DPCs) in a spent nuclear fuel (SNF) repository. Criticality during the repository performance period (10,000 years or more) is one of the major concerns related to direct disposal of DPCs, specifically as the system undergoes degradation in the repository environment and timeframe. Oak Ridge National Laboratory (ORNL) is developing an as-loaded criticality analysis methodology using full (actinides + fission products) burnup credit that exploits the inherent criticality margin associated with actual canister-specific loading configuration. Burnup credit criticality analysis requires validation of the depletion/decay codes used to generate the burned isotopic inventory of an assembly by comparing the code-predicted inventory with experimentally determined isotopic data. Currently, isotopic measurement data for boiling water reactors (BWR) SNF are limited, and additional measurements will be highly beneficial for BWR burnup credit analysis, which is essential to demonstrate disposability of BWR DPCs. Moreover, new pressurized water reactor (PWR) samples of isotopic measurements will expand the PWR sample population and consequently will greatly improve sample statistics. In turn, this will reduce uncertainty in the computational determination of the isotopic composition of commercial SNF and eliminate additional penalties currently used for lack of data. As part of the isotopic analysis task, eight diverse, high burnup (HBU) samples from several PWR rods are being dissolved and isotopically analyzed to provide high-quality measurement data for PWR SNF to reducing the uncertainties associated with PWR isotopic depletion validation. The isotopics of interest focus on nuclides important to burnup credit, shielding, and decay heat in PWR SNF. Additionally, eight high burnup BWR fuel samples from the Limerick nuclear power plant have been identified for measurement to support reducing uncertainties associated with BWR isotopic depletion validation.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

NASA NTRSDate not supplied

Development and Assessment of a New Particle Image Velocimetry System in the NASA GRC 225 cm2 Wind Tunnel

As part of an ongoing campaign to provide detailed and thorough measurements in a two-dimensional impinging shock-wave/boundary-layer interaction (SWBLI), a custom implementation of the Particle Image Velocimetry (PIV) measurement technique in the NASA Glenn 225 cm2 Wind Tunnel was constructed. The flow seeding apparatus was devised to locally seed the region of interest in the overall flowfield to avoid coating the viewing window with seed material. The ability of the PIV system to provide small particles which faithfully track the underlying gas-phase flowfield was of key importance for the success of this system to make quality measurements in the SWBLI flowfield. In order to optimize and assess the performance of the particle seeding system, PIV measurements were made across a planar oblique shock wave and particle response was analyzed to quantify the particle lag effects due to the finite inertia of the seed droplets. Video recordings from a camera placed in the wind tunnel plenum tank were also used to discern the near-field behavior of the seeded plume and guide the design evolution of the seeding apparatus. The resulting optimized seeding configuration was applied to make PIV measurements in the wind tunnel test section boundary layer to assess the seed particle spatial coverage and concentration. This sample boundary layer dataset provides an analog to the eventual boundary layer measurements to be made in the axisymmetric test section under much more challenged viewing conditions.

PIV↗

NASA NTRSDate not supplied

Development and Assessment of a New Particle Image Velocimetry System in the NASA GRC 225 cm2 Wind Tunnel

PIV↗

DOE OSTI2020

Valence-to-core X-ray emission spectroscopy of titanium compounds using energy dispersive detectors

X-ray emission spectroscopy (XES) of transition metal compounds is a powerful tool for investigating the spin and oxidation state of the metal centers. Valence-to-core (vtc) XES is of special interest, as it contains information on the ligand nature, hybridization, and protonation. To date, most vtc-XES studies have been performed with high-brightness sources, such as synchrotrons, due to the weak fluorescence lines from vtc transitions. Here, we present a systematic study of the vtc-XES for different titanium compounds in a laboratory setting using an X-ray tube source and energy dispersive microcalorimeter sensors. With a full-width at half-maximum energy resolution of approximately 4 eV at the Ti Kβ lines, we measure the XES features of different titanium compounds and compare our results for the vtc line shapes and energies to previously published and newly acquired synchrotron data as well as to new theoretical calculations. Finally, we report simulations of the feasibility of performing time-resolved vtc-XES studies with a laser-based plasma source in a laboratory setting. Our results show that microcalorimeter sensors can already perform high-quality measurements of vtc-XES features in a laboratory setting under static conditions and that dynamic measurements will be possible in the future after reasonable technological developments.

36 MATERIALS SCIENCE↗

NASA NTRS2011

Receiver Gain Modulation Circuit

A receiver gain modulation circuit (RGMC) was developed that modulates the power gain of the output of a radiometer receiver with a test signal. As the radiometer receiver switches between calibration noise references, the test signal is mixed with the calibrated noise and thus produces an ensemble set of measurements from which ensemble statistical analysis can be used to extract statistical information about the test signal. The RGMC is an enabling technology of the ensemble detector. As a key component for achieving ensemble detection and analysis, the RGMC has broad aeronautical and space applications. The RGMC can be used to test and develop new calibration algorithms, for example, to detect gain anomalies, and/or correct for slow drifts that affect climate-quality measurements over an accelerated time scale. A generalized approach to analyzing radiometer system designs yields a mathematical treatment of noise reference measurements in calibration algorithms. By treating the measurements from the different noise references as ensemble samples of the receiver state, i.e. receiver gain, a quantitative description of the non-stationary properties of the underlying receiver fluctuations can be derived. Excellent agreement has been obtained between model calculations and radiometric measurements. The mathematical formulation is equivalent to modulating the gain of a stable receiver with an externally generated signal and is the basis for ensemble detection and analysis (EDA). The concept of generating ensemble data sets using an ensemble detector is similar to the ensemble data sets generated as part of ensemble empirical mode decomposition (EEMD) with exception of a key distinguishing factor. EEMD adds noise to the signal under study whereas EDA mixes the signal with calibrated noise. It is mixing with calibrated noise that permits the measurement of temporal-functional variability of uncertainty in the underlying process. The RGMC permits the evaluation of EDA by modulating the receiver gain using an external signal. Without the RGMC, samples of calibrated references from radiometers form an ensemble data set of the natural occurring fluctuations within a receiver. By driving the gain of an otherwise stable receiver with an external signal, the conceptual framework and generalization of the mathematics of EDA can be tested. A series of measurements was conducted to evaluate and characterize the performance of the RGMC. Test signals stepped the RGMC across its dynamic range of performance using a radiometer that sampled four noise references; analysis indicates that the RGMC successfully modulated the receiver gain with an external signal. Calibration algorithms applied to four noise references demonstrate the RGMC produced ensemble data sets of the external signal.

Jones, Hollis↗

DOE OSTI2021

Dispersion calibration for the National Ignition Facility electron–positron–proton spectrometers for intense laser matter interactions

Electron–positron pairs, produced in intense laser–solid interactions, are diagnosed using magnetic spectrometers with image plates, such as the National Ignition Facility Electron–Positron–Proton Spectrometers (EPPSs). Although modeling can help infer the quantitative value, the accuracy of the models needs to be verified to ensure measurement quality. The dispersion of low-energy electrons and positrons may be affected by fringe magnetic fields near the entrance of the EPPS. We have calibrated the EPPS with six electron beams from a Siemens Oncor linear accelerator (linac) ranging in energy from 2.7 MeV to 15.2 MeV as they enter the spectrometer. A Geant4 Tool for Particle Simulation Monte Carlo simulation was set up to match depth dose curves and lateral profiles measured in water at 100 cm source–surface distance. An accurate relationship was established between the bending magnet current setting and the energy of the electron beam at the exit window. The simulations and measurements were used to determine the energy distributions of the six electron beams at the EPPS slit. Furthermore, analysis of the scanned image plates together with the determined energy distribution arriving in the spectrometer provides improved dispersion curves for the EPPS.

47 OTHER INSTRUMENTATION↗

NASA NTRS2005

Strawman Philosophical Guide for Developing International Network of GPM GV Sites

The creation of an international network of ground validation (GV) sites that will support the Global Precipitation Measurement (GPM) Mission's international science programme will require detailed planning of mechanisms for exchanging technical information, GV data products, and scientific results. An important component of the planning will be the philosophical guide under which the network will grow and emerge as a successful element of the GPM Mission. This philosophical guide should be able to serve the mission in developing scientific pathways for ground validation research which will ensure the highest possible quality measurement record of global precipitation products. The philosophical issues, in this regard, partly stem from the financial architecture under which the GV network will be developed, i.e., each participating country will provide its own financial support through committed institutions -- regardless of whether a national or international space agency is involved.At the 1st International GPM Ground Validation Workshop held in Abingdon, UK in November-2003, most of the basic tenants behind the development of the international GV network were identified and discussed. Therefore, with this progress in mind, this presentation is intended to put forth a strawman philosophical guide supporting the development of the international network of GPM GV sites, noting that the initial progress has been reported in the Proceedings of the 1st International GPM GV Workshop -- available online. The central philosophical issues themselves, all flow from the fact that each participating institution can only bring to the table, GV facilities and scientific personnel that are affordable to the sanctioning (funding) national agency (be that a research, research-support, or operational agency). This situation imposes on the network, heterogeneity in the measuring sensors, data collection periods, data collection procedures, data latencies, and data reporting capabilities. Therefore, in order for the network to be effective in supporting the central scientific goals of the GPM mission, there must be a basic agreed upon doctrine under which the network participants function vis-a-vis: (1) an overriding set of general scientific requirements, (2) a minimal set of policies governing the free flow of GV data between the scientific participants, (3) a few basic definitions concerning the prioritization of measurements and their respective value to the mission, (4) a few basic procedures concerning data formats, data reporting procedures, data access, and data archiving, and (5) a simple means to differentiate GV sites according to their level of effort and ability to perform near real-time data acquisition - data reporting tasks. Most important, in case they choose to operate as a near real-time data collection-data distribution site, they would be expected to operate under a fairly narrowly defined protocol needed to ensure smooth GV support operations. This presentation will suggest measures responsive to items (1) - (5) from which to proceed,. In addition, this presentation will seek to stimulate discussion and debate concerning how much heterogeneity is tolerable within the eventual GV site network, given that the any individual GV site can only be considered scientifically useful if it supports the achievement of the central GPM Mission goals. Only ground validation research that has a direct connection to the space mission should be considered justifiable given the overarching scientific goals of the mission. Therefore each site will have to seek some level of accommodation to what the GPM Mission requires in the way of retrieval error characterization, retrieval error detection and reporting, and generation of GV data products that support assessment and improvement of the mission's standard precipitation retrieval algorithms. These are all important scientific issues that will be best resolved in open scientific debate.

Smith, Eric A.↗

NASA NTRS2021

Simultaneous Focused Laser Differential Interferometry and High-Speed Schlieren in a Mach 6 Flow

An instrument is demonstrated that is capable of simultaneous and independent flow density fluctuation measurements over the same line-of-sight by combining two optical techniques: focused laser differential interferometry (FLDI) and high-speed schlieren (HSS). The FLDI instrument measures fluctuations at a single point in the flowfield at 10 MHz, with the resulting signal most sensitive in the region nearest the focal plane of the FLDI laser beam. The HSS instrument acquires images at 20 kHz along the same optical axis as the FLDI beam, but with the resulting signal path averaged over the entire HSS line-of-sight. The introduction of the HSS optics into the FLDI beam path provides two high-quality measurement capabilities in a single system with no degradation of performance relative to stand-alone FLDI or HSS instruments.

Focused Laser Differential Interferometry↗