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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 1,495 records · Page 83
All sourcesNASA NTRSDOE OSTI
DOE OSTI2019

Time-resolved imaging of atoms and molecules in laser-produced uranium plasmas

Gas-phase oxidation of uranium (U), plume chemistry, and its impact on optical emission features of the uranium plasma are investigated. Plasmas were produced via nanosecond laser ablation of a natural uranium target in a chamber where uranium oxidation was controlled by varying the oxygen partial pressure within argon cover gas. Monochromatic imaging of uranium atoms and monoxide molecules was performed using narrowband optical filters, which clearly reveals the spatio-temporal evolution of these species in the plasma. Uranium oxides are found to be formed at the plasma edges, where lower temperatures favor molecular recombination. Segregation between the distribution of uranium atoms and monoxide species is observed at later times of plasma evolution, and is more apparent at lower oxygen partial pressures. At higher oxygen partial pressures, significant variation in plume morphology is noticed for UO species, which is attributed to higher rate of oxide (UxOy) formation at the plume edges. The monochromatic images of U atoms and molecules and corresponding spectral features at various oxygen partial pressures presented here provide a unique insight into gas-phase, high-temperature uranium oxidation, and its chemistry and have implications for a wide range of nuclear applications, from stand-off detection of radioisotopes to forensics and safeguards.

(140.3440) Laser-induced breakdown, (280.4788) Opt↗
DOE OSTI2018

Impact of forging direction on the recrystallization behaviour of nickel base superalloy AD730 billet material at subsolvus temperatures

Highlights: • Large unrecrystallized grains present a fine distribution of intragranular γ′ precipitates; • Intragranular precipitates play a key role on strain distribution and subsequent recrystallization behaviour for AD730; • Continuous dynamic recrystallization (CDRX) promotes the gradual consumption of large unrecrystallized grains. • Undissolved secondary precipitates play a key role on the microstructural evolution of AD730 • No significant effect associated to the forging direction on the recrystallization behaviour of AD730 was found. AD730™ is a newly developed Ni-based superalloy for turbine disk applications produced by cast and wrought processes. Conventional ingot-to-billet conversion is an expensive and very complex operation. Because of the difficulties to achieve a uniform strain for recrystallization, large unrecrystallized grains are retained along this process. Heterogeneities of grain size have a negative impact on subsequent forging processes as well as ultrasonic inspectability of the destination part. The main aim of this work is to analyse the impact of both forging direction (billet, cogging) and strain (ε = 0.3–2) on the microstructural evolution of AD730 at subsolvus temperatures from a semi-finished product (billet) under conditions representative of both cogging and hot forging operations. Special attention to the presence of large unrecrystallized grains was paid. Double truncated cones (DTCs) were hot forged at subsolvus temperatures followed by air cooling. SEM and EBSD analysis were conducted in the as-received (billet) and the as-forged conditions. AD730 alloy presents a complex microstructure characterized by the presence of large unrecrystallized grains, aligned in the billet direction, with remarkable differences in γ′ precipitates distribution as compared to recrystallized structures. The fine distribution of primary γ′ precipitates (pinning effect) plays a key role on grain size control but also on the recrystallization behaviour. Continuous dynamic recrystallization (CDRX) mechanism was found to be operating in the large unrecrystallized grains, promoting the formation intragranular DRX grains and the gradual recrystallization of these grains. Strain presents a strong effect on the microstructural evolution of AD730, increasing the recrystallization fraction and refining the structure. By contrast, no significant effect associated to the forging direction was found. Conditions representative of cogging operations (ε ≤ 0.6) at subsolvus temperatures were translated into large fractions of unrecrystallized structures (strain accumulation).

36 MATERIALS SCIENCE↗
DOE OSTI2025

Coupled Thermo-Hydrological-Mechanical-Chemical Behavior of Anisotropic Granite for Geologic Disposal of High-Level Radioactive Waste: A Core-Scale Laboratory Investigation

The coupled thermo-hydrological-mechanical-chemical (THMC) behavior of rock within an Excavation Damaged Zone (EDZ) is critical for the safety and long-term performance of a geological repository for high-level radioactive wastes. While many laboratory experiments have been conducted to investigate EDZ rocks, the flow and deformation characteristics resulting from anisotropic rock textures and microcrack distribution under triaxial loading and elevated temperatures remain poorly understood. Particularly, cracks at various scales serve as fast paths for fluid flow and solute transport and present as focal points of mechanical weakness, which complicate the coupled THMC processes in anisotropic EDZ rocks and challenge modeling predictions. Here, in this study, a series of core-scale experiments was conducted on three granite samples under repository-relevant conditions. These rock samples were obtained from the Grimsel Underground Research Laboratory (URL), featured by anisotropic minerals (represented by bedding layers) and microcrack distributions and coarse cm-scale grain sizes. During the experiments, samples were subjected to an elevated temperature at 90 °C and different triaxial loading conditions either by radial (normal to bedding layers) or axial (parallel to bedding layers) compaction. Water was injected into the samples, and the rock permeability evolutions and effluent water chemistry were monitored closely. For intact samples, thermal expansion of minerals at 90 °C resulted in a large, 75% irreversible permeability reduction and rock strengthening under radial compaction, while thermal impact was limited to a 15% permeability reduction under axial compaction. In contrast, for a sample containing open cracks, the growth of fractures during the experiment resulted in an abrupt permeability increase and fast failure at 90 °C. The effluent water chemistry indicates much more considerable mineral dissolution from large shear sliding than that in rocks dominated by mechanical compaction. These results helped better understand the coupled THMC processes in anisotropic rocks containing cracks, evaluate the behaviors of EDZ rocks, and predict the long-term evolution of EDZ for the performance of the repositories.

Coupled THMC processes↗
DOE OSTI2021

Three influential factors on colloidal nanoparticle deposition for heat conduction enhancement in 3D chip stacks

Thermal management is one of the major challenges facing the development of three-dimensional (3D) chip stacks. Recently, experimental studies have shown that neck-based thermal structure (NTS) between chip layers formed by drying of colloidal suspension in cavity filled with micro-size particles can improve the vertical heat conduction threefold. However, a deep understanding of the mechanisms of neck formation and its influence on heat conduction is still lacking. In this paper, we numerically study the effects of three parameters, i.e., initial nanoparticle concentration, drying temperature and chip surface wettability on neck formation between filler particles and on the resulting heat conduction of the NTS. With increasing nanoparticle concentration, the size and number of necks increase, resulting in an increased effective thermal conductivity (ETC) of NTS. The drying temperature is found to have only little influence on the ETC of resultant NTS, while the neck size and spatial distribution become more uniform at higher drying temperature. When reducing the wettability of the top and bottom surfaces of the cavity, the necks shrink in size until completing evacuating at the top and bottom layers, while the size of the necks between filler particles in the middle height of the cavity expands slowly. In consequence, the ETC of NTS drops at an increasing rate. Being able to reveal the underlying multiple mechanisms of two-phase flow, phase change and heat transport, the current numerical study suggests optimal values for the deposition process, with initial nanoparticle concentration over 0.8%, a drying temperature of 60°C and a uniform contact angle of 30° for practical production of NTS.

3D chip stacks↗
DOE OSTI2025

First Temperature Profile of a Stellar Flare Using Differential Chromatic Refraction

We present the first derivation of a stellar flare temperature profile from single-band photometry. Stellar flare DWF 030225.574−545707.45129 was detected in 2015 by the Dark Energy Camera as part of the Deeper, Wider, Faster program. The brightness (Δm g = −6.12) of this flare, combined with the high air mass (1.45 ≲ X ≲ 1.75) and blue filter (DES g, 398–548 nm) in which it was observed, provided ideal conditions to measure the zenithward apparent motion of the source due to differential chromatic refraction (DCR) and, from that, infer the effective temperature of the event. We model the flare’s spectral energy distribution as a blackbody to produce the constraints on flare temperature and geometric properties derived from single-band photometry. We additionally demonstrate how simplistic assumptions on the flaring spectrum, as well as on the evolution of flare geometry, can result in solutions that overestimate the effective temperature. Exploiting DCR enables studying chromatic phenomena with ground-based astrophysical surveys, and stellar flares on M dwarfs are a particularly enticing target for such studies due to their ubiquity across the sky and the heightened color contrast between their red quiescent photospheres and the blue flare emission. Our novel method will enable similar temperature constraints for a large sample of objects in upcoming photometric surveys like the Vera C. Rubin Legacy Survey of Space and Time.

Clarke, Riley W. [University of Delaware, Newark, ↗
DOE OSTI2015

Tempo-spatial characteristics of sub-daily temperature trends in mainland China

The spatial and temporal pattern of sub-daily temperature change in mainland China was analysed for the period from 1973 to 2011 using a 3-hourly dataset based on 408 stations. The increase in surface air temperature was more significant by night between 1973 and 1992, with the fastest upward trend around local midnight being about 0.27 °C/decade, while it was more significant by day between 1992 and 2011, with the fastest upward trend being about 0.46 °C/decade in mid-late morning. The season with rapid temperature increase also shifted from winter in 1973–1992 (the largest increase happened near midnight in December, 0.75 °C/decade) to spring in 1992–2011 (the largest increase happened at in the early afternoon in March, 0.82 °C/decade). The change in the spatial distributions of the sub-daily temperature trends shows that Northeast China warmed more significantly in 1973–1992 than elsewhere, but it cooled in 1992–2011, when Southwest China was the new focus of temperature increase whereas it had previously been cooling. A preliminary analysis of the possible causes implies that changes in solar radiation, cloud cover, aerosols and the observational environments near the stations might have contributed to these observed temperature changes.

Meteorology & Atmospheric Sciences↗
DOE OSTI2019

Effect of Tempering Mode on the Microstructure and Mechanical Properties of a Lean Alloy Martensitic Steel: Conventional Reheating Versus Induction Reheating

The present study elucidates the effect of the reheating rate and tempering temperature on the type, size, and distribution of carbides/cementite formed within martensite (M)/lower bainite (LB) during the tempering of a high-strength low-alloy (HSLA) steel. A comparison is made between conventional reheating and induction reheating. All the experimental samples were quenched from the austenitization temperature of 920 °C for 30 min. An ultra-high yield strength of 1180 MPa and a good toughness of 94 J at 0 °C were obtained after tempering at 400 °C for 15 min by induction reheating (~ 100 °C/s), while in the case of conventional reheating (~ 2 °C/s) and tempering at 400 °C for 15 min, the steel had a high strength of 1159 MPa, but a poor toughness of 47 J at 0 °C. After induction reheating to 500 °C and tempering for 15 min, a higher toughness was obtained (91 J at 0 °C), but the strength was decreased to 967 MPa. Microstructural characterization revealed that fine needle-like carbides (ε-Fe{sub 2.4}C) were obtained by induction reheating to 400 °C and tempering for 15 min. However, samples tempered at 400 °C by conventional reheating and 500 °C by induction reheating both precipitated coarse θ-Fe{sub 3}C. In the former, θ-Fe{sub 3}C precipitated at locations that were previously austenite grain boundaries and led to tempered martensite embrittlement (TME). In the latter, Ostwald ripening occurred, and the precipitates could not maintain high strength. The excellent mechanical properties of induction reheated steel (400 °C, 15 min) are attributed to the following aspects: (a) The selection of appropriate tempering temperature did not lead to decarburization and ensured high strength, and (b) a high reheating rate promoted carbide dispersion and avoided TME in steel.

36 MATERIALS SCIENCE↗
DOE OSTI2016

The temperature dependence of intermediate range oxygen-oxygen correlations in liquid water

We analyze the recent temperature dependent oxygen-oxygen pair-distribution functions from experimental high-precision x-ray diffraction data of bulk water by Skinner et al. [J. Chem. Phys. 141, 214507 (2014)] with particular focus on the intermediate range where small, but significant, correlations are found out to 17 Å. The second peak in the pair-distribution function at 4.5 Å is connected to tetrahedral coordination and was shown by Skinner et al. to change behavior with temperature below the temperature of minimum isothermal compressibility. Here we show that this is associated also with a peak growing at 11 Å which strongly indicates a collective character of fluctuations leading to the enhanced compressibility at lower temperatures. We note that the peak at ∼13.2 Å exhibits a temperature dependence similar to that of the density with a maximum close to 277 K or 4 °C. We analyze simulations of the TIP4P/2005 water model in the same manner and find excellent agreement between simulations and experiment albeit with a temperature shift of ∼20 K.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2018

The effect of finish rolling temperature and tempering on the microstructure, mechanical properties and dislocation density of direct-quenched steel

Highlights: • The effect of thermomechanical treatment and tempering on direct-quenched steel has been studied. • Dislocation density of direct-quenched and tempered martensite is evaluated using both TEM and Williamson-Hall method. • Statistical analysis has been performed to study the effect of different factors on toughness of direct-quenched martensite. - Abstract: A unique batch tempering treatment for industrial scale direct-quenched steel coils has been studied using laboratory simulations. The tempering treatment was non-isothermal with slow heating to 570 °C and slow cooling to simulate the tempering of large steel coils. The paper presents the effect of finishing rolling temperature (FRT) relative to the non-recrystallization temperature (T{sub NR}) and the effect of long time tempering on the microstructure, dislocation density and mechanical properties of direct-quenched coiled strips. Conditioning austenite below the recrystallization stop temperature resulted in a finer effective grain size distribution, which correlated strongly with the impact toughness of the final product. Furthermore low finish rolling temperature resulted in partially ferritic microstructures while higher finishing rolling temperatures led to mixtures of bainite and martensite. Dislocation densities determined with TEM and XRD showed somewhat different trends regarding the effect of tempering: intra-lath dislocation density, as measured with TEM, showed a statistically significant drop in only one case, while XRD analysis indicated a drop in all cases. Furthermore, no significant correlation between finishing rolling temperature and dislocation density existed in XRD studies. The XRD results indicate that the decrease in dislocation density corresponds to about 100 MPa lower dislocation strengthening. However, precipitation hardening and potential internal micro stress relief compensates this as yield strength remains unchanged or even increases during tempering.

36 MATERIALS SCIENCE↗
DOE OSTI2015

Possible Demonstration of a Polaronic Bose-Einstein(-Mott) Condensate in UO 2(+x) by Ultrafast THz Spectroscopy and Microwave Dissipation

Bose-Einstein condensates (BECs) composed of polarons would be an advance because they would combine coherently charge, spin, and a crystal lattice. Following our earlier report of unique structural and spectroscopic properties, we now identify potentially definitive evidence for polaronic BECs in photo- and chemically doped UO 2(+x) on the basis of exceptional coherence in the ultrafast time dependent terahertz absorption and microwave spectroscopy results that show collective behavior including dissipation patterns whose precedents are condensate vortex and defect disorder and condensate excitations. Furthermore, that some of these signatures of coherence in an atom-based system extend to ambient temperature suggests a novel mechanism that could be a synchronized, dynamical, disproportionation excitation, possibly via the solid state analog of a Feshbach resonance that promotes the coherence. Such a mechanism would demonstrate that the use of ultra-low temperatures to establish the BEC energy distribution is a convenience rather than a necessity, with the actual requirement for the particles being in the same state that is not necessarily the ground state attainable by other means. Interestingly, a macroscopic quantum object created by chemical doping that can persist to ambient temperature and resides in a bulk solid would be revolutionary in a number of scientific and technological fields.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2017

County-Level Climate Uncertainty for Risk Assessments: Volume 2 Appendix A - Historical Near-Surface Air Temperature.

This report uses the CMIP5 series of climate model simulations to produce country- level uncertainty distributions for use in socioeconomic risk assessments of climate change impacts. It provides appropriate probability distributions, by month, for 169 countries and autonomous-areas on temperature, precipitation, maximum temperature, maximum wind speed, humidity, runoff, soil moisture and evaporation for the historical period (1976-2005), and for decadal time periods to 2100. It also provides historical and future distributions for the Arctic region on ice concentration, ice thickness, age of ice, and ice ridging in 15-degree longitude arc segments from the Arctic Circle to 80 degrees latitude, plus two polar semicircular regions from 80 to 90 degrees latitude. The uncertainty is meant to describe the lack of knowledge rather than imprecision in the physical simulation because the emphasis is on unfalsified risk and its use to determine potential socioeconomic impacts. The full report is contained in 27 volumes.

54 ENVIRONMENTAL SCIENCES↗
DOE OSTI2017

County-Level Climate Uncertainty for Risk Assessments: Volume 4 Appendix C - Historical Maximum Near-Surface Air Temperature.

This report uses the CMIP5 series of climate model simulations to produce country- level uncertainty distributions for use in socioeconomic risk assessments of climate change impacts. It provides appropriate probability distributions, by month, for 169 countries and autonomous-areas on temperature, precipitation, maximum temperature, maximum wind speed, humidity, runoff, soil moisture and evaporation for the historical period (1976-2005), and for decadal time periods to 2100. It also provides historical and future distributions for the Arctic region on ice concentration, ice thickness, age of ice, and ice ridging in 15-degree longitude arc segments from the Arctic Circle to 80 degrees latitude, plus two polar semicircular regions from 80 to 90 degrees latitude. The uncertainty is meant to describe the lack of knowledge rather than imprecision in the physical simulation because the emphasis is on unfalsified risk and its use to determine potential socioeconomic impacts. The full report is contained in 27 volumes.

54 ENVIRONMENTAL SCIENCES↗
DOE OSTI2017

County-Level Climate Uncertainty for Risk Assessments: Volume 6 Appendix E - Historical Minimum Near-Surface Air Temperature.

This report uses the CMIP5 series of climate model simulations to produce country- level uncertainty distributions for use in socioeconomic risk assessments of climate change impacts. It provides appropriate probability distributions, by month, for 169 countries and autonomous-areas on temperature, precipitation, maximum temperature, maximum wind speed, humidity, runoff, soil moisture and evaporation for the historical period (1976-2005), and for decadal time periods to 2100. It also provides historical and future distributions for the Arctic region on ice concentration, ice thickness, age of ice, and ice ridging in 15-degree longitude arc segments from the Arctic Circle to 80 degrees latitude, plus two polar semicircular regions from 80 to 90 degrees latitude. The uncertainty is meant to describe the lack of knowledge rather than imprecision in the physical simulation because the emphasis is on unfalsified risk and its use to determine potential socioeconomic impacts. The full report is contained in 27 volumes.

54 ENVIRONMENTAL SCIENCES↗
DOE OSTI2017

County-Level Climate Uncertainty for Risk Assessments: Volume 3 Appendix B - Forecast Near-Surface Air Temperature

This report uses the CMIP5 series of climate model simulations to produce country- level uncertainty distributions for use in socioeconomic risk assessments of climate change impacts. It provides appropriate probability distributions, by month, for 169 countries and autonomous-areas on temperature, precipitation, maximum temperature, maximum wind speed, humidity, runoff, soil moisture and evaporation for the historical period (1976-2005), and for decadal time periods to 2100. It also provides historical and future distributions for the Arctic region on ice concentration, ice thickness, age of ice, and ice ridging in 15-degree longitude arc segments from the Arctic Circle to 80 degrees latitude, plus two polar semicircular regions from 80 to 90 degrees latitude. The uncertainty is meant to describe the lack of knowledge rather than imprecision in the physical simulation because the emphasis is on unfalsified risk and its use to determine potential socioeconomic impacts. The full report is contained in 27 volumes.

54 ENVIRONMENTAL SCIENCES↗
DOE OSTI2017

County-Level Climate Uncertainty for Risk Assessments: Volume 7 Appendix F - Forecast Minimum Near-Surface Air Temperature

This report uses the CMIP5 series of climate model simulations to produce country- level uncertainty distributions for use in socioeconomic risk assessments of climate change impacts. It provides appropriate probability distributions, by month, for 169 countries and autonomous-areas on temperature, precipitation, maximum temperature, maximum wind speed, humidity, runoff, soil moisture and evaporation for the historical period (1976-2005), and for decadal time periods to 2100. It also provides historical and future distributions for the Arctic region on ice concentration, ice thickness, age of ice, and ice ridging in 15-degree longitude arc segments from the Arctic Circle to 80 degrees latitude, plus two polar semicircular regions from 80 to 90 degrees latitude. The uncertainty is meant to describe the lack of knowledge rather than imprecision in the physical simulation because the emphasis is on unfalsified risk and its use to determine potential socioeconomic impacts. The full report is contained in 27 volumes.

54 ENVIRONMENTAL SCIENCES↗