Evaluation of the thermal properties of materials. Volume 2 - Data handbook Final report, 29 Jun. 1965 - 28 Jun. 1966
Thermal properties of spacecraft materials - evaluation of aluminum honeycomb panel structures and ablator materials
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Thermal Stability of a 4 Meter Primary Reflector for the Scanning Microwave Limb Sounder
The Scanning Microwave Limb Sounder (SMLS) is a space-borne heterodyne radiometer which will measure pressure, temperature and atmospheric constituents from thermal emission in [180,680] GHz. SMLS, planned for the NRC Decadal Survey's Global Atmospheric Composition Mission, uses a novel toric Cassegrain antenna to perform both elevation and azimuth scanning. This provides better horizontal and temporal resolution and coverage than were possible with elevation-only scanning in the two previous MLS satellite instruments. SMLS is diffraction-limited in the vertical plane but highly astigmatic in the horizontal (beam aspect ratio approx. 1:20). Nadir symmetry ensures that beam shape is nearly invariant over plus or minus 65 deg azimuth. A low-noise receiver FOV is swept over the reflector system by a small azimuth-scanning mirror. We describe the fabrication and thermal-stability test of a composite demonstration primary reflector, having full 4m height and 1/3 the width planned for flight. Using finite-element models of reflectors and structure, we evaluate thermal deformations and optical performance for 4 orbital environments and isothermal soak. We compare deformations with photogrammetric measurements made during soak tests in a chamber. The test temperature range exceeds predicted orbital ranges by large factors, implying in-orbit thermal stability of 0.21 micron rms (root mean square)/C, which meets SMLS requirements.
thermal distortion↗
Comparative Flow Path Analysis and Design Assessment of an Axisymmetric Hydrogen Fueled Scramjet Flight Test Engine at a Mach Number of 6.5
NASA has contracted with the Central Institute of Aviation Motors CIAM to perform a flight test and ground test and provide a scramjet engine for ground test in the United States. The objective of this contract is to obtain ground to flight correlation for a supersonic combustion ramjet (scramjet) engine operating point at a Mach number of 6.5. This paper presents results from a flow path performance and thermal evaluation performed on the design proposed by the CIAM. This study shows that the engine will perform in the scramjet mode for stoichiometric operation at a flight Mach number of 6.5. Thermal assessment of the structure indicates that the combustor cooling liner will provide adequate cooling for a Mach number of 6.5 test condition and that optional material proposed by CIAM for the cowl leading-edge design are required to allow operation with or without a type IV shock-shock interaction.
McClinton, C.↗
An experimental and theoretical evaluation of increased thermal diffusivity phase change devices
This study was to experimentally evaluate and mathematically model the performance of phase change thermal control devices containing high thermal conductivity metal matrices. Three aluminum honeycomb filters were evaluated at five different heat flux levels using n-oct-adecane as the test material. The system was mathematically modeled by approximating the partial differential equations with a three-dimensional implicit alternating direction technique. The mathematical model predicts the system quite well. All of the phase change times are predicted. The heating of solid phase is predicted exactly while there is some variation between theoretical and experimental results in the liquid phase. This variation in the liquid phase could be accounted for by the fact that there are some heat losses in the cell and there could be some convection in the experimental system.
White, S. P.↗
Deposit formation in hydrocarbon rocket fuels with an evaluation of a propane heat transfer correlation
A high pressure fuel coking testing apparatus was designed and developed and was used to evaluate thermal decomposition limits and carbon decomposition rates in heated copper tubes for hydrocarbon fuels. A commercial propane (90% grade) and chemically pure (CP) propane were tested. Heat transfer to supercritical propane was evaluated at 136 atm, bulk fluid velocities of 6 to 30 m/s, and tube wall temperatures in the range of 422 to 811 K. A forced convection heat transfer correlation developed in a previous test effort verified a prediction of most of the experimental data within a + or - 30% range, with good agreement for the CP propane data. No significant differences were apparent in the predictions derived from the correlation when the carbon resistance was included with the film resistance. A post-test scanning electron microprobe analysis indicated occurrences of migration and interdiffusion of copper into the carbon deposit.
Masters, P. A.↗
Development, fabrication and evaluation of composite thermal engine insulation
Foil enclosure configurations of 10 variations were fabricated and evaluated. A discussion of the thermal protection system panel design includes: (1) description of 3DSX/foil concept, (2) design environment, (3) material selection, (4) fabrication enclosure, (5) structural design, (6) thermal sizing, and (7) weight analysis. The structural design study includes foil evaluation, venting pressure loads, thermomechanical behavior, and enclosure venting (burst) pressure tests. Results of experimental demonstrations of performance and reuse capabilities are given for both thermal and acoustic testing.
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Thermal control of power supplies with electronic packaging techniques
The integration of low-cost commercial heat pipes in the design of a NASA candidate standard modular power supply with a 350 watt output resulted in a 44% weight reduction. Part temperatures were also appreciably reduced, increasing the environmental capability of the unit. A complete 350- watt modular power converter was built and tested to evaluate thermal performance of the redesigned supply.
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Environmental Testing Of High Temperature Materials and Coatings
Materials for today′s extreme environments have unique challenges and design requirements that require multi-faceted evaluations. Thermal and mechanical testing and analysis is important in design, but environmental effects are often the limiting factor of materials in service. Degradation modes such as oxidation, recession, erosion, foreign object damage, and chemical corrosion can negatively impact the materials thermo-mechanical behavior. While materials may ultimately fail under thermo−mechanical stresses, environmental effects are many times the root cause. Evaluation of materials systems under relevant conditions are critical.....start by identifying mechanisms and develop corresponding test methods. Comprehensive modeling begins with thermo-mechanical behavior, then considers environmental degradation modes that provide a “knock down” of that behavior.
Thermal testing Mechanical testing↗
Measurement of Thermal Radiation Properties of Solids
The overall objectives of the Symposium were to afford (1) an opportunity for workers in the field to describe the equipment and procedures currently in use for measuring thermal radiation properties of solids, (2) an opportunity for constructive criticism of the material presented, and (3) an open forum for discussion of mutual problems. It was also the hope of the sponsors that the published proceedings of the Symposium would serve as a valuable reference on measurement techniques for evaluating thermal radiation properties of solids, partic.ularly for those with limited experience in the field. Because of the strong dependence of emitted flux upon temperature, the program committee thought it advisable to devote the first session to a discussion of the problems of temperature measurement. All of the papers in Session I were presented at the request of and upon topics suggested by the Committee. Because of time and space limitations, it, was impossible to consider all temperature measurement problems that might arise--the objective was rather to call to the attention of the reader some of the problems that might be encountered, and to provide references that might provide solutions.
EMISSION↗
Processes in relativistic plasmas
The establishment and maintenance of a Boltzmann distribution in particle kinetic energies is investigated for a plasma with theta = KTe/mc-squared much greater than unity, where m is the electron mass. It is shown that thermalization of the electron gas by binary collisions is not sufficiently effective to maintain the equilibrium distribution when other processes that perturb the equilibrium are taken into account. Electron-positron pair production in electron-electron and electron-ion collisions, and perturbations of a Boltzmann distribution by nonthermal processes are evaluated. Thermalization by means of other mechanisms, such as interaction with plasma waves is discussed, and the opacity of a relativistic plasma is computed for Compton scattering, pair production in the fields of electrons and ions, inverse bremsstrahlung, and synchrotron self-absorption.
Gould, R. J.↗
Temporal Treatment of a Thermal Response for Defect Depth Estimation
Transient thermography, which employs pulse surface heating of an inspected component followed by acquisition of the thermal decay stage, is gaining wider acceptance as a result of its remoteness and rapidness. Flaws in the component s material may induce a thermal contrast in surface thermograms. An important issue in transient thermography is estimating the depth of a subsurface flaw from the thermal response. This improves the quantitative ability of the thermal evaluation: from one scan it is possible to locate regions of anomalies in thickness (caused by corrosion) and estimate the implications of the flaw on the integrity of the structure. Our research focuses on thick composite aircraft components. A long square heating pulse and several minutes observation period are required to receive an adequate thermal response from such a component. Application of various time-related informative parameters of the thermal response for depth estimation is discussed. A three-dimensional finite difference model of heat propagation in solids in Cartesian coordinates is used to simulate the thermographic process. Typical physical properties of polymer graphite composites are assumed for the model.
Plotnikov, Y. A.↗
Evaluating Three Active Thermal Architectures for Exploration Missions
Mass and cost are typically the two biggest challenges facing space craft designers. Active thermal control systems for crewed space-craft are typically among the more massive and costly systems on the vehicle. A study was completed evaluating three different thermal control system architectures to evaluate overall performance, mass and cost for a typical exploration mission profile. The architectures that were evaluated were 1 - a two-loop system using an internal liquid loop interfacing with an external liquid loop and flow loop with flow through radiators; 2 - a-single loop architecture with flow through radiators utilizing a regenerative heat exchanger and heater; and 3 - a single-loop architecture with heat pipe radiators. Environmental conditions, calculated for a given lunar exploration mission, and mission heat load profiles, generated based on previous Orion time lines, were evalauated through the phases of the on orbit mission. Performance for each of the architectures was evaluated along with the resultant mass of each system. Recommendations include adding a thermal topping system to lunar missions due to the extreme hot environments encountered in near-lunar approaches.
Cross, Cynthia D.↗
A high temperature thermal diffusivity determination procedure for solids and liquids
A new method for measuring the thermal diffusivity of materials at high temperatures is presented. The method is applicable to solids on Earth, and to liquids in the reduced gravity environment of space. It is especially suited to levitated liquid metals at elevated temperatures where thermal diffusivity data is not available. The method is applied in two parts, such that lumped analysis is valid in the first part, and Fourier's law of conduction is valid in the second. In both parts, the spherical specimen is assumed to have been heated to a desired temperature and cooled. An inverse conduction problem is then formulated and solved using Laplace transformation techniques. Using this solution, sample sizes, and experimentally obtained surface temperature history, the thermal diffusivity is determined by minimizing a function that satisifies the heat balance at the surface. Minimization is performed using a modified quasilinearization algorithm. Accuracy is very sensitive to error in the temperature data and increases with better curve fits to the temperature data. An error analysis is also performed, and the effect of errors in the various parameters on the evaluated thermal diffusivity is determined. An experimental study for solids on Earth is suggested, before development for implementation in space.
Bayazitoglu, Yildiz↗
Thermal barrier coating evaluation needs
A 0.025 cm (0.010 in) thick thermal barrier coating (TBC) applied to turbine airfoils in a research gas turbine engine provided component temperature reductions of up to 190 C. These impressive temperature reductions can allow increased engine operating temperatures and reduced component cooling to achieve greater engine performance without sacrificing component durability. The significant benefits of TBCs are well established in aircraft gas turbine engine applications and their use is increasing. TBCs are also under intense development for use in the Low Heat Rejection (LHR) diesel engine currently being developed and are under consideration for use in utility and marine gas turbines. However, to fully utilize the benefits of TBCs it is necessary to accurately characterize coating attributes that affect the insulation and coating durability. The purpose there is to discuss areas in which nondestructive evaluation can make significant contributions to the further development and full utilization of TBCs for aircraft gas turbine engines and low heat rejection diesel engines.
Brindley, William J.↗
Thermal-Control Coatings Evaluated
Report describes tests of variety of thermal-control coating materials, including white paints, second-surface-metalized fluorinated ethylene propylene, aluminum anodized in sulfuric acid, and plasma-sprayed alumina.
Dever, Joyce A.↗
Carbon Nanotube – Polysiloxane Nanocomposites for Ablative Thermal Protection Systems
Ultra-high temperature resins (UHTR) such as polysiloxane possess excellent characteristics for ablation including low thermal conductivity, lightweight composition, high thermal resistance, and the ability to form a durable char layer. To enhance its mechanical strength, the aerospace industry utilizes fiber reinforcement, such as carbon fiber reinforced polysiloxane (CF-polysiloxane), due to its high strength-to-weight ratio. Carbon nanotubes (CNTs) have advantages over microfibers including higher specific strength, lower density, and customizable thermal conductivity. Their nano-scale dimensions allow for a more homogenous material compared to traditional microfibers. Conventional methods of incorporating CNTs into resins often have structural defects such as voids, CNT agglomerations, and randomly dispersed CNTs, resulting in marginal improvements in properties. A novel approach known as bulk nanocomposite laminating (BNL) has been introduced involving CNT densification, resin polymer infiltration, and pressurized curing to achieve a high packing density exceeding 35% by volume. Characterization and testing to simulate re-entry conditions is performed with a sample of CNT-polysiloxane nanocomposite cured onto a CF-polysiloxane backing. These samples are subjected to ablation by an oxyacetylene flame while collecting temperature data to evaluate thermal protection properties.
Palak B Patel↗
Bearing Tester Data Compilation Analysis, and Reporting and Bearing Math Modeling
The magnitude and direction of fluid induced torques and forces on the 57 mm bearing cage is considered to be a contributing factor in possible cage instabilities that can produce intermittent high heating in the bearing. Analyses of the fluid forces and torques are presented. Heat generated by viscous fluid work was estimated for two flow diverter configurations and a coolant flow of 10 lbs/sec to support the thermal evaluation of the LOX Bearing Materials Tester. Results of the analysis of the LOX turbopump turbine end bearings are discussed. Coolant velocities for the no. 4 LOX turbopump turbine end bearings were estimated as a function of shaft speed and coolant flow rate. Contact angles and track width data were developed for the 57 mm bearing as functions of shaft speed, and axial and radial loads. The Advanced Dynamics of Rolling Elements (ADORE) computer program was installed on the MSFC UNIVAC 1100 and a test case successfully run. Both the text output and the plotting output were verified. The Bearing Seal and Materials Tester - Test Condition Data Base was developed. The parametric analysis of the operating characteristics of the LOX turbopump pump end bearing using the 45 mm bearing thermal model was begun.
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Thermal Stability of a 4 Meter Primary Reflector for the Scanning Microwave Limb Sounder
We describe the fabrication and thermal-stability analysis and test of a composite demonstration model of the Scanning Microwave Limb Sounder (SMLS) primary reflector, having full 4m height and 1/3 the width planned for flight. SMLS is a space-borne heterodyne radiometer which will measure pressure, temperature and atmospheric constituents from thermal emission between 180 and 660 GHz. Current MLS instruments in low Earth orbit scan pencil-beam antennas (sized to resolve about one scale height) vertically over the atmospheric limb. SMLS, planned for the Global Atmospheric Composition Mission of the NRC Decadal Survey, adds azimuthal scanning for better horizontal and temporal resolution and coverage than typical orbit spacing provides. SMLS combines the wide scan range of the parabolic torus with unblocked offset Cassegrain optics. The resulting system is diffraction-limited in the vertical plane but highly astigmatic in the horizontal, having a beam aspect ratio [tilde operator]1:20. Symmetry about the nadir axis ensures that beam shape is nearly invariant over +/-65(white bullet) azimuth. The a feeds a low-noise SIS receiver whose FOV is swept over the reflector system by a small scanning mirror. Using finiteelement models of antenna reflectors and structure, we evaluate thermal deformations and the resulting optical performance for 4 orbital environments and isothermal soak. We compare deformations with photogrammetric measurements made during wide-range (ambient+[-97,+75](white bullet) C) thermal soak tests of the primary in a chamber. This range exceeds predicted orbital soak ranges by large factors, implying in-orbit thermal stability of 0.21(mu)m rms/(white bullet)C, which meets SMLS requirements.
Thermal stability tests↗