Composite propellant combustion
Temperature measurements in gaseous reaction zone near surface of burning composite solid propellant, using modified line reversal pyrometer
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Temperature measurements in gaseous reaction zone near surface of burning composite solid propellant, using modified line reversal pyrometer
A study program is discussed which includes a survey of industry and government laboratories and was undertaken to determine the state of the art in dealing with problems of high power levels in reentry antenna design. A laboratory program to develop techniques for testing dielectric materials for effects on RF transmission is also considered, with emphasis on high power applications in space and reentry flights. The study program resulted in a set of guidelines for avoiding breakdown in antenna design. A discussion of temperature effects on dielectric breakdown is also given. From the laboratory program, a description is presented of techniques for (1) heating with a carbon arc image furnace, (2) temperature measurement (using thermocouples and an infrared pyrometer), (3) mass spectrometric monitoring of outgassing, (4) testing for RF breakdown in both heated dielectrics and the dielectric/air and dielectric/plasma interfaces. Data and observations are reported from technique development using candidate shuttle materials falling into three categories: (1) lightweight refractory foams, (2) dense RF window materials, and (3) ablative materials.
Seven superalloy models were tested in a plasma arc tunnel facility. The test models were 3 in. (7.62cm) square flat surfaces (nominally 0.01 to 0.02 in. (0.0254 to 0.0508 cm) thick) held in a water-cooled wedge holder at a 60 deg (1.05 rad) angle of attack. The models were cycled 25 times (two were cycled 50 times) for 10 min each cycle in a Mach 4.6 test stream with the model leading edge temperature maintained at 2200 F (1478 K) (one at 2000 F (1367 K)). Backface temperatures were measured with four platinum-platinum 10% rhodium thermocouples and the front surface temperatures with an optical pyrometer. Four different nickel base alloy materials and one cobalt material were evaluated.
The technology developed in defining a facility to be used on the Skylab mission for electromagnetic suspension of small, molten spheres in the weightless space environment is described. The technologies discussed include: four-coil optimization, four-coil versus six-coil configuration comparison, four-coil position servocontrol, four-coil breadboard, position sensing and servosystem, two-color pyrometer, and specimen toration mode analysis.
A variety of tests was undertaken to determine the nature of heat generation associated with a pneumatic tire operating under various conditions. Tests were conducted to determine the magnitude and distribution of internally generated heat caused by hysteresis in the rubber and ply fabric in an automobile tire operating under conditions of load, pressure, and velocity representative of normal operating conditions. These included tests at various yaw angles and tests with braking applied. In other tests, temperature sensors were mounted on a road to measure the effect of a tire rolling over and an attempt was made to deduce the magnitude and nature of interfacial friction from the resulting information. In addition, tests were performed using the scratch plate technique to determine the nature of the motion between the tire and road. Finally, a model tire was tested on a roadwheel, the surface covering which could be changed, and an optical pyrometer was used to measure rubber surface temperatures.
Ultrasonic pulse techniques have been developed which, when applied to inert gases, provide temperature measurements up to 8000 K. The response time can be less than 1 msec. This is a significant feature in studying shock-heated or combusting gases. Using a momentary contact coupling technique, temperature has been measured inside steel from 300 to 1500 K. Thin-wire sensors have been used above 2000 K in nuclear and industrial applications where conditions preclude the use of thermocouples, resistance devices, or optical pyrometers. At 2500 K, temperature sensitivity of 0.1% is obtained in Re wire sensors 5 cm long by timing five round trips with an electronic instrument that resolves the time interval between selected echoes to 0.1 microsec. Sensors have been operated at rotational speeds over 2000 rpm and in noisy environments. Temperature profiling of up to ten regions using only a single guided path or beam has also been accomplished.
Seven tantalum sheathed, BeO insulated, 0.157-cm-diam, grounded-junction W-3%Re/W-25%Re thermocouples were irradiated in a helium-argon environment at a temperature of 1900 to 2100 K. Six other thermocouples from the same lot were operated out-of-pile with the same temperature history as the in-pile thermocouples. Drift-in-pile was determined by periodically replacing a 'reference' thermocouple in the irradiation capsule. Drift out-of-pile was determined with an optical pyrometer. After 8000 hours irradiation, the estimated neutron fluence was 4 x 10 to the 21st power thermal neutrons/sq cm and 0.9 x 10 to the 21st power fast neutrons/sq cm (E greater than 0.18 MeV). At this time the in-pile group had decreased in output the equivalent of 340 K at 2073 K, while the out-of-pile group had decreased in output the equivalent of 54 K at 2073 K. The maximum deviation in drift between thermocouples of the in-pile group and between thermocouples of the out-of-pile group was less than plus or minus 15 K and less than plus or minus 10 K, respectively.
The results of testing an on-line quadrupole gas analyzer system are reported. Gas samples were drawn from the exhaust of a hydrogen-oxygen-nitrogen rocket which simulated the flow composition and dynamics at the combustor exit of a supersonic combustion ramjet engine. System response time of less than 50 milliseconds was demonstrated, with analytical accuracy estimated to be + or - 5 percent. For more complex chemical systems with interfering atom patterns, analysis would be more difficult. A cooled-gas pyrometer probe was evaluated as a total temperature indicator and as the primary mass flow measuring element for the total sample flow rate.
A heating array is described for testing full-scale sections of the leading edge and lower fuselage surfaces of the shuttle. The heating array was designed to provide a tool for development and acceptance testing of leading edge segments and large flat sections of the main body thermal protection system. The array was designed using a variable length module concept to meet test requirements using interchangeable components from one test configuration in another configuration. Heat generating modules and heat absorbing modules were employed to achieve the thermal gradient around the leading edge. A support was developed to hold the modules to form an envelope around a variety of leading edges; to supply coolant to each module; the support structure and to hold the modules in the flat surface heater configuration. An optical pyrometer system mounted within the array was designed to monitor specimen surface temperatures without altering the test article's surface.
Instrumented ATJ-S graphite shell nosetip models were tested in the AFFDL 50 MW RENT Facility. The inside surface of the models were instrumented with seven thermocouples and three clip-on extensometers. One thermocouple was located at the inside stagnation point and three thermocouples were located at 120 degree intervals on the aft portion of the skirt of the model. In addition, three thermocouples at 120 degree intervals plus three clip-on extensometers at 120 degree intervals offset 60 degrees from the thermocouples were located in the critical region. The outside surface temperature of the models was monitored in two locations by optical pyrometers. Finally, the tests were recorded by three high speed motion picture cameras. Pressure models and calorimeters were also tested in order to help define the flow field condition and heating distribution around the models.
Elevated temperature measurements of the spectral emittance of reinforced carbon-carbon (RCC) as the thermal protection material for the leading edge areas of the Space Shuttle Orbiter were carried out in situ, with environments provided by arc-heated streams of air and argon. A monochromator, infrared pyrometers, and thermocouples were used in evaluating the response of the RCC test specimens during the emittance measurements. Results indicate that the material is nongray, with lowest spectral emittance at the short wavelengths and with relatively high total emittance. The trend of the total emittance data suggests a slight decrease in total emittance with increasing temperature, although the emittance value stabilizes with continuing exposure.
Various types of instrumentation for the development of propulsion systems are discussed. For the steady-state measurement of local temperature, pressure and flow velocity in gases the devices include: a multielement probe, calibrated thermocouple probes, thermocouple probes designed for low gas velocities, pressure measuring devices for high-speed rotors, and instruments for data pickup from rotating members. For the dynamic measurements of the same factors attention is given to 2-mm diameter pressure transducers, flush-diaphragm transducers, resistance thermometers or thermocouples, and miniature transducers for velocity measurements. Instruments for compressor and turbine-blade instrumentation are described with reference to a pyrometer for mapping turbine-blade surface temperature, a capacitance method for making rotor clearance measurements, and optical detection procedures for blade vibration amplitude.
The spectral emittance of a NASA developed zirconia ceramic thermal barrier coating system, consisting of a metal substrate, a layer of Ni-Cr-Al-Y bond material and a layer of yttria-stabilized zirconia ceramic material, is analyzed. The emittance, needed for evaluation of radiant heat loads on cooled coated gas turbine components, was measured over a range of temperatures that would be typical of its use on such components. Emittance data were obtained with a spectrometer, a reflectometer and a radiation pyrometer at a single bond coating thickness of 0.010 cm and at a ceramic coating thickness of 0-0.076 cm. The data were transformed into the hemispherical total emittance and were correlated to the ceramic coating thickness and temperature using multiple-regression curve-fitting techniques. The system was found to be highly reflective, and, consequently, capable of significantly reducing radiation heat loads on cooled gas turbine engine components.
The paper presents the measurements of linear triatomic carbon opacity (C3) made in a graphite tube furnace to extend the wavelength range of Brewer and Engelke (1962) to the 280-600 nm range. An electrooptical method was used to determine C3 absorption in argon at 2720 to 3060 K; a quartic polynomial regression expression was derived to provide a complete temperature profile from pyrometer measurements. The C3 spectra were plotted for several opacity levels. It was concluded that the extension of the spectral range to the near u.v. levels made it easier to identify C3 particles.
The work done to fabricate Marchuk plasma discharge tubes for measurement of the cesiated emission of lanthanum hexaboride and thoriated tungsten electrodes is described. A photon counting pyrometer was completed and is to be calibrated with a gold standard.
A continuous requirement exists for calibration and environmental testing of instruments in use at multitude of test facilities at Langley Research Center. Brief summarizes several automated systems available for calibration of research instruments to include: six-component balance, multimeter, amplifier, pyrometer, voltage-controlled oscillator, pressure transducer and accelerometer.
Six growth runs used the Kayex-Hameo Automatic Games Logic (AGILE) computer based system for growth from larger melts in the Mod CG2000. The implementation of the melt pyrometer sensor allowed for dip temperature monitoring and usage by the operator/AGILE system. Use of AGILE during recharge operations was successfully evaluated. The tendency of crystals to lose cylindrical shape (spiraling) continued to be a problem. The hygrometer was added to the Furnace Gas Analysis System and used on several growth runs. The gas chromatograph, including the integrator, was also used for more accurate carbon monoxide concentration measurements. Efforts continued for completing the automation of the total Gas Analysis System. An economic analysis, based on revised achievable straight growth rate, is presented.
Shock wave (Hugoniot), shock temperature, and release data are presented for several geophysically important, refractory materials. A sensitive multichannel optical pyrometer was developed to measure shock temperatures (2500 to 5600 K at pressures from 48 to 117 GPa) in anorthite (CaAl2Si2O8) glass. Shock temperatures of 3750 to 6000 K at pressures from 140 to 182 GPa were measured in calcium oxide (CaO). Temperature data were used to constrain the energetics of the B1-B2 phase transition at 70 GPa in CaO, and to construct a finite strain equation of state for CaO consistent with previous Hugoniot data. The CaO equation of state was used with equation of state parameters of other oxides to construct a theoretical mixed oxide Hugoniot of anorthite, which is in agreement with new Hugoniot data above about 50 GPa, determined using experimental techniques developed. The mixed oxide model, however, overestimates the shock temperatures, and does not accurately predict measured release paths.