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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 1,495 records · Page 83
All sourcesNASA NTRSDOE OSTI
DOE OSTI2018

High-temperature deformation behavior and microstructural characterization of high-Mn bearing titanium-based alloy

Highlights: • The hot deformation behavior of a biomedical low-cost Ti-10Mn alloys was studied. • The flow curves of the alloy display periodic serrations attributed to dynamic strain aging. • Mn alloying increases the activation energy to 243 kJ/mol compared to pure Ti. • The dynamic recovery is more effective than dynamic recrystallization at hot deformation. - Abstract: Ti-Mn alloys exhibit an excellent potential for biomedical applications as well as structural engineering applications, especially in the aerospace industry. In order to control and enhance grain structure during the manufacturing of Ti-Mn alloys and thereby help to enhance mechanical properties such as strength and toughness, we studied the hot-deformation behavior of βTi-10Mn alloys. Isothermal compression tests were conducted in the strain rate range of 0.01–10 s{sup −1} and temperatures in the range of 850–1000 °C using a Gleeble thermomechanical simulator. High-temperature flow stress curves exhibited discontinuous yielding and pronounced periodic serrations without any strain hardening during compression straining of these alloys. Such peculiar behavior of this alloy is due to active dynamic strain aging in its β-bcc structure. Metallographic observations by electron-backscattered diffraction (EBSD) analysis revealed that dynamic recovery (DRV) is more active than continuous dynamic recrystallization (CDRX) when the alloy is deformed at high strain rates, i.e. higher than 1 s{sup −1}. Furthermore, the constitutive behavior of the alloy was modeled and the apparent hot-deformation activation energy of the alloy was estimated to be 243 kJ/mol, which is ~60% higher than the self-diffusion energy in pure titanium.

36 MATERIALS SCIENCE↗
DOE OSTI2020

A Comparison of Interface Growth Models Applied to Rayleigh–Taylor and Richtmyer–Meshkov Instabilities

Sophisticated numerical models that contain fluid interfaces rely upon interface evolution models to approximate the transition to turbulence near interfaces, in the presence of Rayleigh–Taylor (RTI) or Richtmyer–Meshkov (RMI) instability. Semi-analytical models have been developed in recent decades to predict the interface growth from an initial state into the nonlinear regime. Two of these models are considered in this study. They are the Goncharov and the z-models. Both of these interface models have strengths and weaknesses, which are examined here. Both of them have been implemented in the xRAGE compressible flow solver, which models fluid interfaces. The flow solver provides the fluids acceleration as a body force to the interface model. The purpose of such interface model is to evolve the early times of interface position as a subgrid model within a compressible flow simulation in order to then initialize a turbulence model. In this work, the interface models are assessed and compared for their evolution of RTI and RMI. The z-model performed better than the Goncharov model for all cases that were explored.

42 ENGINEERING↗
NASA NTRS1974

Studies of Martian polar regions

The flow law determined experimentally for solid CO2 establishes that an hypothesis of glacial flow of CO2 at the Martian poles is not physically unrealistic. Compression experiments carried out under 1 atmosphere pressure and constant strain rate conditions demonstrate that the strength of CO2 near its sublimation point is considerably less than the strength of water ice near its melting point. A plausible glacial model for the Martian polar caps was constructed. The CO2 deposited near the pole would have flowed outward laterally to relieve high internal shear stresses. The topography of the polar caps, and the uniform layering and general extent of the layered deposits were explained using this model.

Smith, C. I.↗
NASA NTRS1980

Saturn's magnetic field and magnetosphere

Results of Pioneer Saturn vector helium magnetometer measurements of the magnetic field and magnetosphere of Saturn are reported. The detection of a bow shock at 23.7 Saturn radii and the magnetosphere crossing at 17.4 Saturn radii suggest an equatorial surface field of 0.3 gauss, which is similar to that of the earth, and the polarity of the field is observed to be similar to that of Jupiter and opposite to the earth's. An increase of magnetic field strength with decreasing radius indicates the dipole nature of the magnetic field, which modified by the compression of the magnetosphere by the solar wind and the presence of a ring current in the middle magnetosphere. Inversions of the field measurements to obtain equivalent dipole source vectors reveal that the tilt angle between the magnetic dipole and the rotation axis is less than 1 deg, and spherical harmonic analysis of the data indicates that the magnetic field is more uniform than those of the earth and Jupiter, consistent with a small Saturn core. An apparent hydromagnetic wake associated with Titan was also observed.

Smith, E. J.↗
NASA NTRS1994

A comparison of graphite/epoxy tape laminates and 2-D braided composites mechanical properties

A comparison of the in-plane mechanical properties of unidirectional composite tape laminates and of two dimensional triaxially braided composite was conducted. The tape laminate layups were designed to match the percentage of axial fibers and the angle of the bias tows in the braided composite. The material system used for the laminates is AS4/3501-6 which was chosen as the closest available match to AS4/1895 used for the braids. This report documents the results of the testing of the laminates and compares these results with data previously obtained for the braided composite. The strength and stiffness properties measured here include tension, open-hole tension, filled-hole tension, compression, and open-hole compression, all of these in both the longitudinal and transverse direction, as well as in-plane shear and bearing.

Minguet, Pierre J.↗
DOE OSTI2020

Thermally-Induced Breakouts: Insights from True-Triaxial Tests with Acoustic Emission Monitoring

Borehole breakouts are used to constrain the magnitude of maximum horizontal stress. However, when the borehole wall strength is higher than the in situ tangential stress, borehole wall failure does not develop. Additional compressive stress can be induced by heating borehole walls. To validate this concept experimentally, we conducted room-temperature and elevated temperature true-triaxial tests on Berea sandstone and Niagaran dolomite samples. We used acoustic emission sensors to capture the onset of breakout development, and we measured the temperature close to borehole wall to assess the magnitude of induced thermal hoop stress. The test results show that within a specific rock type, the breakouts develop in similar manner in room-temperature and elevated-temperature tests. Therefore, the maximum horizontal stress can be constrained from the following dataset: critical tangential stress at which breakout develops, minimum horizontal stress, elastic and thermal properties, and temperature change at the borehole wall.

Trzeciak, Maciej↗
NASA NTRS2004

Deep-Sea Video Cameras Without Pressure Housings

Underwater video cameras of a proposed type (and, optionally, their light sources) would not be housed in pressure vessels. Conventional underwater cameras and their light sources are housed in pods that keep the contents dry and maintain interior pressures of about 1 atmosphere (.0.1 MPa). Pods strong enough to withstand the pressures at great ocean depths are bulky, heavy, and expensive. Elimination of the pods would make it possible to build camera/light-source units that would be significantly smaller, lighter, and less expensive. The depth ratings of the proposed camera/light source units would be essentially unlimited because the strengths of their housings would no longer be an issue. A camera according to the proposal would contain an active-pixel image sensor and readout circuits, all in the form of a single silicon-based complementary metal oxide/semiconductor (CMOS) integrated- circuit chip. As long as none of the circuitry and none of the electrical leads were exposed to seawater, which is electrically conductive, silicon integrated- circuit chips could withstand the hydrostatic pressure of even the deepest ocean. The pressure would change the semiconductor band gap by only a slight amount . not enough to degrade imaging performance significantly. Electrical contact with seawater would be prevented by potting the integrated-circuit chip in a transparent plastic case. The electrical leads for supplying power to the chip and extracting the video signal would also be potted, though not necessarily in the same transparent plastic. The hydrostatic pressure would tend to compress the plastic case and the chip equally on all sides; there would be no need for great strength because there would be no need to hold back high pressure on one side against low pressure on the other side. A light source suitable for use with the camera could consist of light-emitting diodes (LEDs). Like integrated- circuit chips, LEDs can withstand very large hydrostatic pressures. If power-supply regulators or filter capacitors were needed, these could be attached in chip form directly onto the back of, and potted with, the imager chip. Because CMOS imagers dissipate little power, the potting would not result in overheating. To minimize the cost of the camera, a fixed lens could be fabricated as part of the plastic case. For improved optical performance at greater cost, an adjustable glass achromatic lens would be mounted in a reservoir that would be filled with transparent oil and subject to the full hydrostatic pressure, and the reservoir would be mounted on the case to position the lens in front of the image sensor. The lens would by adjusted for focus by use of a motor inside the reservoir (oil-filled motors already exist).

Cunningham, Thomas↗
NASA NTRS2008

Miniature High-Force, Long-Stroke SMA Linear Actuators

Improved long-stroke shape-memory-alloy (SMA) linear actuators are being developed to exert significantly higher forces and operate at higher activation temperatures than do prior SMA actuators. In these actuators, long linear strokes are achieved through the principle of displacement multiplication, according to which there are multiple stages, each intermediate stage being connected by straight SMA wire segments to the next stage so that relative motions of stages are additive toward the final stage, which is the output stage. Prior SMA actuators typically include polymer housings or shells, steel or aluminum stages, and polymer pads between successive stages of displacement-multiplication assemblies. Typical output forces of prior SMA actuators range from 10 to 20 N, and typical strokes range from 0.5 to 1.5 cm. An important disadvantage of prior SMA wire actuators is relatively low cycle speed, which is related to actuation temperature as follows: The SMA wires in prior SMA actuators are typically made of a durable nickel/titanium alloy that has a shape-memory activation temperature of 80 C. An SMA wire can be heated quickly from below to above its activation temperature to obtain a stroke in one direction, but must then be allowed to cool to somewhat below its activation temperature (typically, less than or equal to 60 C in the case of an activation temperature of 80 C) to obtain a stroke in the opposite direction (return stroke). At typical ambient temperatures, cooling times are of the order of several seconds. Cooling times thus limit cycle speeds. Wires made of SMA alloys having significantly higher activation temperatures [denoted ultra-high-temperature (UHT) SMA alloys] cool to the required lower return-stroke temperatures more rapidly, making it possible to increase cycle speeds. The present development is motivated by a need, in some applications (especially aeronautical and space-flight applications) for SMA actuators that exert higher forces, operate at greater cycle speeds, and have stronger housings that can withstand greater externally applied forces and impacts. The main novel features of the improved SMA actuators are the following: 1) The ends of the wires are anchored in compact crimps made from short steel tubes. Each wire end is inserted in a tube, the tube is flattened between planar jaws to make the tube grip the wire, the tube is compressed to a slight U-cross-section deformation to strengthen the grip, then the crimp is welded onto one of the actuator stages. The pull strength of a typical crimp is about 125 N -- comparable to the strength of the SMA wire and greater than the typical pull strengths of wire-end anchors in prior SMA actuators. Greater pull strength is one of the keys to achievement of higher actuation force; 2) For greater strength and resistance to impacts, housings are milled from aluminum instead of being made from polymers. Each housing is made from two pieces in a clamshell configuration. The pieces are anodized to reduce sliding friction; 3) Stages are made stronger (to bear greater compression loads without excessive flexing) by making them from steel sheets thicker than those used in prior SMA actuators. The stages contain recessed pockets to accommodate the crimps. Recessing the pockets helps to keep overall dimensions as small as possible; and, 4) UHT SMA wires are used to satisfy the higher-speed/higher-temperature requirement.

Cummin, Mark A.↗
DOE OSTI2021

Composites and additive manufacturing for high-field coil supports for stellarators

The utilization of composites layered on an additive manufactured substrate, for the production of coil supports for modular coils in small or middle size experimental stellarators is assessed. The focus of the study is a monolithic coil support comprising the coils of a half-period of a stellarator, somewhat similar to the ones in UST_2 and ARIES-CS stellarators. However, the concept may be applicable to quasi-monolithic coil supports (coil forms of NCSX type) or individual coil casings (W7-X type).Coil supports for stellarators require high precision, stiffness and strength for large contorted parts. Traditionally, monolithic coil supports are produced by steel casting/forging and final machining. This production method and material gives accurate, stiff and strong coil supports, but the method may be expensive for monolithic supports due to the geometrical complexity and required accuracy of the structure. In relation to those matters, this work investigates whether a monolithic coil support comprising an additive manufactured resin substrate, which is externally (outward from the coils) surrounded with a thick layer of fibre-reinforced resin, may achieve enough strength and stiffness under middle/high magnetic fields. Finite element calculations are produced to obtain the direction of the principal stresses and their values in compression and tension at different areas of the monolithic support, which is relevant for anisotropic materials. The feasibility of directional application of (carbon) fibres on the winding surface of the stellarator outward from the coils is experimentally tested on a scaled-down additively manufactured prototype of a monolithic support. The strength and stiffness of the composite structure appears sufficient for common magnetic fields in experimental stellarators, and the 3D-composite design and manufacturing was technically feasible.

Queral, Vicente↗
NASA NTRS1995

High-velocity, high-excitation neutral carbon in a cloud in the Vela supernova remnant

HD 72089 is situated behind the Vela supernova remnant, and the interstellar absorption lines in the spectrum of this star are remarkable for two reasons. First, there are six distinct velocity components that span the (heliocentric) velocity range -60 to +121 km/s in the lines of Na I and Ca II. Second, two of the components at high velocity, one at +85 km/s and another at +121.5 km/s, have densities that are large enough to produce observable lines from neutral carbon. The gas moving at +121.5 km/s has such a large pressure that the excited fine-structure levels of the ground electronic state of C I are collisionally populated nearly in proportion to their level degeneracies. This high-velocity gas exhibits unusually low column densities of Mg I and Na I, compared to that of C I. We propose that the +121.5 km/s component represents gas that has cooled and recombined in a zone that follows a shock driven into a cloud by the very recent passage of a supernova blast wave. A representative preshock density of n(sub H) approximately = 13/cc and velocity v(sub s) = 100 km/s is indicated by the strength of diffuse (O III) emission lines seen in directions very near HD 72089. The strong collisional population of excited C I and apparent absence of excited levels of O I give a most favorable fit to the conditions 1000 less than n(sub H) less than 2900/cc over a temperature range 300 less than T less than 1000 K. The fact that the compression is not substantially more than this indicates that the preshock gas may have had an embedded, transverse magnetic field with a strength B greater than or approximately = 1 micro-G. The large dynamical pressure of the supernova blast wave that would be needed to create the cloud shock that we describe implies that the energy of the supernova was 8 x 10(exp 51) ergs, if the Vela remnant is 500 pc away. We can bring this value much closer to typical supernova energies E less than or approximately = 10(exp 51) ergs if the distance to the remnant is revised downward by at least a factor of 2.

Jenkins, Edward B.↗
DOE OSTI2023

Evolution of microstructure and strength of a high entropy alloy undergoing the strain-induced martensitic transformation

In a recent work, we have reported outstanding strength and work hardening exhibited by a metastable high entropy alloy (HEA), Fe 42 Mn 28 Co 10 Cr 15 Si 5 (in at. %), undergoing the strain-induced martensitic transformation from metastable gamma austenite (γ) to stable epsilon martensite (ε). However, the alloy exhibited poor ductility, which was attributed to the presence of the brittle sigma (σ) phase in its microstructure. The present work reports the evolution of microstructure, strength, and ductility of a similar HEA, Fe 38.5 Mn 20 Co 20 Cr 15 Si 5 Cu 1.5 (in at. %), designed to suppress the formation of σ phase. A cast and then rolled plate of the alloy was processed into four conditions by annealing for 10 and 30 min at 1100 °C and by friction stir processing (FSP) at tool rotation rates of 150 and 400 revolutions per minute (RPM) to facilitate detailed examinations of variable initial grain structures. Neutron diffraction and electron microscopy were employed to characterize the microstructure and texture evolution. The initial materials had variable grain size but nearly 100% γ structure. Diffusionless strain induced γ→ε phase transformation took place under compression with higher rate initially and slower rate at the later stages of deformation, independent on the initial grain size. The transformation facilitated part of plastic strain accommodation and rapid strain hardening owing to a transformation-induced dynamic Hall-Petch-type barrier effect, increase in dislocation density, and texture. Here, the peak strength of nearly 2 GPa was achieved under compression using the structure created by double pass FSP (150 RPM followed by 150 RPM). Remarkably, the tensile elongation exhibited by the alloy was nearly 20% with fracture surfaces featuring a combination of ductile dimples and cleavage.

36 MATERIALS SCIENCE↗
DOE OSTI2021

High Density of Strong yet Deformable Intermetallic Nanorods Leads to an Excellent Room Temperature Strength-Ductility Combination in a High Entropy Alloy

This paper introduces a new microstructural template for high entropy alloys (HEAs), where the face centered cubic (FCC) complex concentrated solid solution is reinforced with a high density of strong, yet deformable, nanorods of an ordered multi-component intermetallic L12 compound. Thermodynamic modeling has been employed to design this HEA with a large L12 volume fraction. Thermo-mechanical processing by isothermal annealing of the conventionally processed bulk cold-rolled alloy directly at precipitation temperatures, has been applied to produce a high density of uniformly distributed L12 nanorods within refined FCC grains, resulting from concomitant recrystallization and discontinuous precipitation processes. The nanorod morphology of the discontinuous L12 product has been established from three-dimensional atom probe tomography. The refined grains result in a complete coverage of the microstructure with discontinuously precipitated intermetallic nanorods. This nanorod strengthened HEA exhibits an exceptionally high room temperature yield strength of ~1630 MPa, good tensile ductility of ~15%, and an ultimate tensile strength of ~1720 MPa. Furthermore, a single L12 phase alloy, melted based on the precipitate composition in the two-phase FCC + L12 HEA, exhibits very high compressive deformability and strain hardenability, unusual for ordered intermetallic compounds. These results open a new strategy for design of fine-grained microstructures strengthened via ordered intermetallic phases, exploiting the beneficial effects of discontinuous precipitation, for achieving very high room temperature tensile strengths while maintaining good ductility.

Gwalani, Bharat↗
DOE OSTI2024

Predicting the tensile and compressive modulus of electrospun fiber mat‐reinforced hydrogels using the Halpin–Tsai equations

Abstract The reinforcement of mechanically‐weak hydrogels to yield composites with increased stiffness, strength, or toughness is a well‐established approach. In particular, introducing electrospun nanofibers into hydrogels is a common strategy for biomedical applications, as the resulting hierarchical structure mimics biology and allows for control over fiber diameter and alignment and tuning of mechanical properties. However, further study of the link between the constituent materials and the mechanical properties of the composite is uncommon. One potential model to understand the mechanical properties of fiber‐reinforced hydrogels involves the Halpin–Tsai equations, which relate the modulus values of the fibers and hydrogel matrix and the fiber volume fraction, to the modulus of the composite. To assess the application of this model to fiber‐reinforced hydrogels, predicted values were compared with experimental values from mechanical testing of a poly(ethylene glycol) (PEG) matrix reinforced with an electrospun polycaprolactone (PCL) fiber mat. Although the equations described these systems well in tension, providing a facile approach to identify a fiber volume fraction that will achieve a desired modulus, the Halpin–Tsai approach was less successful under compression. This study motivates additional investigation of the role of structural features of hydrogel composites in determining mechanical properties to enable design of materials for specific applications.

Polymer Science↗
DOE OSTI2022

Continuous fiber malleable thermoset composites with sub-1-minute dwell times; validation of impact performance and evaluation of the efficacy of the compression forming process. CRADA Final Report

Mallinda is developing polyimine malleable thermoset prepreg composite materials which have excellent mechanical properties (100 GPa tensile modulus, 2 GPA tensile strength, 2.4% elongation at break) and high operating temperatures (Tg>200°C). At scale, polyimine resins are commensurate in price with commodity epoxy resins. What distinguishes malleable thermoset prepreg from traditional thermoset prepreg materials, is that they are fully cured during Mallinda’s roll-to-roll production of prepreg laminate. This results in 5 key value-differentiating benefits. First, it simplifies manufacturing logistics by enabling ambient transportation and storage, and by significantly extending out-life and shelf-life almost indefinitely. Second, elimination of autoclave curing reduces the economic and energy costs to the customer. Third, scrap rates can be reduced as malleable thermoset prepreg materials are directly reusable. Fourth, the manufacturing consolidation step can be roughly 10x faster than traditional thermosets, because the resin is already cured. Parts can be made via compression forming by the application of heat and pressure to quickly vitrify and consolidate a multilayer part – easily leading to sub 3-minute cycle times (at lab scale we have demonstrated a 20 second dwell time, with room for further optimization). Finally, the closed-loop cradle-to-cradle solution-based recyclability of malleable thermoset composites can also contribute significantly to the future of sustainable lightweight materials. The focus of this project was the development, optimization and validation of malleable thermoset composite materials which exhibit manufacturing cycle times of 3-minute or less, high speed impact performance on par with incumbent technologies, and defect-free consolidation of 3 dimensional parts.

36 MATERIALS SCIENCE↗
DOE OSTI2018

Irradiation Enhances Strength and Deformability of Nano‐Architected Metallic Glass

The quest for radiation‐damage tolerant materials has found good candidates in nanoporous metals, whose abundance of free surfaces provides ample sinks for radiation‐induced defects, as well as in metallic glasses, whose characteristic failure via shear banding can be alleviated by irradiation. This type of catastrophic failure in metallic glass can also be suppressed by reducing their dimensions to the nanoscale. To combine the beneficial effects of resilience against irradiation in materials containing many free surfaces and nano‐sized metallic glasses, the authors fabricate Zr–Ni–Al metallic glass nano‐architecture and irradiate them with 12 MeV Ni 4+ ions. These 3D nanolattices are composed of hollow beams of sputtered metallic glass with beam wall thicknesses ≈10–100 nm, with a relative density of ≈5%, which renders them to be 20 times lighter than their bulk‐level counterparts. The authors find that the thickest‐walled nanolattices, those with a median wall thickness of ≈88 nm, are able to withstand irradiation without significant contraction; all other substantially shrunk; and collapsed upon irradiation. In situ nanomechanical experiments on the irradiated samples compressed inside a scanning electron microscope (SEM) reveal substantial improvement in mechanical response upon irradiation, with an average increase in yield strength of 35.7% and a significant enhancement in deformability. Enhanced deformability upon irradiation is apparent from the nanolattices' accommodation of larger strains before any kind of failure, as well as the presence of smaller strain bursts and stress drops throughout the stress–strain response. The irradiated nanolattices are largely intact after compression, with in situ SEM videos demonstrating a layer‐by‐layer like collapse in the irradiated nanolattices in contrast to the catastrophic failure with complete destruction of the failed layers observed in equivalent as‐fabricated samples. This work points to nano‐architected metallic glasses being a promising candidate for creating ultra‐lightweight, radiation tolerant materials, and irradiation as a promising technique for improving the mechanical response of metallic glass nanolattices with stiffness on the order of 250 MPa.

Thompson, Rachel L.↗
NASA NTRS2010

Effect of Microscopic Damage Events on Static and Ballistic Impact Strength of Triaxial Braid Composites

The reliability of impact simulations for aircraft components made with triaxial-braided carbon-fiber composites is currently limited by inadequate material property data and lack of validated material models for analysis. Methods to characterize the material properties used in the analytical models from a systematically obtained set of test data are also lacking. A macroscopic finite element based analytical model to analyze the impact response of these materials has been developed. The stiffness and strength properties utilized in the material model are obtained from a set of quasi-static in-plane tension, compression and shear coupon level tests. Full-field optical strain measurement techniques are applied in the testing, and the results are used to help in characterizing the model. The unit cell of the braided composite is modeled as a series of shell elements, where each element is modeled as a laminated composite. The braided architecture can thus be approximated within the analytical model. The transient dynamic finite element code LS-DYNA is utilized to conduct the finite element simulations, and an internal LS-DYNA constitutive model is utilized in the analysis. Methods to obtain the stiffness and strength properties required by the constitutive model from the available test data are developed. Simulations of quasi-static coupon tests and impact tests of a represented braided composite are conducted. Overall, the developed method shows promise, but improvements that are needed in test and analysis methods for better predictive capability are examined.

Littell, Justin D.↗
DOE OSTI2018

High‐Strength Nanotwinned Al Alloys with 9R Phase

Abstract Light‐weight aluminum (Al) alloys have widespread applications. However, most Al alloys have inherently low mechanical strength. Nanotwins can induce high strength and ductility in metallic materials. Yet, introducing high‐density growth twins into Al remains difficult due to its ultrahigh stacking‐fault energy. In this study, it is shown that incorporating merely several atomic percent of Fe solutes into Al enables the formation of nanotwinned (nt) columnar grains with high‐density 9R phase in Al(Fe) solid solutions. The nt Al–Fe alloy coatings reach a maximum hardness of ≈5.5 GPa, one of the strongest binary Al alloys ever created. In situ uniaxial compressions show that the nt Al–Fe alloys populated with 9R phase have flow stress exceeding 1.5 GPa, comparable to high‐strength steels. Molecular dynamics simulations reveal that high strength and hardening ability of Al–Fe alloys arise mainly from the high‐density 9R phase and nanoscale grain sizes.

Li, Qiang↗