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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 1,603 records · Page 89
All sourcesNASA NTRSDOE OSTI
NASA NTRS2002

Sulfur Saturation Limits in Silicate Melts and their Implications for Core Formation Scenarios for Terrestrial Planets

This study explores the controls of temperature, pressure, and silicate melt composition on S solubility in silicate liquids. The solubility of S in FeO-containing silicate melts in equilibrium with metal sulfide increases significantly with increasing temperature but decreases with increasing pressure. The silicate melt structure also exercises a control on S solubility. Increasing the degree of polymerization of the silicate melt structure lowers the S solubility in the silicate liquid. The new set of experimental data is used to expand the model of Mavrogenes and O'Neill(1999) for S solubility in silicate liquids by incorporating the influence of the silicate melt structure. The expected S solubility in the ascending magma is calculated using the expanded model. Because the negative pressure dependence of S solubility is more influential than the positive temperature dependence, decompression and adiabatic ascent of a formerly S-saturated silicate magma will lead to S undersaturation. A primitive magma that is S-saturated in its source region will, therefore, become S-undersaturated as it ascends to shallower depth. In order to precipitate magmatic sulfides, the magma must first cool and undergo fractional crystallization to reach S saturation. The S content in a metallic liquid that is in equilibrium with a magma ocean that contains approx. 200 ppm S (i.e., Earth's bulk mantle S content) ranges from 5.5 to 12 wt% S. This range of S values encompasses the amount of S (9 to 12 wt%) that would be present in the outer core if S is the light element. Thus, the Earth's proto-mantle could be in equilibrium (in terms of the preserved S abundance) with a core-forming metallic phase.

Holzheid, Astrid↗
NASA NTRS1982

Use of thermocapillary migration in a controllable heat valve

In accordance with the Marangoni effect, immiscible droplets in a host fluid in which a temperature gradient exists move in the direction of increasing temperature. It is proposed that this thermocapillary migration could be used to construct a 'liquid wick' that would return the condensed vapor at the condenser end of a heat pipe back to the evaporator, thus completing the fluid circuit. The droplets would be formed by capillary pressure forcing the condensate through a perforated diaphragm whose temperature would control the droplet flux, and hence the heat flux between the two ends of the heat pipe, thus making it a controllable heat valve.

Schmid, L. A.↗
NASA NTRS1999

A New Method to Measure Temperature and Burner Pattern Factor Sensing for Active Engine Control

The determination of the temperatures of extended surfaces which exhibit non-uniform temperature variation is very important for a number of applications including the "Burner Pattern Factor" (BPF) of turbine engines. Exploratory work has shown that use of BPF to control engine functions can result in many benefits, among them reduction in engine weight, reduction in operating cost, increase in engine life, while attaining maximum engine efficiency. Advanced engines are expected to operate at very high temperature to achieve high efficiency. Brief exposure of engine components to higher than design temperatures due to non-uniformity in engine burner pattern can reduce engine life. The engine BPF is a measure of engine temperature uniformity. Attainment of maximum temperature uniformity and high temperatures is key to maximum efficiency and long life. A new approach to determine through the measurement of just one radiation spectrum by a multiwavelength pyrometer is possible. This paper discusses a new temperature sensing approach and its application to determine the BPF.

Ng, Daniel↗
DOE OSTI2023

Preliminary Development of Heat Transfer Model-Based Control Algorithms of Liquid Sodium Purification System: Advanced Sensors and Instrumentation Advanced Controls

Monitoring the operation of sodium purification system is essential for efficient operation of sodium fast reactors. In this work, a heat transfer model has been developed for monitoring the plugging meter and cold trap systems at the Mechanisms Engineering Test Loop (METL) liquid sodium facility at Argonne National Laboratory. The model of the purification system was developed by treating the respective aspects of the cold trap purification loop and plugging meter diagnostic loop as two separate control volumes using information from the METL piping and instrumentation diagram (P&ID). A model predictive controller was designed using first order differential equations with the specified boundary conditions. The system behavior was studied with a tuned optimized procedure using the internal cold trap temperature and plugging meter outlet temperature as control variables, and the air blower temperature as an independent variable respectively. Results of computer simulations obtained in this study compared favorably with experimental data showing very good reference tracking response with negligible overshoot as both plugging meter and cold trap physical models approach the setpoint.

22 GENERAL STUDIES OF NUCLEAR REACTORS↗
DOE OSTI2018

A comparative study on the oxidation of two-dimensional Ti 3 C 2 MXene structures in different environments

The oxidation of two-dimensional Ti 3 C 2 MXene structures has been recognized as a promising method for the formation of hybrid structures of carbon supported nanotitania. Here, we studied the oxidation of Ti 3 C 2 MXene structures using reactive force field (ReaxFF) based molecular dynamics simulations. To investigate the effect of oxidizing agent, we used three different environments including dry air (oxygen molecules), wet air (oxygen and water molecules) and hydrogen peroxide (H 2 O 2 molecules). Oxidation simulations were performed at different temperatures of 1000, 1500, 2000, 2500 and 3000 K. We found that by controlling the temperature, carbon supported titania can be formed by diffusion of Ti atoms to the surface of MXene structures during the oxidation. These results were confirmed by the increase in the average bond orders of C–C and Ti–O and decrease in the average bond orders of Ti–C. Moreover, it was revealed that by increasing the temperature, the oxidation rate increases, and the rate depends on the oxidant according to the following order: H 2 O 2 > wet air > dry air. This was validated by heating the MXene in wet air and dry air followed by examining the products using X-ray diffraction and Raman spectroscopy. To investigate the effect of the presence of the oxidant, the MXene structure was also heated under vacuum, and it was found that in this case the MXene structure was converted to cubic TiC. Furthermore, it was indicated that during the heating process of the MXene structure in a vacuum, the average bond orders for C–C, Ti–C and Ti–O do not change significantly due to the lack of oxidants in the environment, leaving room for only topotactic transformation of atoms during the heating. In conclusion, the formation of the TiC structure by heating the MXene in an inert environment was confirmed experimentally as well.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2024

Controlling optical-cavity locking using reinforcement learning

Abstract This study applies an effective methodology based on Reinforcement Learning to a control system. Using the Pound–Drever–Hall locking scheme, we match the wavelength of a controlled laser to the length of a Fabry-Pérot cavity such that the cavity length is an exact integer multiple of the laser wavelength. Typically, long-term drift of the cavity length and laser wavelength exceeds the dynamic range of this control if only the laser’s piezoelectric transducer is actuated, so the same error signal also controls the temperature of the laser crystal. In this work, we instead implement this feedback control grounded on Q-Learning. Our system learns in real-time, eschewing reliance on historical data, and exhibits adaptability to system variations post-training. This adaptive quality ensures continuous updates to the learning agent. This innovative approach maintains lock for eight days on average.

47 OTHER INSTRUMENTATION↗
NASA NTRS1992

Cryogenic leak testing of tube fittings/valves

A high pressure and variable temperature cryogenic leak testing system was conceived and designed in order to conduct leakage testing of pipe fittings/valves in liquid hydrogen supply lines of the Space Shuttle. The system can create a continuous testing environment of variable temperature, 5.5 to about 300 K, and variable pressure, 0.01 to about 70 x 10 exp 5 Pa, with a large sample space, 90 mm diameter x 228 mm length, and at low operating cost. In terms of cryogenic leak testing the system has a special capability for extensive applications. The system comprised a variable temperature cryostat, a high pressure sample chamber, a vacuum pumping station, gas flow control system, pressure and temperature control systems, and leak detecting and measuring systems. A general discussion of cryogenic leak testing methods is also presented.

Jia, L. X.↗
NASA NTRS1996

Development of the Plant Growth Facility for Use in the Shuttle Middeck and Test Units for Ground-Based Experiments

The plant growth facility (PGF), currently under development as a Space Shuttle middeck facility for the support of research on higher plants in microgravity, is presented. The PGF provides controlled fluorescent lighting and the active control of temperature, relative humidity and CO2 concentration. These parameters are designed to be centrally controlled by a dedicated microprocessor. The status of the experiment can be displayed for onboard analysis, and will be automatically archived for post-flight analysis. The facility is designed to operate for 15 days and will provide air filtration to remove ethylene and trace organics with replaceable potassium permanganate filters. Similar ground units will be available for pre-flight experimentation.

Chapman, David K.↗
NASA NTRS1976

Behavioral fever in newborn rabbits

New Zealand white rabbit pups aged 12 to 72 hr were divided into three groups and given an intraperitoneal injection of Pseudomonas polysaccharide, a saline vehicle alone, and no treatment, respectively. The animals injected with pyrogen and maintained at an ambient temperature of 32 C for 2 hr did not develop fever. When placed in a thermally graded alleyway, the animals injected with pyrogen selected gradient positions that represented significantly higher temperatures than controls injected with saline. Further stay at selected positions for 5 min caused a considerable increase in the rectal temperature of the pyrogen-injected pups but not that of controls. The results support the hypothesis that newborn rabbits will develop a fever by behavioral means after a single injection of an exogenous pyrogen if the opportunity for thermoregulatory behavior is present. No fever develops if the pups must rely solely on internal thermoregulatory mechanisms. The behavioral system for producing a fever is mature at birth, but an adequate system of internal reflexes does not appear to develop for some days.

Satinoff, E.↗
DOE OSTI2020

Signal Temporal Logic Control for Residential HVAC Systems to Accommodate High Solar PV Penetration

This paper proposes a new signal temporal logic (STL) control for ON/OFF residential buildings' Heating Ventilation and Air Conditioning (HVAC) systems. STL is used to control indoor temperatures while consuming most of the generated solar photovoltaic (PV) power locally to minimize its impact on the grid and reduce the need for large energy storage devices. In contrast to most, if not all, control mechanisms such as the traditional model predictive control (MPC), STL control allows for including temporal constraints in the control formulation to further relax indoor temperatures' constraints and allow them to exceed the comfort band limits for a prespecified (short) period of time. This relaxation allows to consume an additional PV power by the HVAC systems, which prevents such an unwanted intermittent power from affecting the grid. We formulate the MPC-based STL control mechanism to implement the objective. Simulation results show that the PV tracking performance has been improved while employing the proposed STL controller.

Wu, Tumin↗
DOE OSTI2017

Field test and simulation evaluation of variable refrigerant flow systems performance

Our study aims to compare the performance of a Variable Refrigerant Flow (VRF) system with a Roof Top Unit, (RTU) and a variable-air-volume (VAV) system through field tests and energy simulations. The field test was conducted in as similar conditions as possible between the two systems, such as the installation and operating environments of heating, the ventilation and air conditioning (HVAC) system, including internal heat gain and outdoor conditions, including buildings to compare the performance of the two systems accurately. A VRF system and RTU were installed at the test building located in Oak Ridge, Tennessee, in the USA. The same internal heat gain was generated at the same operating time of the two systems using lighting, electric heaters, and humidifiers inside the building. The HVAC system was alternately operated between cooling and heating operations to acquire energy performance data and to compare energy usage. Furthermore, an hourly building energy simulation model was developed with regard to the VRF system and RTU, and then the model was calibrated using actual measured data. Then, annual energy consumption of the two systems were compared and analyzed using the calibrated model. Moreover, additional analysis was conducted when the controlled discharge air temperature in the RTU was changed. The field test result showed that when energy consumptions of two systems were compared at the same outdoor conditions, using the weather-normalized model, the VRF system exhibited an energy reduction of approximately 17% during cooling operation and of approximately 74% during heating operations. A comparison on the annual energy consumption using simulations showed that the VRF system reduced energy consumption more than that of the RTU by 60%. Furthermore, when the discharge air temperature in the RTU was controlled according to the outdoor air temperature, energy consumption of the RTU was reduced by 6% in cooling operations and by 18% in heating operation. As a result, energy consumption of the VRF system was reduced by more than that of the RTU by 55% approximately.

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗
DOE OSTI2016

Systems and methods for energy cost optimization in a building system

Methods and systems to minimize energy cost in response to time-varying energy prices are presented for a variety of different pricing scenarios. A cascaded model predictive control system is disclosed comprising an inner controller and an outer controller. The inner controller controls power use using a derivative of a temperature setpoint and the outer controller controls temperature via a power setpoint or power deferral. An optimization procedure is used to minimize a cost function within a time horizon subject to temperature constraints, equality constraints, and demand charge constraints. Equality constraints are formulated using system model information and system state information whereas demand charge constraints are formulated using system state information and pricing information. A masking procedure is used to invalidate demand charge constraints for inactive pricing periods including peak, partial-peak, off-peak, critical-peak, and real-time.

29 ENERGY PLANNING, POLICY, AND ECONOMY↗
DOE OSTI2021

Tuning 2D magnetism in Fe 3+X GeTe 2 films by element doping

Two-dimensional (2D) ferromagnetic materials have been discovered with tunable magnetism and orbital-driven nodal-line features. Controlling the 2D magnetism in exfoliated nanoflakes via electric/magnetic fields enables a boosted Curie temperature (T C ) or phase transitions. One of the challenges, however, is the realization of high T C 2D magnets that are tunable, robust and suitable for large scale fabrication. Here, we report molecular-beam epitaxy growth of wafer-scale Fe 3+X GeTe 2 films with T C above room temperature. By controlling the Fe composition in Fe 3+X GeTe 2 , a continuously modulated T C in a broad range of 185–320 K has been achieved. This widely tunable T C is attributed to the doped interlayer Fe that provides a 40% enhancement around the optimal composition X = 2. We further fabricated magnetic tunneling junction device arrays that exhibit clear tunneling signals. Our results show an effective and reliable approach, i.e. element doping, to producing robust and tunable ferromagnetism beyond room temperature in a large-scale 2D Fe 3+X GeTe 2 fashion.

2D ferromagnetic material↗
NASA NTRS1993

Temperature dependence of protein solubility-determination, application to crystallization, and growth kinetics studies

A scintillation method was developed for determinations of the temperature dependence of the solubility, and of nucleation induction times of proteins, in 50-100 mu(l) volumes of solution. Solubility data for lysozyme and horse serum albumin were obtained for various combinations of pH and precipitant concentrations. These data and the nucleation induction information were used for dynamic crystallization control, that is, for the controlled separation of nucleation and growth stages. Individual lysozyme and horse serum albumin crystals were grown in 15-20 mu(l) solution volumes contained in x-ray capillaries. The morphology and kinetics of the growth and dissolution of lysozyme in aqueous solutions with 2.5 percent NaCl and at pH = 4.5 was studied in situ with a depth resolution of 300 A (4 unit cells) by high resolution optical microscopy and digital image processing. The bulk super- or under saturation, sigma, of the solution inside a closed growth cell was controlled by temperature. The growth habit was bound by (110) and (101) faces that grew through layer spreading, although with different growth rate dependencies on supersaturation/temperature. At sigma less than 10 (obtained at higher temperatures) growth was purely kinetic ally controlled, with impurity effects (macrostep formation and kinetic hindrance) becoming significant for sigma less than 2. At sigma greater than 10 (lower temperatures), anisotropies in the interfacial kinetics were more pronounced, with interfacial kinetics and bulk transport becoming equally important to the growth morphology. Growth rates were growth history dependent. The formation of striations (layers of irregularly incorporated solution) was unambiguously correlated with growth temperature variations. Etching exposed dislocations and various high-index faces whose growth morphologies were studied during return to the steady state growth form. Growth steps were observed to originate from two-dimensional nuclei or from outcrops of growth striations, and from dislocations that preferentially formed in growth sector boundaries.

Rosenberger, Franz↗
NASA NTRS1983

High-temperature optically activated GaAs power switching for aircraft digital electronic control

Gallium arsenide high-temperature devices were fabricated and assembled into an optically activated pulse-width-modulated power control for a torque motor typical of the kinds used in jet engine actuators. A bipolar heterojunction phototransistor with gallium aluminum arsenide emitter/window, a gallium arsenide junction field-effect power transistor and a gallium arsenide transient protection diode were designed and fabricated. A high-temperature fiber optic/phototransistor coupling scheme was implemented. The devices assembled into the demonstrator were successfully tested at 250 C, proving the feasibility of actuator-located switching of control power using optical signals transmitted by fibers. Assessments of the efficiency and technical merits were made for extension of this high-temperature technology to local conversion of optical power to electrical power and its control at levels useful for driving actuators. Optical power sources included in the comparisons were an infrared light-emitting diode, an injection laser diode, tungsten-halogen lamps and arc lamps. Optical-to-electrical power conversion was limited to photovoltaics located at the actuator. Impedance matching of the photovoltaic array to the load was considered over the full temperature range, -55 C to 260 C. Loss of photovoltaic efficiency at higher temperatures was taken into account. Serious losses in efficiency are: (1) in the optical source and the cooling which they may require in the assumed 125 C ambient, (2) in the decreased conversion efficiency of the gallium arsenide photovoltaic at 260 C, and (3) in impedance matching. Practical systems require improvements in these areas.

Berak, J. M.↗
DOE OSTI2025

Controllable oxygen vacancy defect engineering of BiVO 4 porous structures for room temperature NH 3 detection

Controlling structural features of sensing material while judiciously introducing vacancy defect states for revamping the electronic properties of the sample to obtain its superior gas sensing performance, is quite rare. Herein, we report for the first time, the room temperature (RT) ammonia (NH 3 ) detection of peanut-like porous bismuth vanadate (BiVO 4 ) with a stable monoclinic phase. The developed BiVO 4 possess abundant oxygen vacancies and porosity by virtue of calcinations (400–800 ℃). BiVO 4 calcined at 400 ℃ exhibits high selectivity towards NH 3 with a maximum response of 1421 @ 270 ppm at RT, which is 2.5 fold enhanced compared to without calcined BiVO 4 (response of 547 @ 270 ppm NH 3 ). The oxygen defective BiVO 4 appeared highly durable and stable even under high humid conditions (∼60 %). Besides, the porosity of BiVO 4 not only enhances the specific surface area (19.8 m 2 /g) but also results in fast diffusion of NH 3 molecules, leading to a reduction in the decay time (34 s for 90 ppm NH 3 ). The density functional theory (DFT) uncovers that the oxygen vacancy formation in BiVO 4 augments the NH 3 sensing capabilities by enhancing the adsorption energy of NH 3 . This work provides insight into the sensing mechanism of increased response caused by defect engineering and porosity, which will be favourable for fabricating high-performance NH 3 sensors at RT.

DFT analysis↗
DOE OSTI2018

Use of Confocal Microscope for Environmental Tensile Mechanical Testing

Mechanical testing in environmental chambers is typically limited to 450°C. Some specialty chambers have been designed but at a high cost. Furthermore, accurate extensometers in environmental chambers are rare and expensive to operate. A unique solution investigated in this manuscript is the mating of a confocal laser scanning microscope with a sealed environmental chamber fitted with loading clevises for mechanical testing. Such a setup allows the researcher to measure strain data at elevated temperatures in controlled environments. Utilizing a laser light source avoids problems with blackbody radiation at elevated temperatures. Setup and accuracy of the microscope are discussed concerning tensile loading. P91 boiler steel was selected for this work because of the long history of the alloy in the fossil energy industry. Optical strain uncertainty was measured between 1.6% and 3.5%. Here, other tensile parameters were satisfactorily measured within the experimental error of larger standard specimens.

36 MATERIALS SCIENCE↗