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At least 1,477 records · Page 82

Dendritic deformation modes in additive manufacturing revealed by operando x-ray diffraction

Abstract Dynamic solidification behavior during metal additive manufacturing directly influences the as-built microstructure, defects, and mechanical properties of printed parts. How the formation of these features is driven by temperature variation (e.g., thermal gradient magnitude and solidification front velocity) has been studied extensively in metal additive manufacturing, with synchrotron x-ray imaging becoming a critical tool to monitor these processes. Here, we extend these efforts to monitoring full thermomechanical deformation during solidification through the use of operando x-ray diffraction during laser melting. With operando diffraction, we analyze thermomechanical deformation modes such as torsion, bending, fragmentation, assimilation, oscillation, and interdendritic growth. Understanding such phenomena can aid the optimization of printing strategies to obtain specific microstructural features, including localized misorientations, dislocation substructure, and grain boundary character. The interpretation of operando diffraction results is supported by post-mortem electron backscatter diffraction analyses.

Dass, Adrita (ORCID:000000019100635X)↗

Temperature dependent Raman scattering and far-infrared reflectance spectra of MgO modified Pb{sub 0.99}(Zr{sub 0.95}Ti{sub 0.05}){sub 0.98}Nb{sub 0.02}O{sub 3} ceramics: A composition effect

Lattice dynamics and phase transition of MgO modified Pb{sub 0.99}(Zr{sub 0.95}Ti{sub 0.05}){sub 0.98}Nb{sub 0.02}O{sub 3} (PZTN-x wt. % MgO, x = 0, 0.1, 0.2, 0.5) ceramics have been investigated by far-infrared (FIR) reflectance in the temperature range of 5.5–300 K and Raman spectra between 77 and 300 K, respectively. With the aid of above complementary methods, the structure of all ceramics was defined as low-temperature ferroelectric rhombohedral phase [F{sub R(LT)}] at room temperature. The FIR dielectric functions were extracted from the multi-Lorentz oscillator dispersion model. The lowest frequency phonon mode, which is related to Pb-BO{sub 3} (B = Zr, Ti, Nb) vibration, mainly dominates the FIR dielectric response. With increasing MgO composition, the dielectric constants ε(0) at room temperature are estimated to 85.4, 73.4, 73.9, and 41.9, respectively. The decreasing trend can be due to the doubly ionized oxygen vacancies induced by Mg substitution for B-site. The order-disorder phase transition located around 120 K can be clearly clarified from temperature evolution of phonon frequency, damping, and intensity. It decreases slightly with increasing MgO composition, which influence the distortion due to the broken correlation chains and local permanent dipoles creation. Moreover, the transformation from antiferroelectric orthorhombic A{sub O} to [ F{sub R(LT)} ] phase has been observed around 250 K, which is associated with the antiferroelectric displacement of Pb atoms along 〈 110 〉 and coupled rotations of the corner-connected oxygen octahedral. Furthermore, the transition from [ F{sub R(LT)} ] to [ F{sub R(HT)} ] (high-temperature ferroelectric rhombohedral phase) was identified around 290 K for MgO-doped PZTN ceramics. It arises from the shift of cation (Pb and Zr/Ti/Nb/Mg ions) along the 〈 111 〉 direction and the transition temperature slightly decreases compared to the pure ceramic.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

Optical design for the single crystal neutron diffractometer Pioneer

Pioneer is a single-crystal neutron diffractometer optimized for small-volume samples and weak signals at the Second Target Station at Oak Ridge National Laboratory. This paper presents the preliminary optical design progress, focusing on the rationale behind key design choices. It covers the T 0 and bandwidth disk choppers, guide and beam control system, incident-beam polarizer, scattering beam collimators, and additional strategies. The chopper locations are selected to maximize neutron transport while taking advantage of standardized shielding structures. To accommodate the maintenance shield, operational shutter, and polarizing V-cavity, the guide design includes significant gaps. When these optical components are moved out of the beam path, oversized collimators, rather than guides, will be translated in. Pioneer will utilize slit packages to control beam size and divergence and a translatable polarizing V-cavity. Absorbing panels are strategically placed near the end station to minimize background. An oscillating radial collimator, operating in a shift mode, will be used with the vertical cylindrical detector, while a fixed multi-cone collimator will be used with the bottom flat detector. In conclusion, these collimators will enable the detection of weak signals when complex sample environments are used.

47 OTHER INSTRUMENTATION↗

Narrow-band erbium-doped fibre linear–ring laser

We have demonstrated a narrow-band linear – ring fibre laser with an output power of 15 mW at a wavelength of 1.55 μm and an emission bandwidth less than 5 kHz. The laser frequency is stabilised by an unpumped active fibre section and fibre Bragg grating. The fibre laser operates in a travelling wave mode, which allows the spatial hole burning effect to be avoided. At a certain pump power level, the laser switches from continuous mode to repetitivepulse operation, corresponding to relaxation oscillations. (control of laser radiation parameters)

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

Spatially-resolved dynamic sampling of different phasic magnetic resonances of nanoparticle ensembles in a magnetotactic bacterium Magnetospirillum magnetotacticum

Abstract Nanoscaled magnetic particle ensembles are promising building blocks for realizing magnon based binary logic. Element-specific real-space monitoring of magnetic resonance modes with sampling rates in the GHz regime is imperative for the experimental verification of future complex magnonic devices. Here we present the observation of different phasic magnetic resonance modes using the element-specific technique of time-resolved scanning transmission x-ray microscopy within a chain of dipolarly coupled Fe 3 O 4 nanoparticles (40–50 nm particle size) inside a single cell of a magnetotactic bacterium Magnetospirillum magnetotacticum . The particles are probed with 25 nm resolution at the Fe L 3 x-ray absorption edge in response to a microwave excitation of 4.07 GHz. A plethora of resonance modes is observed within multiple particle segments oscillating in- and out-of-phase, well resembled by micromagnetic simulations.

time-resolved scanning transmission x-ray microsco↗

Domain wall fluctuations in ferroelectrics coupled to strain

Using a Ginzburg-Landau-Devonshire model that includes the coupling of polarization to strain, we calculate the fluctuation spectra of ferroelectric domain walls. The influence of the strain coupling differs between 180 degrees. and 90 degrees. walls due to the different strain profiles of the two configurations. The finite speed of acoustic phonons, vs, retards the response of the strain to polarization fluctuations, and the results depend on v(s). For v(s) -> infinity, the strain mediates an instantaneous electrostrictive interaction, which is long-range in the 90 degrees. wall case. For finite v(s), acoustic phonons damp the wall excitations, producing a continuum in the spectral function. As v(s) -> 0, a gapped mode emerges, which corresponds to the polarization oscillating in a fixed strain potential.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

Southern Hemisphere dominates recent decline in global water availability

Global land water underpins livelihoods, socioeconomic development, and ecosystems. It remains unclear how water availability has changed in recent decades. Using an ensemble of observations, we quantified global land water availability over the past two decades. We show that the Southern Hemisphere has dominated the declining trend in global water availability from 2001 to 2020. The significant decrease occurs mainly in South America, southwestern Africa, and northwestern Australia. In the Northern Hemisphere, the complex regional increasing and decreasing trends cancel each other, resulting in a negligible hemispheric trend. The variability and trend in water availability in the Southern Hemisphere are largely driven by precipitation associated with climate modes, particularly the El Niño-Southern Oscillation. Finally, this study highlights their dominant role in controlling global water availability.

54 ENVIRONMENTAL SCIENCES↗

Machine Learning Training for HOM reduction and Emittance Preservation in a TESLA-type Cryomodule at FAST

Low emittance electron beams are of high importance at facilities like the LCLS-II at SLAC. Emittance dilution effects due to off-axis beam transport for a TESLA-type cryomodule (CM) have been shown at the Fermilab Accelerator Science and Technology facility. The results showed the correlation between the electron beam-induced cavity high-order modes (HOMs) and submacropulse centroid slewing and oscillation downstream of the CM. Mitigation of emittance dilution can be achieved by reducing the HOM signals and the variances in the submacropulse beam positions downstream of the CM. Here we present a Machine Learning based optimization and model construction for HOM signal level reduction using Neural Networks and Gaussian Processes. To gather training data we performed experiments using single bunch and 50 bunch electron beams with charges up to 125 pC/b. We measured HOM signals of all cavities and beam position with a set of BPMs downstream of the CM. The beam trajectory was changed using V/H125 corrector set located upstream of the CM. The results presented here will inform the LCLS-II injector commissioning and will serve as a prototype for HOM reduction and emittance preservation.

43 PARTICLE ACCELERATORS↗

The Pioneer 11 radio occultation measurements of the Jovian ionosphere

Radio occultation data obtained with the Pioneer 11 spacecraft are utilized to study Jupiter's ionosphere. The ingress measurements, which were conducted by using a stable earth-based frequency reference for the tracking link, yielded ionospheric data near the morning terminator at about 79 deg south latitude. Data were also taken during egress on the evening side near 20 deg north latitude. The latter measurements were conducted in the one-way mode; i.e., an on-board crystal oscillator was employed as a frequency reference for the downlink (spacecraft-to-earth) signal. These data confirm previous results obtained with Pioneer 10 and show that Jupiter has a multilayered ionosphere extending over an altitude range of more than 3000 km. The topside scale height near 79 deg south latitude was 540 + or - 60 km. Assuming a topside electron, H(+) distribution controlled by diffusion yields a plasma temperature of 850 + or - 100 K in this region. The radio data indicate that the upper atmosphere is either warmer or more dissociated into atomic hydrogen than previously anticipated.

Fjeldbo, G.↗

Recent advances in capacitance type of blade tip clearance measurements

Two recent electronic advances at NASA-Lewis that meet the blade tip clearance needs of a wide class of fans, compressors, and turbines are described. The first is a frequency modulated (FM) oscillator that requires only a single low cost ultrahigh frequency operational amplifier. Its carrier frequency is 42.8 MHz when used with a 61 cm long hermetically sealed coaxial cable. The oscillator can be calibrated in the static mode and has a negative peak frequency deviation of 400 kHz for a typical rotor blade. High temperature performance tests of the probe and 13 cm of the adjacent cable show good accuracy up to 600 C, the maximum which produces a clearance error of + or - 10 microns at a clearance of 500 microns. In the second advance, a guarded probe configuration allows a longer cable capacitance. The capacitance of the probe is part of a small time constant feedback in a high speed operational amplifier. The solution of the governing differential equation is applied to a ramp type of input. The results show an amplifier output that contains a term which is proportional to the derivative of the feedback capacitance. The capacitance is obtained by subtracting a balancing reference channel followed by an integration stage.

Barranger, John P.↗

Stability analysis of large space structure control systems with delayed input

Large space structural systems, due to their inherent flexibility and low mass to area ratio, are represented by large dimensional mathematical models. For implementation of the control laws for such systems a finite amount of time is required to evaluate the control signals; and this time delay may cause instability in the closed loop control system that was previously designed without taking the input delay into consideration. The stability analysis of a simple harmonic oscillator representing the equation of a single mode as a function of delay time is treated analytically and verified numerically. The effect of inherent damping on the delay is also analyzed. The control problem with delayed input is also formulated in the discrete time domain.

Reddy, A. S. S. R.↗

Stability analysis of large space structure control systems with delayed input

Large space structural systems, due to their inherent flexibility and low mass to area ratio, are represented by large dimensional mathematical models. For implementation of the control laws for such systems a finite amount of time is required to evaluate the control signals; and this time delay may cause instability in the closed loop control system that was previously designed without taking the input delay into consideration. The stability analysis of a simple harmonic oscillator representing the equation of a single mode as a function of delay time is analyzed analytically and verified numerically. The effect of inherent damping on the delay is also analyzed. The control problem with delayed input is also formulated in the discrete time domain.

Reddy, A. S. S. R.↗

Recent advances in capacitance type of blade tip clearance measurements

Two recent electronic advances at NASA-Lewis that meet the blade tip clearance needs of a wide class of fans, compressors, and turbines are described. The first is a frequency modulated (FM) oscillator that requires only a single low cost ultrahigh frequency operational amplifier. Its carrier frequency is 42.8 MHz when used with a 61 cm long hermetically sealed coaxial cable. The oscillator can be calibrated in the static mode and has a negative peak frequency deviation of 400 kHz for a typical rotor blade. High temperature performance tests of the probe and 13 cm of the adjacent cable show good accuracy up to 600 C, the maximum which produces a clearance error of + or - 10 microns at a clearance of 500 microns. In the second advance, a guarded probe configuration allows a longer cable capacitance. The capacitance of the probe is part of a small time constant feedback in a high speed operational amplifier. The solution of the governing differential equation is applied to a ramp type of input. The results show an amplifier output that contains a term which is proportional to the derivative of the feedback capacitance. The capacitance is obtained by subtracting a balancing reference channel followed by an integration stage.

Barranger, John P.↗

Fast frequency tuning and phase locking of diode-pumped Nd:YAG ring lasers

A diode-pumped single-mode monolithic Nd:YAG ring-laser oscillator has been built which can be tuned piezoelectrically over several tens of MHz in a few microsecs. Frequency stability over 1 msec is better than 500 Hz. Two lasers have been electronically phase locked for periods of minutes with a phase noise of 29 mrad rms.

Kane, Thomas J.↗

Dark matter and the age of globular clusters

The ability of weakly interacting particles called cosmions to suppress convection in the cores of horizontal-branch stars is investigated numerically. It is found that such convection-breaking in horizontal-branch stars by cosmions or by any other novel mode of energy transfer induces thermal relaxation oscillations with a period of about 500,000 yr, corresponding to the core Kelvin-Helmholtz time scale. These thermal pulses can be understood analytically in terms of a simple two-zone model. Observationally, the brightness and brightness dispersion of horizontal-branch stars increases, the periods of RR Lyrae stars change over a pulsation time scale, and the duration of central helium burning slightly decreases. None of these effects is in conflict with observations but, on the contrary, point to a speculative resolution of the age problem for globular clusters and to an alternative explanation of the period fluctuations of RR Lyrae stars.

Dearborn, David↗

Application of unstructured grid methods to steady and unsteady aerodynamic problems

The purpose is to describe the development of unstructured grid methods which have several advantages when compared to methods which make use of structured grids. Unstructured grids, for example, easily allow the treatment of complex geometries, allow for general mesh movement for realistic motions and structural deformations of complete aircraft configurations which is important for aeroelastic analysis, and enable adaptive mesh refinement to more accurately resolve the physics of the flow. Steady Euler calculations for a supersonic fighter configuration to demonstrate the complex geometry capability; unsteady Euler calculations for the supersonic fighter undergoing harmonic oscillations in a complete-vehicle bending mode to demonstrate the general mesh movement capability; and vortex-dominated conical-flow calculations for highly-swept delta wings to demonstrate the adaptive mesh refinement capability are discussed. The basic solution algorithm is a multi-stage Runge-Kutta time-stepping scheme with a finite-volume spatial discretization based on an unstructured grid of triangles in 2D or tetrahedra in 3D. The moving mesh capability is a general procedure which models each edge of each triangle (2D) or tetrahedra (3D) with a spring. The resulting static equilibrium equations which result from a summation of forces are then used to move the mesh to allow it to continuously conform to the instantaneous position or shape of the aircraft. The adaptive mesh refinement procedure enriches the unstructured mesh locally to more accurately resolve the vortical flow features. These capabilities are described in detail along with representative results which demonstrate several advantages of unstructured grid methods. The applicability of the unstructured grid methodology to steady and unsteady aerodynamic problems and directions for future work are discussed.

Batina, John T.↗

Rosat sky survey observations of the eclipsing binary V471 Tauri

Rosat observations of the DA white dwarf + K2V binary system V471 Tauri, obtained during the sky survey phase of the mission, are presented. A lower amplitude shorter time-scale variability is seen in both the soft X-ray and EUV bands. This is associated with the white dwarf pulsations previously discovered by Exosat and also observed at optical wavelengths. The minimum in the EUV light curve is found to coincide with the maximum in the optical. This direct comparison of the phases of the optical and EUV pulses confirms the prediction made by an earlier indirect comparison and shows conclusively that the V471 Tau oscillations cannot arise from nonradial g-mode pulsations in the white dwarf. They are argued to be caused by rotation of the white dwarf with accretion-darkened magnetic poles. On the basis of the EUV and optical pulse shapes, the accretion geometry is studied, and it is estimated that the rate of accretion onto the white dwarf is about (4-11) x 10 exp -13 solar mass/yr.

Barstow, M. A.↗