Search NASA⌕ Search

SEARCH · Search NASA

Results for “Bulk density”

Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

Quote a phrase for an exact phrase match. Source license links do not imply unrestricted reuse.

At least 163 records · Page 9

Compositing and Characterization of SE Quadrant Waste Exemplars

This report outlines the experimental investigation and characterization of transport properties in Hanford SE quadrant High-Level Waste (HLW). The goal of the study was to establish baseline behaviors of bulk composite rheology and settling characteristics to facilitate waste treatment process design for the Waste Treatment and Immobilization Plant (WTP) and avoid waste conditions and properties favorable to bubble cascade gas release events. The study focused on two major objectives: 1) identifying, obtaining, and preparing relevant Hanford tank waste samples for evaluation and 2) quantifying the “as-received” rheology and transport properties of the samples. Twenty-three centrifuged core segments originating from tanks AN-101, AN-106, and AW-105 were selected based on compositional relevance to SE quadrant PUREX cladding waste. These materials were composited into five waste composites enriched with target analytes: aluminum (Al), iron (Fe), phosphate (PO 4 ), uranium (U), and zirconium (Zr). Physical property and transport testing examined particle size distributions, bulk densities, settling behaviors, rheological properties, shear strengths, and just-suspended mixing speeds (NJS). Testing revealed two distinct composite classifications based on rheological characteristics: non-Newtonian composites (Fe and PO 4 ) and Newtonian composites (Al, U, and Zr). The Fe and PO 4 composites exhibited slow settling rates and reduced mobilization proclivity, attributable to strong particle-particle interactions and the formation of yield structures within non-Newtonian slurries. In contrast, the Al, U, and Zr composites displayed rapid settling and dense compaction behaviors, indicative of minimal structuring and interactions. Shear strengths for all composites were generally low relative to prior studies of SE quadrant waste, with only the U composite showing elevated strength approaching values reported in previous literature. Repeat shear strength measurements revealed contributions from dense granular material in the U composite and stronger cohesive properties in the Al composite. Settling data highlighted hindered settling behavior, with rates falling more than one order of magnitude below estimates based on Stokes’ law and rate decreasing as composite UDS content increased. NJS testing demonstrated different mobilization behaviors between cohesive and granular composites. The Fe composite required the highest mixing rate for resuspension, while the Al composite was the easiest to resuspend. Comparison of measured NJS against predictions made using the Zwietering correlation suggests non-Newtonian behavior alters resuspension mechanics, rendering non-Newtonian systems more stable against resuspension lift forces relative to their granular counterparts.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Pressureless Sintering of Pre-Alloyed Nanostructured Bainitic Steel Powders

A recent study shows that powder metallurgy and pressureless sintering are a viable pathway to realize full-density bulk components of nanostructure bainitic steels. A scalable, pressureless supersolidus liquid phase sintering (SLPS) approach to process nanostructured bainitic steel is evaluated. Furthermore, to address the oxidation issues associated with the mechanical alloying of elemental powders, powder atomization is used to produce pre-alloyed nanostructured bainitic steel powders.

mechanical alloying↗

Fabrication and Evaluation of Large Alumina Crucibles by Vat Photopolymerization Additive Manufacturing for High-Temperature Actinide Chemistry

Additive manufacturing (AM) offers opportunities to advance the design and function of ceramic tooling in high temperature actinide pyrochemistry. In technical ceramics such as alumina, conventional forming techniques often restrict design flexibility and can limit experimental progress. In this study, we investigate the use of vat photopolymerization (VP) with commercial resins to fabricate large-scale alumina crucibles, reaching dimensions up to 125 mm, which is significantly larger than typically reported for dense VP ceramics. Notably, these additively manufactured components are produced using consumer-grade hardware, which limits process control, but offers significant upside in scalability and accessibility. Using microscopy and X-ray computed tomography, the VP alumina parts have high bulk densities above 95%, but also the prevalence of AM-induced artifacts and surface defects. Mechanical testing showed these defects to significantly reduce flexural strength and compromise part reliability. Electrorefining trials under sustained exposure to molten salts and metals reveal mixed results, with the AM material exhibiting high chemical compatibility, but mechanical failures due to the reduced strength were prevalent. Our findings illustrate both the promise and current limitations of AM ceramics for actinide chemistry, and point toward future improvements in process optimization, design strategies, and part screening to enhance performance and reliability.

Materials science↗

Structural and High-Temperature Tensile Properties of Special Pitch-Coke Graphites

The room-temperature structural properties and the tensile properties up to 5000 F (275O C) were determined for ten grades of specially prepared petroleum-coke coal-tar-pitch graphites which were graphitized at 5430 F (3000 C). One impregnation with coal-tar pitch increased the bulk density from 1.41 to 1.57 g/cm3 and the maximum strength at 4500 F (2500 C) from 4000 to 5700 psi. None of the processing parameters studied had a marked effect on the closed porosity or the X-ray structure or the per cent graphitization. The coarse-particle filler resulted in the lowest coefficient of thermal expansion and the fine-particle filler in the highest coefficient. A marked improvement in uniformity of tensile strength was observed. A standard-deviation analysis gave a one-sigma value of approximately 150 psi for one of these special grades and values of 340-420 psi for three commercial grades.

GRAPHITE↗

Packing properties of fine powders and the depth of the lunar dust layer

Previous experimental and theoretical studies by Hapke and Van Horn [1963] and Hapke [1963] of surfaces which reflect light like the moon support the hypothesis that the lunar surface is covered with a layer of fine rock dust. The material in this layer appears to be in an extremely unconsolidated state, having a bulk density of the order of one-eighth that of solid rock. Such photometric studies can give information concerning only the upper few millimeters of the lunar soil. However, analyses of radiofrequency observations indicate that extensive areas of the moon may be covered to depths of the order of a meter or greater by a substance which is also much less dense than solid rock. From the radar reflectivity of the lunar surface at meter wavelengths Evans [1962] infers a dielectric constant of K = 2.7; Troitsky [1962] estimates K = 1.6 on the basis of radio-thermal observations at centimeter wavelengths. Since the RF dielectric constants of stony meteorites and of terrestrial rocks range from about 4 to 45 [Fensler et al., 1962] it is clear that the density of the lunar soil is unusually low at least to depths to which RF radiation can penetrate; Troitsky estimates this depth to be of the order of 20 wavelengths or greater in the 3-cm-wavelength range.

Powder↗

Lunar soil coefficient of friction determined from Surveyor data and laboratory tests

A series of laboratory tests on simulated soils was conducted to evaluate some of these physical properties. Using soils similar to lunar soil composition, particle size distribution, and cohesion as determined from the Surveyor mission, the coefficient of friction and bulk density were evaluated by reproducing soils with the same force vs penetration characteristics as demonstrated at the Surveyor landing sites. The determination of soil coefficient of friction is presented in this paper; the soil density is treated separately in the previous paper’ of this report.

Choate, R.↗

Soil mechanics results of Luna 16 and Lunokhod 1: A preliminary report

The physical and mechanical properties of the lunar soil, as determined by Luna 16 and Lunokhod 1 experiments, are discussed. Data are included for interactions between vehicle wheels and the lunar soil, compressibility, resistance to penetration, and friction characteristics of the soil. The shear strength of the returned lunar soil for various bulk densities is also examined. Several potential spacecraft materials were tested in contact with lunar soil to determine their friction and wear characteristics.

Johnson, S. W.↗

Cracking of the lunar soil

Rather than a pattern of cracks in an apparently flat surface, the Apollo 12 photographs suggest an irregular surface that consists of clods or fragments. The impression of flat tiles and crusting, obtained by monoscopic viewing, is an illusion. Instead, the lunar soil deforms and cracks in the same manner as homogeneous isotropic terrestrial soils of moderate bulk density, having a small amount of cohesion.

Jaffe, L. D.↗

Cracking of lunar mare soil.

Demonstration that lunar soil deforms and cracks in the same manner as homogeneous isotropic terrestrial soil s of moderate bulk density with a small amount of cohesion. This conclusion is made from an analysis of Surveyor 3 TV pictures and of Apollo 11 closeup picture of lunar surface disturbances by bearing tests and instrument pressure.

Jaffe, L. D.↗

Apollo 12 thermal radiation properties.

The spectral and total thermal radiation properties are presented as a function of bulk density for lunar fines from the Apollo 12 mission collected on the Ocean of Storms. The total emittance is presented as a function of temperature from 90 to 400 K and the solar reflectance (albedo) for near normal incidence.

Birkebak, R. C.↗

Spectral reflectance and emittance of Apollo 11 and 12 lunar material.

The thermal radiation properties of Apollo 11 and 12 fines (soils) are reviewed and presented as a function of wavelength, angle of illumination, and bulk density. The spectral directional reflectance is presented for wavelengths from 0.6 to 2 microns and for angles of illumination of 10, 20, 30, 45, and 60 deg. The normal emittance is presented for wavelengths from 2.5 to 14.5 microns. The solar albedo and total normal emittance as a function of temperature were calculated from the spectral values. The solar albedo for Apollo 11 fines is 0.099 whereas for Apollo 12 fines is approximately 0.119 for angles of illumination of 10 deg and a density of 1600 kg cu m.

Birkebak, R. C.↗

Reflectance measurements for the detection and mapping of soil limitations

During 1971 and 1972 research was conducted on two fallow fields in the proposed Oahe Irrigation Project to investigate the relationship between the tonal variations observed on aerial photographs and the principal soil limitations of the area. A grid sampling procedure was used to collected detailed field data during the 1972 growing season. The field data was compared to imagery collected on May 14, 1971 at 3050 meters altitude. The imagery and field data were initially evaluated by a visual analysis. Correlation and regression analysis revealed a highly significant correlation and regression analysis revealed a highly significant correlation between the digitized color infrared film data and soil properties such as organic matter content, color, depth to carbonates, bulk density and reflectivity. Computer classification of the multiemulsion film data resulted in maps delineating the areas containing claypan and erosion limitations. Reflectance data from the red spectral band provided the best results.

Benson, L. A.↗

Pore Structure Analysis of RSI Tile

Mercury porosimetry gives a means of characterizing RSI tile pore structure in terms of porosity, pore size distribution, bulk density, specific surface area, mean pore diameter, and mean fiber diameter. It also allows the determination of the effects of heat treatment on these parameters. It is limited in application to open-pored structures, however, since any closed pore volume is ignored.

Whittemore, O. J., Jr.↗

Strength and compressibility of returned lunar soil.

Two oedometer and three direct shear tests have been performed in vacuum on a 200 g sample of lunar soil from Apollo 12 (12001, 119). The compressibility data have been used to calculate bulk density and shear wave velocity versus depth on the lunar surface. The shear wave velocity was found to increase approximately with the one-fourth power of the depth, and the results suggest that the Apollo 14 Active Seismic Experiment may not have detected the Fra Mauro formation at a depth of 8.5 m, but only naturally consolidated lunar soil. The shear data indicate that the strength of the lunar soil sample is about 65% that of a ground basalt simulant at the same void ratio.

Carrier, W. D., III↗