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Delving into the depths of NGC 3783 with XRISM II. Cross-calibration of X-ray instruments used in the large, multi-mission observational campaign

Context. Accurate X-ray spectroscopic measurements are fundamental for deriving basic physical parameters of the most abundant baryon components in the Universe. The plethora of X-ray observatories currently operational enables a panchromatic view of the high-energy emission of celestial sources. However, uncertainties in the energy-dependent calibration of the instrument transfer functions (e.g. the effective area, energy redistribution, or gain) can limit - and historically, did limit - the accuracy of X-ray spectroscopic measurements. Aims. We revised the status of the cross-calibration among the scientific payload on board four operation missions: Chandra, NuSTAR, XMM-Newton, and the recently launched XRISM. XRISM carries the micro-calorimeter Resolve, which yields the best energy resolution at energies ≥2 keV. For this purpose, we used the data from a 10-day-long observational campaign targeting the nearby active galactic nucleus NGC 3783, carried out in July 2024. Methods. We present a novel model-independent method for assessing the cross-calibration status that is based on a multi-node spline of the spectra with the highest-resolving power (XRISM/Resolve in our campaign). We also estimated the impact of the intrinsic variability of NGC 3783 on the cross-calibration status due to the different time coverages of participating observatories and performed an empirical reassessment of the Resolve throughput at low energies. Results. Based on this analysis, we derived a set of energy-dependent correction factors of the observed responses, enabling a statistically robust analysis of the whole spectral dataset. They will be employed in subsequent papers describing the astrophysical results of the campaign. Aims. We revised the status of the cross-calibration among the scientific payload on board four operation missions: Chandra, NuSTAR, XMM-Newton, and the recently launched XRISM. XRISM carries the micro-calorimeter Resolve, which yields the best energy resolution at energies ≥2 keV. For this purpose, we used the data from a 10-day-long observational campaign targeting the nearby active galactic nucleus NGC 3783, carried out in July 2024. Methods. We present a novel model-independent method for assessing the cross-calibration status that is based on a multi-node spline of the spectra with the highest-resolving power (XRISM/Resolve in our campaign). We also estimated the impact of the intrinsic variability of NGC 3783 on the cross-calibration status due to the different time coverages of participating observatories and performed an empirical reassessment of the Resolve throughput at low energies. Results. Based on this analysis, we derived a set of energy-dependent correction factors of the observed responses, enabling a statistically robust analysis of the whole spectral dataset. They will be employed in subsequent papers describing the astrophysical results of the campaign.

Active Galactic Nuclei, individual: NGC 3783↗

Radioactive source calibration test of the CMS Hadron Endcap Calorimeter test wedge with Phase I upgrade electronics

The Phase I upgrade of the CMS Hadron Endcap Calorimeters consists of new photodetectors (Silicon Photomultipliers in place of Hybrid Photo-Diodes) and front-end electronics. The upgrade will eliminate the noise and the calibration drift of the Hybrid Photo-Diodes and enable the mitigation of the radiation damage of the scintillators and the wavelength shifting fibers with a larger spectral acceptance of the Silicon Photomultipliers. The upgrade also includes increased longitudinal segmentation of the calorimeter readout, which allows pile-up mitigation and recalibration due to depth-dependent radiation damage. As a realistic operational test, the responses of the Hadron Endcap Calorimeter wedges were calibrated with a $^{60}$Co radioactive source with upgrade electronics. The test successfully established the procedure for future source calibrations of the Hadron Endcap Calorimeters. Lastly we describe the instrumentation details and the operational experiences related to the sourcing test.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Production rate calibration for cosmogenic 10 Be in pyroxene by applying a rapid fusion method to 10 Be-saturated samples from the Transantarctic Mountains, Antarctica

Measurements of multiple cosmogenic nuclides in a single sample are valuable for various applications of cosmogenic nuclide exposure dating and allow for correcting exposure ages for surface weathering and erosion and establishing exposure–burial history. Here we provide advances in the measurement of cosmogenic 10 Be in pyroxene and constraints on the production rate that provide new opportunities for measurements of multi-nuclide systems, such as 10 Be/ 3 He, in pyroxene-bearing samples. We extracted and measured cosmogenic 10 Be in pyroxene from two sets of Ferrar Dolerite samples collected from the Transantarctic Mountains in Antarctica. One set of samples has 10 Be concentrations close to saturation, which allows for the production rate calibration of 10 Be in pyroxene by assuming production–decay equilibrium. The other set of samples, which has a more recent exposure history, is used to determine if a rapid fusion method can be successfully applied to samples with Holocene to Last Glacial Maximum exposure ages. From measured 10 Be concentrations in the near-saturation sample set we find the production rate of 10 Be in pyroxene to be 3.74 ± 0.10 atoms g -1 yr -1 , which is consistent with 10 Be/ 3 He paired nuclide ratios from samples assumed to have simple exposure. Given the high 10 Be concentration measured in this sample set, a sample mass of ~ 0.5 g of pyroxene is sufficient for the extraction of cosmogenic 10 Be from pyroxene using a rapid fusion method. However, for the set of samples that have low 10 Be concentrations, measured concentrations were higher than expected. We attribute spuriously high 10 Be concentrations to failure in removing all meteoric 10 Be and/or a highly variable and poorly quantified procedural blank background correction.

58 GEOSCIENCES↗

Statistically Rigorous Uncertainty Quantification for Physical Parameter Model Calibration with Functional Output

In experiments conducted on the Z-machine at Sandia National Laboratories, dynamic material properties cannot be analyzed using traditional analytic methods, necessitating solving an inverse problem. Bayesian model calibration is a statistical framework for solving an inverse problem to estimate parameters input into a computational model in the presence of multiple uncertainties. Disentangling input parameter uncertainty and model misspecification is often poorly identified problem. When using computational models for physical parameter estimation, the issue of parameter identifiability must be carefully considered to obtain accurate and precise estimates of physical parameters. Additionally, in dynamic material properties applications, the experimental output is a function, velocity over time. While we can sample an arbitrarily large number of points from the measured velocity, these curves only contain a finite amount of information about the calibration parameters. In this report, we propose modifications to the Bayesian model calibration framework to simplify and improve the estimation of physical parameters with functional outputs. Specifically, we propose scaling the likelihood function by an effective sample size rather than modeling the discrepancy function; and modularizing input nuisance parameters with weakly identified parameters. We evaluate the performance of these proposed methods using a statistical simulation study and then apply these methods to estimate parameters of the tantalum equation of state. We conclude that these proposed methods can provide simple, fast, and statistically valid alternatives to the full Bayesian model calibration procedure; and that these methods can be used to estimate parameters of the equation of state for tantalum.

97 MATHEMATICS AND COMPUTING↗

Calibration and Measurement in Turbulence Research by the Hot-Wire Method

The problem of turbulence in aerodynamics is at present being attacked both theoretically and experimentally. In view of the fact however that purely theoretical considerations have not thus far led to satisfactory results the experimental treatment of the problem is of great importance. Among the different measuring procedures the hot wire methods are so far recognized as the most suitable for investigating the turbulence structure. The several disadvantages of these methods however, in particular those arising from the temperature lag of the wire can greatly impair the measurements and may easily render questionable the entire value of the experiment. The name turbulence is applied to that flow condition in which at any point of the stream the magnitude and direction of the velocity fluctuate arbitrarily about a well definable mean value. This fluctuation imparts a certain whirling characteristic to the flow.

Kovasznay, Kaszlo↗

A Novel Non-Intrusive Method to Resolve the Thermal-Dome-Effect of Pyranometers: Radiometric Calibration and Implications

Traditionally the calibration equation for pyranometers assumes that the measured solar irradiance is solely proportional to the thermopile's output voltage; therefore only a single calibration factor is derived. This causes additional measurement uncertainties because it does not capture sufficient information to correctly account for a pyranometer's thermal effect. In our updated calibration equation, temperatures from the pyranometer's dome and case are incorporated to describe the instrument's thermal behavior, and a new set of calibration constants are determined, thereby reducing measurement uncertainties. In this paper, we demonstrate why a pyranometer's uncertainty using the traditional calibration equation is always larger than a-few-percent, but with the new approach can become much less than 1% after the thermal issue is resolved. The highlighted calibration results are based on NIST-traceable light sources under controlled laboratory conditions. The significance of the new approach lends itself to not only avoiding the uncertainty caused by a pyranometer's thermal effect but also the opportunity to better isolate and characterize other instrumental artifacts, such as angular response and non-linearity of the thermopile, to further reduce additional uncertainties. We also discuss some of the implications, including an example of how the thermal issue can potentially impact climate studies by evaluating aerosol's direct-radiative effect using field measurements with and without considering the pyranometer's thermal effect. The results of radiative transfer model simulation show that a pyranometer's thermal effect on solar irradiance measurements at the surface can be translated into a significant alteration of the calculated distribution of solar energy inside the column atmosphere.

Ji, Qiang↗

Ground and flight calibration assessment of HiRAP accelerometer data from missions STS-35 and STS-40

A method of removing non-aerodynamic signals and calibrating the High Resolution Accelerometer Package (HiRAP) flight data was developed and is discussed for Shuttle Orbiter missions STS-35 and STS-40. These two mission data sets were analyzed using ground (dynamic) calibration data and flight calibrations using a flight calibration technique that was developed and refined over the HiRAP operational lifetime. This technique evolved early in the flight program, since it was recognized that ground calibration factors are insufficient to determine absolute low acceleration levels. The application of flight calibration factors to the data sets from these missions produced calibrated acceleration levels within an accuracy of less than plus or minus 1.5 micro-g of zero during a time in the flight when the acceleration level was known to be less than 1 micro-g. This analysis further confirms the theory that flight calibrations are required in order to obtain the absolute measurement of low-frequency, low-acceleration flight signals.

Blanchard, Robert C.↗

Closing the Accuracy Gap in Tandem Photovoltaic Testing: An Accessible and Efficient Spectral Tuning Method Using LED-Based Simulators for Research Laboratories and Industry

Accurate performance calibration of multijunction (MJ) solar cells is critical for advancing this technology toward large-scale terrestrial application, yet existing testing methods developed by photovoltaics calibration laboratories remain prohibitively complex and resource intensive for most research laboratories. Current approaches rely on expensive multisource simulators and/or intricate spectral tuning algorithms, limiting accessibility and hindering standardized comparisons of emerging MJ technologies such as perovskite-based tandems. This paper introduces a streamlined spectral irradiance adjustment method for light-emitting diode (LED)-based solar simulators, which are increasingly adopted in the photovoltaics community due to their versatility and cost-effectiveness. The method we present bins LED channels into groups based on the number of junctions of the MJ photovoltaic device under test (DUT) and their corresponding band gaps and incorporates an automated tuning algorithm that eliminates the need to adjust each channel’s irradiance individually. This tuning algorithm requires the relative spectral responsivities of both the DUT and a broadband reference cell, as well as a calibrated spectroradiometer. Measurement validation across various MJ devices, including III-V and perovskite/silicon tandems, demonstrates excellent agreement within 1% with well-established xenon-tungsten multisource simulators and associated tuning algorithms. By enabling precise spectral tuning with readily available equipment and a simple tuning algorithm, our approach bridges the measurement accuracy gap between research laboratories and accredited testing facilities, fostering more reliable device comparisons and accelerating the translation of MJ technologies into real-world energy systems.

14 SOLAR ENERGY↗

Kinetic parameters of the GUINEVERE reference configuration in VENUS-F reactor obtained from a pile noise experiment using Rossi and Feynman methods

A pile noise measurement campaign has been conducted by the CEA in the VENUS-F reactor (SCK-CEN, Mol Belgium) in April 2011 in the reference critical configuration of the GUINEVERE experimental program. The experimental setup made it possible to estimate the core kinetic parameters: the prompt neutron decay constant, the delayed neutron fraction and the generation time. A precise assessment of these constants is of prime importance. In particular, the effective delayed neutron fraction is used to normalize and compare calculated reactivities of different subcritical configurations, obtained by modifying either the core layout or the control rods position, with experimental ones deduced from the analysis of measurements. This paper presents results obtained with a CEA-developed time stamping acquisition system. Data were analyzed using Rossi-α and Feynman-α methods. Results were normalized to reactor power using a calibrated fission chamber with a deposit of Np-237. Calculated factors were necessary to the analysis: the Diven factor was computed by the ENEA (Italy) and the power calibration factor by the CNRS/IN2P3/LPC Caen. Results deduced with both methods are consistent with respect to calculated quantities. Recommended values are given by the Rossi-α estimator, that was found to be the most robust. The neutron generation time was found equal to 0.438 ± 0.009 μs and the effective delayed neutron fraction is 765 ± 8 pcm. Discrepancies with the calculated value (722 pcm, calculation from ENEA) are satisfactory: -5.6% for the Rossi-α estimate and -2.7% for the Feynman-α estimate. (authors)

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

Bayesian calibration of bubble size dynamics applied to CO 2 gas fermenters

To accelerate the scale-up of gaseous CO 2 fermentation reactors, computational models need to predict gas-to-liquid mass transfer which requires capturing the bubble size dynamics, i.e. bubble breakup and coalescence. However, the applicability of existing models beyond air–water mixtures remains to be established. Here, an inverse modeling approach, accelerated with a neural network surrogate, calibrates the breakup and coalescence closure models, that are used in class methods for population balance modeling (PBM). The calibration is performed based on experimental results obtained in a CO 2 -air–water-coflowing bubble column reactor. Bayesian inference is used to account for noise in the experimental dataset and bias in the simulation results. To accurately capture gas holdup and interphase mass transfer, the results show that the breakage rate needs to be increased by one order of magnitude. In conclusion, the inferred model parameters are then used on a separate configuration and shown to also improve bubble size distribution predictions.

09 BIOMASS FUELS↗

Transportable absolute yields of underground nuclear explosions. Application to the North Korean nuclear tests

The method developed and presented here improves our nuclear explosion monitoring capability by providing a new independent and transportable method to determine the explosive yields of seismically recorded events associated with foreign weapons development. Here we report new independent absolute yield and depth of burial estimates of the North Korean nuclear tests which are commensurate with previously determined source parameters. The key advantage of this method over other methods which estimate absolute explosive yields is that this method does not require any a priori calibration, and can be immediately applied to any region of interest. This method uses the source information obtained from the spectral ratios of envelopes of measured seismic coda waves to invert for model-derived yield and depth of burial. The only requirements of this method are that the region of interest must contain several (> 3) seismic sources which have been well recorded (SNR > 2) by a set of shared stations. For regions with only a few events (~ 3) and/or extremely band-limited observations for which the depth of burial is unknown, an earthquake with a known magnitude may be required to obtain an accurate and robust yield estimate.

45 MILITARY TECHNOLOGY, WEAPONRY, AND NATIONAL DEF↗

Comparison of three thrust calculation methods using in-flight thrust data

The gross thrust of an experimental airplane was determined by each method using the same flight maneuvers and generally the same data parameters. Coefficients determined from thrust stand calibrations for each of the three methods were then extrapolated to cruise flight conditions. The values of total aircraft gross thrust calculated by the three methods for cruise flight conditions agreed within + or - 3 percent. The disagreement in the values of thrust calculated by the different techniques manifested itself as a bias in the data. There was little scatter (0.5 percent) for the thrust levels examined in flight.

Hughes, D. L.↗

Calibration-free analysis of Li isotope ratios using laser ablation and laser absorption spectroscopy

We introduce a rapid, calibration-free, all-optical method for high-precision lithium isotope ratio measurements in solid materials using laser ablation combined with tunable laser absorption spectroscopy. A new asynchronous acquisition method is used to acquire time-resolved, high-resolution spectra of the 6Li and 7Li D1 and D2 transitions near 671 nm. Isotope ratios and atomic column densities are extracted from measured spectra via a physics-based fitting model including hyperfine structure. Under 1 Torr air, spectra recorded = 0.75 ms after plasma onset exhibit narrow linewidths corresponding to Doppler temperatures = 400 K, enabling resolution of the isotope peaks with high signal-to-noise ratios. Analysis of LiAlO2 samples with varying 6Li:7Li ratios demonstrates isotopic precisions of 0.6–1.7% for spectra acquired in 30 s. Isotope ratios determined from the spectral fits show accuracy within –0.3% to –1.7% of reference ICP-MS measurements without requiring calibration to external standards. By eliminating sample preparation and enabling spatially resolved isotopic mapping, this method offers a rapid analysis approach to lithium isotope determination in solid materials relevant to nuclear energy, safeguards, and geochemistry.

Phillips, Mark C.↗

Detector calibration using through going and stopping muons in the MicroBooNE LArTPC

The MicroBooNE experiment at Fermilab uses a liquid argon time projection chamber (LArTPC) in the Booster Neutrino Beam to search for anomalous production of electron-neutrino-like events and to study neutrino-argon cross sections in the 1 GeV neutrino energy regime. The detector operates at 0.273 kV/cm drift electric field and its TPC has an active mass of 85 tons of liquid argon. One of the main advantages of the LArTPC technology is its ability to reconstruct both particle track direction and energy with very high precision. Effects such as misconfigured or cross-connected TPC wires, space charge effects, electron attenuation, diffusion, and recombination can worsen the energy resolution of the detector. Therefore the detector calibration is of utmost importance to get the correct dE/dx (energy loss per unit track length) measurement. This is crucial for particle identification and in particular the separation of electrons and photons, essential for oscillation analyses. Here we describe a method developed for MicroBooNE to calibrate the detector by correcting for the above mentioned effects. In this analysis first we make the detector response uniform throughout the detector and time using through-going muons. Next stopping muons are used to determine the energy scale and convert dQ/dx to dE/dx.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Analysis and Evaluation of NASA's MK40B Six-Component TASK Balance

The paper discusses the physical characteristics NASA's MK40B TASK balance. It is NASA's newest TASK balance that was optimized for the testing of wind tunnel models in the NASA Ames 11-ft Transonic Wind Tunnel. The calibration data of the MK40B balance was obtained in Calspan's Automatic Balance Calibration System. A machine load schedule design was used for the calibration that was developed at the NASA Ames Balance Calibration Laboratory. The calibration data was analyzed using both the Non-Iterative Method and the Iterative Method. Then, the chosen regression models of the calibration data were assessed and compared using the percent contribution, the variance inflation factor, and the calibration load residuals. Interactions of single-component loads were also quantified. In addition, the bi-directional characteristics of the six gage outputs of the balance were assessed by applying a semi-empirical test that was developed at the Ames Balance Calibration Laboratory. It was concluded that four of the six gages of the balance have bi-directional characteristics. Finally, the accuracy of the load prediction equations of the balance was tested by applying the equations to independent check load data that was obtained at the NASA Ames Balance Calibration Laboratory. The standard deviation of the check load residuals met expectations. The check load data also confirmed that the interactions of the forward and aft normal forces on the axial force gage output are very small. - This paper is to be presented in the invited special session titled: "65 Years of TASK Wind Tunnel Balances - Past, Present, and Future".

wind tunnel balance↗

Application of Gaussian Mixture Regression for the Correction of Low Cost PM2.5 Monitoring Data in Accra, Ghana

Low-cost sensors (LCSs) for air quality monitoring have enormous potential to improve air quality data coverage in resource-limited parts of the world such as sub-Saharan Africa. LCSs, however, are affected by environment and source conditions. To establish high-quality data, LCSs must be collocated and calibrated with reference grade PM2.5 monitors. From March 2020, a low-cost PurpleAir PM2.5 monitor was collocated with a Met One Beta Attenuation Monitor 1020 in Accra, Ghana. While previous studies have shown that multiple linear regression (MLR) and random forest regression (RF) can improve accuracy and correlation between PurpleAir and reference data, MLR and RF yielded suboptimal improvement in the Accra collocation (R2 = 0.81 and R2 = 0.81, respectively). We present the first application of Gaussian mixture regression (GMR) to air quality data calibration and demonstrate improvement over traditional methods by increasing the collocated PM2.5 correlation and accuracy to R2 = 0.88 and MAE = 2.2 μg/cu. m. Gaussian mixture models (GMMs) are a probability density estimator and clustering method from which nonlinear regressions that tolerate missing inputs can be derived. We find that even when given missing inputs, GMR provides better correlation than MLR and RF performed with complete data. GMR also allows us to estimate calibration certainty. When evaluated, 95% confidence intervals agreed with reference PM2.5 data 96% of the time, suggesting that the model accurately assesses its own confidence. Additionally, clustering within the GMM is consistent with climate characteristics, providing confidence that the calibration approach can learn underlying relationships in data.

Sensors↗