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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 1,585 records · Page 88
All sourcesNASA NTRSDOE OSTI
DOE OSTI2019

A multi-scale calibration approach for process-oriented aggregated building energy demand models

Long-term energy planning relies largely on projections of future energy demand and hourly load profiles. Aggregate building models are increasingly being utilized to characterize the sensitivity of current and future building stocks to changes in climate, population, and building technology on city-to-regional-to-national scales. Due to challenges in the availability of data, those analyses have been limited to projection of energy demand at a single scale, usually state or country, while long-term planning power system models and production cost models might operate at different spatial scales such as energy regions which are focused on ensuring adequate generation infrastructure. In this work, we propose and evaluate a novel method to calibrate an aggregate building energy demand model (PNNL’s BEND model) against the best available data at the spatial scale of balancing authorities. This approach extends previous work on aggregated building energy demand by facilitating analysis of building energy demand across scales, in particular policy and operational decision-making scales. We show that the bias-corrected model estimates building electric loads reasonably well compared with estimates from a statistical model, but has the additional feature of flexibility across spatial scales. While the calibration approach is presently U.S.-centric and associated with U.S. energy regions, it can be extrapolated to other worldwide regions with similar scale challenges between policy and operational implementation decision making. We discuss the significant challenges involved in formulating and calibrating a complex physical model based on simulations of roughly 100,000 individual buildings against available aggregate regional electric load data and highlight areas for potential future work and improved data collection.

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗
DOE OSTI2020

Modified alkaline peroxide pretreatment: An efficient path forward for bioethanol production from bamboo

To overcome the typical delignification saturation point of alkaline peroxide pretreatment and further facilitate lignin removal, a novel modified alkaline hydrogen peroxide pretreatment (MAHP) was proposed by introducing ethanol into the reaction system. The dosages of H 2 O 2 , ethanol, and pretreatment temperature were optimized, and the results revealed that a maximum lignin removal as high as 79.25% could be achieved at only 100 °C, 3 wt% H 2 O 2 concentration and 1 wt% ethanol concentration. Meanwhile, 76.5% of glucan and 56.0% of xylan were preserved at this pretreatment condition. By overcoming the delignification saturation point, enzymatic hydrolysis efficiency was remarkably enhanced, achieving 96.76% and 97.38% of glucan and xylan conversion, respectively, which are 7.4 and 11.4 times as compared to that of the untreated bamboo. Furthermore, the simultaneous saccharification and fermentation (SSF) result indicated an identical ethanol yield of ~75% when elevating the SSF solid loading from 5% to 30%. Based on the sequential SSF and xylose fermentation results, about 5.6 tons of bamboo would be consumed to produce 1 ton of ethanol. Finally, the energy balance revealed that a positive balance of 1255.4 KJ could be generated via processing 1 kg bamboo. Here, the results demonstrate that the MAHP is a promising high-efficiency pretreatment technology for bamboo due to the mild pretreatment severity and robust ethanol yield.

30 DIRECT ENERGY CONVERSION↗
DOE OSTI2025

A Scalable Hardware-and-Human-in-the-Loop Grid-interactive Efficient Building Equipment Performance Dataset

This project developed a publicly available, high-fidelity dataset about the interactions among humans, homes, and heat pumps supporting grid interactive efficient buildings to balance demand on the grid with comfort for occupants. Laboratory measurements and simulations of the hardware capture the second-scale electric power dynamics of heat pumps providing grid services like load shifting and load shedding. Field measurements, behavior tracking, and qualitative surveys of people in their homes over multiple years—including experimentally adjusting the heating and cooling system to provide grid services—to capture the reciprocal effect of human behavior on grid services, and grid services on human comfort. Taken together, these data capture the complete Hardware and Human in the loop system for residential heat pumps, reducing large uncertainties in simulation for design, and models for control of heat pumps, and grid-interactive buildings.

24 POWER TRANSMISSION AND DISTRIBUTION↗
NASA NTRS1989

How gravity and joint scaling affect dynamics response

If a scale model of a space structure is ground tested to establish dynamic characteristics of full-scale space structure, two factors need to be taken into consideration: the joint tolerances may not be scaled, and joint preloads (from gravity) may be present. In some situations, these differences may significantly affect dynamic response so that the model is not representative of the structure in space. In this study, joint effects are investigated by considering the response of a single-degree-of-freedom system that is restrained by a joint linkage. The joint is characterized by its initial stiffness, the load at which it slips, its hardening rate, and the distance it can slip (joint 'slop' or gap). The steady-state response of the system is calculated using a harmonic balance approach. It is found that the system response is multivalued for certain ranges of gap dimensions. When this is the case, small changes in system properties can lead to large differences in dynamic response and make it difficult to obtain meaningful results directly from model testing.

Hsu, S. T.↗
NASA NTRS1995

Affect of Brush Seals on Wave Rotor Performance Assessed

The NASA Lewis Research Center's experimental and theoretical research shows that wave rotor topping can significantly enhance gas turbine engine performance levels. Engine-specific fuel consumption and specific power are potentially enhanced by 15 and 20 percent, respectively, in small (e.g., 400 to 700 hp) and intermediate (e.g., 3000 to 5000 hp) turboshaft engines. Furthermore, there is potential for a 3- to 6-percent specific fuel consumption enhancement in large (e.g., 80,000 to 100,000 lbf) turbofan engines. This wave-rotor-enhanced engine performance is accomplished within current material-limited temperature constraints. The completed first phase of experimental testing involved a three-port wave rotor cycle in which medium total pressure inlet air was divided into two outlet streams, one of higher total pressure and one of lower total pressure. The experiment successfully provided the data needed to characterize viscous, partial admission, and leakage loss mechanisms. Statistical analysis indicated that wave rotor product efficiency decreases linearly with the rotor to end-wall gap, the square of the friction factor, and the square of the passage of nondimensional opening time. Brush seals were installed to further minimize rotor passage-to-cavity leakage. The graph shows the effect of brush seals on wave rotor product efficiency. For the second-phase experiment, which involves a four-port wave rotor cycle in which heat is added to the Brayton cycle in an external burner, a one-dimensional design/analysis code is used in conjunction with a wave rotor performance optimization scheme and a two-dimensional Navier-Stokes code. The purpose of the four-port experiment is to demonstrate and validate the numerically predicted four-port pressure ratio versus temperature ratio at pressures and temperatures lower than those that would be encountered in a future wave rotor/demonstrator engine test. Lewis and the Allison Engine Company are collaborating to investigate wave rotor integration in an existing turboshaft engine. Recent theoretical efforts include simulating wave rotor dynamics (e.g., startup and load-change transient analysis), modifying the one-dimensional wave rotor code to simulate combustion internal to the wave rotor, and developing an analytical wave rotor design/analysis tool based on macroscopic balances for parametric wave rotor/engine analysis.

Source record↗
DOE OSTI2011

A turbulent transport network model in MULTIFLUX coupled with TOUGH2

A new numerical method is described for the fully iterated, conjugate solution of two discrete submodels, involving (a) a transport network model for heat, moisture, and airflows in a high-permeability, air-filled cavity; and (b) a variably saturated fractured porous medium. The transport network submodel is an integrated-parameter, computational fluid dynamics solver, describing the thermal-hydrologic transport processes in the flow channel system of the cavity with laminar or turbulent flow and convective heat and mass transport, using MULTIFLUX. The porous medium submodel, using TOUGH2, is a solver for the heat and mass transport in the fractured rock mass. The new model solution extends the application fields of TOUGH2 by integrating it with turbulent flow and transport in a discrete flow network system. We present demonstrational results for a nuclear waste repository application at Yucca Mountain with the most realistic model assumptions and input parameters including the geometrical layout of the nuclear spent fuel and waste with variable heat load for the individual containers. The MULTIFLUX and TOUGH2 model elements are fully iterated, applying a programmed reprocessing of the Numerical Transport Code Functionalization model-element in an automated Outside Balance Iteration loop. The natural, convective airflow field and the heat and mass transport in a representative emplacement drift during postclosure are explicitly solved in the new model. The results demonstrate that the direction and magnitude of the air circulation patterns and all transport modes are strongly affected by the heat and moisture transport processes in the surrounding rock, justifying the need for a coupled, fully iterated model solution such as the one presented in the paper.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗
DOE OSTI2024

Evaluating SWAT + model uncertainties for human and natural outcomes: Application in a Great Lakes agricultural watershed

Nutrient exports from agricultural lands in the Great Lakes Region pose significant threats to water quality and ecological health through eutrophication, hypoxia, and harmful algal blooms. Climate change and agricultural adaptation practices complicate future nutrient loading due to intensified hydrologic cycles and land use decisions. Our research focuses on evaluating the Soil and Water Assessment Tool (SWAT) plus model parametric uncertainties for human and natural outcomes across different scales. These factors are integral to ensuring a balance between productive agricultural practices and maintaining the health of watershed hydrology. However, uncertainties in modeling such complex interactions pose significant challenges, limiting our ability to precisely determine critical factors that influence crop yield and soil moisture. Our analysis employs Sobol global sensitivity analysis to evaluate first-order, second order, and total-order indices for SWAT crop growth parameter, ensuring comprehensive assessment of individual and interactive effects on model outputs. The objective is to identify the parameters that significantly affect model outputs for crop yield and soil moisture and improve our understanding of their interactions at the basin and hydrological response unit (HRU) scale. Our case study, the Portage River Watershed, which drains into Lake Erie, is chosen to better capture finer scale interactions crucial for predicting nutrient loading under future climate scenarios. This foundational work is aimed at setting the stage for the future development of an agent-based model (ABM). The ABM model would incorporate SWAT outputs to dynamically simulate decision-making processes.

Bunyon, Enock↗
NASA NTRS2016

James Webb Space Telescope Integrated Science Instrument Module Thermal Vacuum Thermal Balance Test Campaign at NASA's Goddard Space Flight Center

The James Webb Space Telescope is a large infrared telescope with a 6.5-meter primary mirror, designed as a successor to the Hubble Space Telescope when launched in 2018. Three of the four science instruments contained within the Integrated Science Instrument Module (ISIM) are passively cooled to their operational temperature range of 36K to 40K with radiators, and the fourth instrument is actively cooled to its operational temperature of approximately 6K. Thermal-vacuum testing of the flight science instruments at the ISIM element level has taken place in three separate highly challenging and extremely complex thermal tests within a gaseous helium-cooled shroud inside Goddard Space Flight Centers Space Environment Simulator. Special data acquisition software was developed for these tests to monitor over 1700 flight and test sensor measurements, track over 50 gradients, component rates, and temperature limits in real time against defined constraints and limitations, and guide the complex transition from ambient to final cryogenic temperatures and back. This extremely flexible system has proven highly successful in safeguarding the nearly $2B science payload during the 3.5-month-long thermal tests. Heat flow measurement instrumentation, or Q-meters, were also specially developed for these tests. These devices provide thermal boundaries o the flight hardware while measuring instrument heat loads up to 600 mW with an estimated uncertainty of 2 mW in test, enabling accurate thermal model correlation, hardware design validation, and workmanship verification. The high accuracy heat load measurements provided first evidence of a potentially serious hardware design issue that was subsequently corrected. This paper provides an overview of the ISIM-level thermal-vacuum tests and thermal objectives; explains the thermal test configuration and thermal balances; describes special measurement instrumentation and monitoring and control software; presents key test thermal results; lists problems encountered during testing and lessons learned.

JWST ISIM Thermal↗
DOE OSTI2017

Techno-Economic Analysis of a Secondary Air Stripper Process

We present results of an initial techno-economic assessment on a post-combustion CO2 capture process developed by the Center for Applied Energy Research (CAER) at the University of Kentucky using Mitsubishi Hitachi Power Systems’ H3-1 aqueous amine solvent. The analysis is based on data collected at a 0.7 MWe pilot unit combined with laboratory data and process simulations. The process adds a secondary air stripper to a conventional solvent process, which increases the cyclic loading of the solvent in two ways. First, air strips additional CO2 from the solvent downstream of the conventional steam-heated thermal stripper. This extra stripping of CO2 reduces the lean loading entering the absorber. Second, the CO2-enriched air is then sent to the boiler for use as secondary air. This recycling of CO2 results in a higher concentration of CO2 in the flue gas sent to the absorber, and hence a higher rich loading of the solvent exiting the absorber. A process model was incorporated into a full-scale supercritical pulverized coal power plant model to determine the plant performance and heat and mass balances. The performance and heat and mass balance data were used to size equipment and develop cost estimates for capital and operating costs. Lifecycle costs were considered through a levelized cost of electricity (LCOE) assessment based on the capital cost estimate and modeled performance. The results of the simulations show that the CAER process yields a regeneration energy of 3.12 GJ/t CO2, a $53.05/t CO2 capture cost, and LCOE of $174.59/MWh. This compares to the U.S. Department of Energy’s projected costs (Case 10) of regeneration energy of 3.58 GJ/t CO2 , a $61.31/t CO2 capture cost, and LCOE of $189.59/MWh. For H3-1, the CAER process results in a regeneration energy of 2.62 GJ/tCO2 with a stripper pressure of 5.2 bar, a capture cost of $46.93/t CO2, and an LCOE of $164.33/MWh.

29 ENERGY PLANNING, POLICY, AND ECONOMY↗
DOE OSTI2011

Synthesis-Structure-Performance Correlation for Polyaniline-Me-C Non-Precious Metal Cathode Catalysts for Oxygen Reduction in Fuel Cells

In this report, we present the systematic preparation of active and durable non-precious metal catalysts (NPMCs) for the oxygen reduction reaction in polymer electrolyte fuel cells (PEFCs) based on the heat treatment of polyaniline/metal/carbon precursors. Variation of the synthesis steps, heat-treatment temperature, metal loading, and the metal type in the synthesis leads to markedly different catalyst activity, speciation, and morphology. Microscopy studies demonstrate notable differences in the carbon structure as a function of these variables. Balancing the need to increase the catalyst's degree of graphitization through heat treatment versus the excessive loss of surface area that occurs at higher temperatures is a key to preparing an active catalyst. XPS and XAFS spectra are consistent with the presence of Me-N{sub x} structures in both the Co and Fe versions of the catalyst, which are often proposed to be active sites. The average speciation and coordination environment of nitrogen and metal, however, depends greatly on the choice of Co or Fe. Taken together, the data indicate that better control of the metal-catalyzed transformations of the polymer into new graphitized carbon forms in the heat-treatment step will allow for even further improvement of this class of catalysts.

30 DIRECT ENERGY CONVERSION↗
DOE OSTI2018

Boil-off losses along LH2 pathway

Losses along the LH 2 pathway are intrinsic to the utilization of a cryogenic fluid. They occur when the molecule is transferred between 2 vessels (liquefaction plant to trailer, trailer to station storage, station storage to pump or compressor, then fuel cell electric vehicles …) and when the fluid is warmed up due to heat transfer with the environment. Those losses can be estimated with good accuracy using thermodynamic models based on conservation of mass and energy, providing the thermodynamic states are correctly described. Indeed, the fluid undergoes various changes as it moves along the entire pathway (2 phase transition, super-heated warming, non-uniform temperature distributions across the saturation film) and accurate equations of state and 2 phase behavior implementations are essential. The balances of mass and energy during the various dynamics processes then enable to quantify the boil-off losses. In this work, a MATLAB code previously developed by NASA to simulate rocket loading is used as the basis for the LH 2 transfer model. This code implements complex physical phenomena such as the competition between condensation and evaporation and the convection vs. conduction heat transfer as a function of the relative temperatures on both sides of the saturated film. The original code was modified to consider real gas equations of state, and some semi-empirical relationships, such as between the heat of vaporization and the critical temperature, were also replaced by a REFPROP equivalent expression, assumed to be more accurate. Non-constant liquid temperature equations were added to simulate sub-cooled conditions. It is shown that although trailer depressurization and transfer losses from the receiving vessel during a LH 2 delivery may constitute the largest sources of losses, those can be greatly reduced and even eliminated if CFR/DOT regulations are properly applied and if no-vent fill methods are implemented, particularly for a stationary LH2 storage operating at reasonably low pressure (45 psia or so). As such, it is expected that the only remaining boil-off losses for a refueling station would come from the LH 2 pump (utilization and idling), pump vessel cool down/warm up, and environment heat transfer. Based on experimental data measured at LLNL on the Linde 875 bar LH 2 cryo-pump and results from the model, and extrapolating for refueling stations of various sizes, it can be shown that boil-off losses can vary from 15% of delivered LH 2 for a 100 kg/day, 5% at 400 kg/day, and down to less than 2% for stations above 1,800 kg/day (for a system similar to the one at LLNL). Less boil-off is to be expected for LH 2 pumps dispensing at 350 bar, so that less than 0.7% can be expected above 1,800 kg/day station capacities. At last, boil-off recovery solutions are briefly analyzed, including compressors, cryo-coolers and stationary fuel cell. Their economic value is strongly related to the costs of H2 and of the electricity needed to perform the recovery, on top of the initial capital expenditures. Effective boil-off could be reduced to 0.6-1% for a 2,000 kg/day station if adequate recovery solutions are used.

08 HYDROGEN↗
NASA NTRS1973

Simulation capability for dynamics of rotating counterweight space stations.

An analysis and computer program were prepared to realistically simulate the dynamic behavior of a class of space stations consisting of two end bodies separated by a connecting structure. The shape and mass distribution of the flexible end bodies are arbitrary; the connecting structure is flexible but massless and is capable of deployment and retraction. Fluid flowing in a piping system and rigid moving masses, representing a cargo elevator or crew members, have been modeled. Connecting structure characteristics, control systems, and externally applied loads are modeled in easily replaced subroutines. Subroutines currently available include a telescopic beam-type connecting structure as well as attitude, deployment, spin, and wobble control. In addition, a unique mass balance control system was developed to sense and balance mass shifts due to the motion of a cargo elevator. The mass of the cargo may vary through a large range. Numerical results are discussed for various types of runs.

Austin, F.↗
NASA NTRS1973

Simulation capability for dynamics of two-body flexible satellites

An analysis and computer program were prepared to realistically simulate the dynamic behavior of a class of satellites consisting of two end bodies separated by a connecting structure. The shape and mass distribution of the flexible end bodies are arbitrary; the connecting structure is flexible but massless and is capable of deployment and retraction. Fluid flowing in a piping system and rigid moving masses, representing a cargo elevator or crew members, have been modeled. Connecting structure characteristics, control systems, and externally applied loads are modeled in easily replaced subroutines. Subroutines currently available include a telescopic beam-type connecting structure as well as attitude, deployment, spin and wobble control. In addition, a unique mass balance control system was developed to sense and balance mass shifts due to the motion of a cargo elevator. The mass of the cargo may vary through a large range. Numerical results are discussed for various types of runs.

Austin, F.↗
NASA NTRS1981

An extension of the local momentum theory to a distorted wake model of a hovering rotor

The local momentum theory is based on the instantaneous balance between the fluid momentum and the blade elemental lift at a local station in the rotor rotational plane. Therefore, the theory has the capability of evaluating time wise variations of air loading and induced velocity distributions along a helicopter blade span. Unlike a complex vortex theory, this theory was developed to analyze the instantaneous induced velocity distribution effectively. The boundaries of this theory and a computer program using this theory are discussed. A concept introduced into the theory is the effect of the rotor wake contraction in hovering flight. A comparison of this extended local momentum theory with a prescribed wake vortex theory is also presented. The results indicate that the extended local momentum theory has the capability of achieving a level of accuracy similar to that of the prescribed wake vortex theory over wide range variations of rotor geometrical parameters. It is also shown that the analytical results obtained using either theory are in reasonable agreement with experimental data.

Kawachi, K.↗
DOE OSTI2015

A Serially-Connected Compensator for Eliminating the Unbalanced Three-Phase Voltage Impact on Wind Turbine Generators

Untransposed transmission lines, unbalanced tap changer operations, and unbalanced loading in weak distribution lines can cause unbalanced-voltage conditions. The resulting unbalanced voltage at the point of interconnection affects proper gird integration and reduces the lifetime of wind turbines due to power oscillations, torque pulsations, mechanical stresses, energy losses, and uneven and overheating of the generator stator winding. This work investigates the dynamic impact of unbalanced voltage on the mechanical and electrical components of integrated Fatigue, Aerodynamics, Structures, and Turbulence (FAST) wind turbine generation systems (WTGs) of Type 1 (squirrel-cage induction generator) and Type 3 (doubly-fed induction generator). To alleviate this impact, a serially-connected compensator for a three-phase power line is proposed to balance the wind turbine-side voltage. Dynamic simulation studies are conducted in MATLAB/Simulink to compare the responses of these two types of wind turbine models under normal and unbalanced-voltage operation conditions and demonstrate the effectiveness of the proposed compensator.

17 WIND ENERGY↗
NASA NTRS2012

NASA Tech Briefs, September 2012

Topics covered include: Beat-to-Beat Blood Pressure Monitor; Measurement Techniques for Clock Jitter; Lightweight, Miniature Inertial Measurement System; Optical Density Analysis of X-Rays Utilizing Calibration Tooling to Estimate Thickness of Parts; Fuel Cell/Electrochemical Cell Voltage Monitor; Anomaly Detection Techniques with Real Test Data from a Spinning Turbine Engine-Like Rotor; Measuring Air Leaks into the Vacuum Space of Large Liquid Hydrogen Tanks; Antenna Calibration and Measurement Equipment; Glass Solder Approach for Robust, Low-Loss, Fiber-to-Waveguide Coupling; Lightweight Metal Matrix Composite Segmented for Manufacturing High-Precision Mirrors; Plasma Treatment to Remove Carbon from Indium UV Filters; Telerobotics Workstation (TRWS) for Deep Space Habitats; Single-Pole Double-Throw MMIC Switches for a Microwave Radiometer; On Shaft Data Acquisition System (OSDAS); ASIC Readout Circuit Architecture for Large Geiger Photodiode Arrays; Flexible Architecture for FPGAs in Embedded Systems; Polyurea-Based Aerogel Monoliths and Composites; Resin-Impregnated Carbon Ablator: A New Ablative Material for Hyperbolic Entry Speeds; Self-Cleaning Particulate Prefilter Media; Modular, Rapid Propellant Loading System/Cryogenic Testbed; Compact, Low-Force, Low-Noise Linear Actuator; Loop Heat Pipe with Thermal Control Valve as a Variable Thermal Link; Process for Measuring Over-Center Distances; Hands-Free Transcranial Color Doppler Probe; Improving Balance Function Using Low Levels of Electrical Stimulation of the Balance Organs; Developing Physiologic Models for Emergency Medical Procedures Under Microgravity; PMA-Linked Fluorescence for Rapid Detection of Viable Bacterial Endospores; Portable Intravenous Fluid Production Device for Ground Use; Adaptation of a Filter Assembly to Assess Microbial Bioburden of Pressurant Within a Propulsion System; Multiplexed Force and Deflection Sensing Shell Membranes for Robotic Manipulators; Whispering Gallery Mode Optomechanical Resonator; Vision-Aided Autonomous Landing and Ingress of Micro Aerial Vehicles; Self-Sealing Wet Chemistry Cell for Field Analysis; General MACOS Interface for Modeling and Analysis for Controlled Optical Systems; Mars Technology Rover with Arm-Mounted Percussive Coring Tool, Microimager, and Sample-Handling Encapsulation Containerization Subsystem; Fault-Tolerant, Real-Time, Multi-Core Computer System; Water Detection Based on Object Reflections; SATPLOT for Analysis of SECCHI Heliospheric Imager Data; Plug-in Plan Tool v3.0.3.1; Frequency Correction for MIRO Chirp Transformation Spectroscopy Spectrum; Nonlinear Estimation Approach to Real-Time Georegistration from Aerial Images; Optimal Force Control of Vibro-Impact Systems for Autonomous Drilling Applications; Low-Cost Telemetry System for Small/Micro Satellites; Operator Interface and Control Software for the Reconfigurable Surface System Tri-ATHLETE; and Algorithms for Determining Physical Responses of Structures Under Load.

Source record↗
DOE OSTI2012

Real sample temperature: a critical issue in the experiments of nuclear resonant vibrational spectroscopy on biological samples

There are several practical and intertangled issues which make the experiments of nuclear resonant vibrational spectroscopy (NRVS) on biological samples difficult to perform. The sample temperature is one of the most important issues. In NRVS the real sample temperatures can be very different from the readings on the temperature sensors. In this study the following have been performed: (i) citing and analyzing various existing NRVS data to assess the real sample temperatures during the NRVS measurements and to understand their trends with the samples’ loading conditions; (ii) designing several NRVS measurements with (Et 4 N)[FeCl 4 ] to verify these trends; and (iii) proposing a new sampleloading procedure to achieve significantly lower real sample temperatures and to balance among the intertangled experimental issues in biological NRVS measurements.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗