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At least 163 records · Page 9

The MECA Payload as a Dust Analysis Laboratory on the MSP 2001 Lander

In a companion abstract, the "Mars Environmental Compatibility Assessment" (MECA) payload for Mars Surveyor Program 2001 (MSP 2001) is described in terms of its capabilities for addressing exobiology on Mars. Here we describe how the same payload elements perform in terms of gathering data about surface dust on the planet. An understanding of the origin and properties of dust is important to both human exploration and planetary geology. The MECA instrument is specifically designed for soil/dust investigations: it is a multifunctional laboratory equipped to assess particulate properties with wet chemistry, camera imagery, optical microscopy (potentially with LTV fluorescence capability), atomic force microscopy (AFM; potentially with mineral-discrimination capabilities), electrometry, active & passive external materials-test panels, mineral hardness testing, and electrostatic & magnetic materials testing. Additionally, evaluation of soil chemical and physical properties as a function of depth down to about 50 cm will be facilitated by the Lander/MECA robot arm on which the camera (RAC) and electrometer are mounted. Types of data being sought for the dust include: (1) general textural and grain-size characterization of the soil as a whole --for example, is the soil essentially dust with other components or is it a clast-supported material in which dust resides only in the clast interstices, (2) size frequency distribution for dust particles in the range 0.01 to 10.00 microns, (3) particle-shape distribution of the soil components and of the fine dust fraction in particular, (4) soil fabric such as grain clustering into clods, aggregates, and cemented/indurated grain amalgamations, as well as related porosity, cohesiveness, and other mechanical soil properties, (5) cohesive relationship that dust has to certain types of rocks and minerals as a clue to which soil materials may be prime hosts for dust "piggybacking", (6) particle, aggregate, and bulk soil electrostatic properties, (7) particle hardness, (8) particle magnetic properties, (9) bulk dust geochemistry (solubility, reactivity, ionic and mineral species). All of these quantities are needed in order for the human exploration program to make assessments of hazards on Mars, and to better enable the production on earth, of soil/dust simulants that can act as realistic test materials in terms of those properties that render dust a contaminant.Such properties include the small grain size that enables penetration of space-suit joints, mechanical interfaces and bearings, seals, etc., and presents difficulty for filtration systems. Size also plays a critical role in the potential for lung disease in long-term habitats. The properties of grain shape and hardness are important parameters in determining the abrasiveness of dust as it enters mechanical systems, or bombards helmet visors and habitat windows in dust-laden winds. Adhesive electrostatic and magnetic properties of dust will be prime causes of contamination of space suits and equipment. Contamination causes mechanical malfunction, tracking of dirt into habitats, "piggybacking" of toxins on dust into habitats, changes in albedo and efficiency of solar arrays and heat exchangers, and changes in electrical conductivity of suit surfaces and other materials that may have specific safety requirements regarding electrical conductivity. Other potentially hazardous properties of dust include the possibility of high solubility of some component grains (rendering them reactive), and toxicity of some materials --grains of superoxidants and heavy metals (there is always the slim, but not inconceivable possibility of biogenic components such as spores). Because Mars has no active surface aqueous regime, volcanic emissions, meteoritic debris, weathering products, and photochemical products of Mars have nowhere to go except reside in the surface; there are few mechanical or chemical (buffering) processes to remove the accumulation of eons. From a planetology perspective, there are many enigmatic issues relating to dust and the aeolian regime in general. MECA will be able to address many questions in this area. For example, if MECA determines a particular particle size distribution (size and sorting values), it will be possible to make inferences about the origin of the dust - - is it all aeolian, or a more primitive residue of weathering, volcanic emissions, and meteoritic gardening? Trenching with the Lander/MECA robot arm will enable local stratigraphy to be determined in terms of depositional rates, amounts and cyclicity in dust storms and/or local aeolian transport. Grain shape will betray the origin of the dust fragments as being the product of recent or ancient weathering, or the comminution products of aeolian transport --the dust-silt ratio might be a measure of aeolian comminution energy. Additional information is contained in the original.

Marshall, J.↗

The MECA Payload as an Exobiology Laboratory on the MSP 2001 Lander

The "Mars Environmental Compatibility Assessment" (MECA) payload for Mars Surveyor Project 2001 (MSP 2001) is comprised of a multifunctional laboratory equipped to assess martian soil properties with wet chemistry, camera imagery, optical microscopy (potentially with UV fluorescence capability), atomic force microscopy (AFM; potentially with mineral-discrimination capabilities), electrometry, active & passive external materials-test panels, mineral hardness testing, and electrostatic and magnetic materials testing. Additionally, evaluation of soil chemical and physical properties as a function of depth down to -50 cm will be facilitated by the Lander/MECA robot arm on which the camera (RAC) and electrometer are mounted. MECA was designed as a NASA Human Exploration and Development of Space (HEDS) payload for determining the properties of martian soil that may be detrimental to human exploration. It is, however, well equipped to address exobiology questions in the following areas: (1)Geochemical clues to Aqueous Mineralogy and Oxidant formation; (2) Soil structures and microfabrics as indicators of water-volatiles migration; (3) Minerals and rocks as clues to ancient hydrology; (4) Grain textures as indicators of aqueous activity and weathering. Additional information is contained in the original.

Marshall, J.↗

Materials Compatibility Testing in Concentrated Hydrogen Peroxide

Materials test methods from the 1960's have been used as a starting point in evaluating materials for today's space launch vehicles. These established test methods have been modified to incorporate today's analytical laboratory equipment. The Orbital test objective was to test a wide range of materials to incorporate the revolution in polymer and composite materials that has occurred since the 1960's. Testing is accomplished in 3 stages from rough screening to detailed analytical tests. Several interesting test observations have been made during this testing and are included in the paper. A summary of the set-up, test and evaluation of long-term storage sub-scale tanks is also included. This sub-scale tank test lasted for a 7-month duration prior to being stopped due to a polar boss material breakdown. Chemical evaluations of the hydrogen peroxide and residue left on the polar boss surface identify the material breakdown quite clearly. The paper concludes with recommendations for future testing and a specific effort underway within the industry to standardize the test methods used in evaluating materials.

Boxwell, R.↗

Low Cost Coherent Doppler Lidar Data Acquisition and Processing

The work described in this paper details the development of a low-cost, short-development time data acquisition and processing system for a coherent Doppler lidar. This was done using common laboratory equipment and a small software investment. This system provides near real-time wind profile measurements. Coding flexibility created a very useful test bed for new techniques.

Barnes, Bruce W.↗

Characteristics of a 60-Inch Arc-Image Furnace and Application to the Study of Materials

An arc-image furnace consisting of two paraboloidal searchlight mirrors 60 inches (152 centimeters) in diameter and a modified electrode mechanism has been developed and has been used as an operational piece of laboratory equipment for the study of the elevated-temperature behavior of engineering materials. Using two types of 16-millimeter high-current anodes and operating in the atmosphere at current levels of 80 to 550 amperes, the arc-image furnace provides a heating-rate range from 100 to 1,000 Btu per square foot-sec (27 to 270 cal per centimeters squared-sec) with good reliability and reproducibility. Running times vary from 60 seconds at 550 amperes to 10 minute or longer at the lower current levels.

Peters, Roger W.↗

Category V Compliant Container for Mars Sample Return Missions

A novel containerization technique that satisfies Planetary Protection (PP) Category V requirements has been developed and demonstrated on the mock-up of the Mars Sample Return Container. The proposed approach uses explosive welding with a sacrificial layer and cut-through-the-seam techniques. The technology produces a container that is free from Martian contaminants on an atomic level. The containerization technique can be used on any celestial body that may support life. A major advantage of the proposed technology is the possibility of very fast (less than an hour) verification of both containment and cleanliness with typical metallurgical laboratory equipment. No separate biological verification is required. In addition to Category V requirements, the proposed container presents a surface that is clean from any, even nonviable organisms, and any molecular fragments of biological origin that are unique to Mars or any other celestial body other than Earth.

Containers↗

Momentum Flux Measurements Using an Impact Thrust Stand

A device has been developed to measure the force caused by a beam of charged and neutral particles impacting a target plate. This device, an impact thrust stand, was developed to allow thrusters, during early stages of development, to be quickly and easily exhausted and compared to other thrusters. Since some thruster concepts are tested using laboratory equipment that is heavy and cumbersome, measuring the momentum flux of the particles in the plume can be much simpler than placing the entire thruster on a thrust stand. Conservation of momentum requires the momentum flux measured in the plume to be related to the thrust produced by the thruster. The impact thrust stand was designed to be placed in the plume of an electric thruster and has been tested and compared to the thrust measured from a Hall thruster placed on a pendulum thrust stand. Force measurements taken at several axial locations in the magnetic nozzle region of the Variable Specific Impulse Magnetoplasma Rocket will be presented.

Chavers, Greg↗

Combined Silicon and Gallium Arsenide Solar Cell UV Testing

The near and long-term effect of UV on silicon solar cells is relatively understood. In an effort to learn more about the effects of UV radiation on the performance of GaAs/Ge solar cells, silicon and gallium arsenide on germanium (GaAs/Ge) solar cells were placed in a vacuum chamber and irradiated with ultraviolet light by a Spectrolab XT 10 solar simulator. Seventeen GaAs/Ge and 8 silicon solar cells were mounted on an 8 inch copper block. By having all the cells on the same test plate we were able to do direct comparison of silicon and GaAs/Ge solar cell degradation. The test article was attached to a cold plate in the vacuum chamber to maintain the cells at 25 degrees Celsius. A silicon solar cell standard was used to measure beam uniformity and any degradation of the ST-10 beam. The solar cell coverings tested included cells with AR-0213 coverglass, fused silica coverglass, BRR-0213 coverglass and cells without coverglass. Of interest in the test is the BRR-0213 coverglass material manufactured by OCLI. It has an added Infrared rejection coating to help reduce the solar cell operating temperature. This coverglass is relatively new and of interest to several current and future programs at Marshall. Due to moves of the laboratory equipment and location only 350 hours of UV degradation have been completed. During this testing a significant leveling off in the rate of degradation was reached. Data from the test and comparisons of the UV effect of the bare cells and cells with coverglass material will be presented.

Willowby, Douglas↗

International Space Station: National Laboratory Education Concept Development Report

The International Space Station (ISS) program has brought together 16 spacefaring nations in an effort to build a permanent base for human explorers in low-Earth orbit, the first stop past Earth in humanity's path into space. The ISS is a remarkably capable spacecraft, by significant margins the largest and most complex space vehicle ever built. Planned for completion in 2010, the ISS will provide a home for laboratories equipped with a wide array of resources to develop and test the technologies needed for future generations of space exploration. The resources of the only permanent base in space clearly have the potential to find application in areas beyond the research required to enable future exploration missions. In response to Congressional direction in the 2005 National Aeronautics and Space Administration (NASA) Authorization Act, NASA has begun to examine the value of these unique capabilities to other national priorities, particularly education. In early 2006, NASA invited education experts from other Federal agencies to participate in a Task Force charged with developing concepts for using the ISS for educational purposes. Senior representatives from the education offices of the Department of Defense, Department of Education, Department of Energy, National Institutes of Health, and National Science Foundation agreed to take part in the Task Force and have graciously contributed their time and energy to produce a plan that lays out a conceptual framework for potential utilization of the ISS for educational activities sponsored by Federal agencies as well as other future users.

Education↗

Automation of Vapor-Diffusion Growth of Protein Crystals

Some improvements have been made in a system of laboratory equipment developed previously for studying the crystallization of proteins from solution by use of dynamically controlled flows of dry gas. The improvements involve mainly (1) automation of dispensing of liquids for starting experiments, (2) automatic control of drying of protein solutions during the experiments, and (3) provision for automated acquisition of video images for monitoring experiments in progress and for post-experiment analysis. The automation of dispensing of liquids was effected by adding an automated liquid-handling robot that can aspirate source solutions and dispense them in either a hanging-drop or a sitting-drop configuration, whichever is specified, in each of 48 experiment chambers. A video camera of approximately the size and shape of a lipstick dispenser was added to a mobile stage that is part of the robot, in order to enable automated acquisition of images in each experiment chamber. The experiment chambers were redesigned to enable the use of sitting drops, enable backlighting of each specimen, and facilitate automation.

Hamrick, David T.↗

Automated Lab-on-a-Chip Electrophoresis System

Capillary electrophoresis is an analytical technique that can be used to detect and quantify extremely small amounts of various biological molecules. In the search for biochemical traces of life on other planets, part of this search involves an examination of amino acids, which are the building blocks of life on Earth. The most sensitive method for detecting amino acids is the use of laser induced fluorescence. However, since amino acids do not, in general, fluoresce, they first must be reacted with a fluorescent dye label prior to analysis. After this process is completed, the liquid sample then must be transported into the electrophoresis system. If the system is to be reused multiple times, samples must be added and removed each time. In typical laboratories, this process is performed manually by skilled human operators using standard laboratory equipment. This level of human intervention is not possible if this technology is to be implemented on extraterrestrial targets. Microchip capillary electrophoresis (CE) combined with laser induced fluorescence detection (LIF) was selected as an extremely sensitive method to detect amino acids and other compounds that can be tagged with a fluorescent dye. It is highly desirable to package this technology into an integrated, autonomous, in situ instrument capable of performing CE-LIF on the surface of an extraterrestrial body. However, to be fully autonomous, the CE device must be able to perform a large number of sample preparation and analysis operations without the direct intervention of a human.

Willis, Peter A.↗

Recirculating 1-K-Pot for Pulse-Tube Cryostats

A paper describes a 1-K-pot that works with a commercial pulse tube cooler for astrophysics instrumentation testbeds that require temperatures <1.7 K. Pumped liquid helium-4 cryostats were commonly used to achieve this temperature. However, liquid helium-4 cryostats are being replaced with cryostats using pulse tube coolers. The closed-cycle 1K-pot system for the pulse tube cooler requires a heat exchanger on the pulse tube, a flow restriction, pump-out line, and pump system that recirculates helium-4. The heat exchanger precools and liquefies helium- 4 gas at the 2.5 to 3.5 K pulse tube cold head. This closed-cycle 1-K-pot system was designed to work with commercially available laboratory pulse tube coolers. It was built using common laboratory equipment such as stainless steel tubing and a mechanical pump. The system is self-contained and requires only common wall power to operate. The lift of 15 mW at 1.1 K and base temperature of 0.97 K are provided continuously. The system can be scaled to higher heat lifts of .30 to 50 mW if desired. Ground-based telescopes could use this innovation to improve the efficiency of existing cryo

Paine, Christopher T.↗

Simulation of Detecting Damage in Composite Stiffened Panel Using Lamb Waves

Lamb wave damage detection in a composite stiffened panel is simulated by performing explicit transient dynamic finite element analyses and using signal imaging techniques. This virtual test process does not need to use real structures, actuators/sensors, or laboratory equipment. Quasi-isotropic laminates are used for the stiffened panels. Two types of damage are studied. One type is a damage in the skin bay and the other type is a debond between the stiffener flange and the skin. Innovative approaches for identifying the damage location and imaging the damage were developed. The damage location is identified by finding the intersection of the damage locus and the path of the time reversal wave packet re-emitted from the sensor nodes. The damage locus is a circle that envelops the potential damage locations. Its center is at the actuator location and its radius is computed by multiplying the group velocity by the time of flight to damage. To create a damage image for estimating the size of damage, a group of nodes in the neighborhood of the damage location is identified for applying an image condition. The image condition, computed at a finite element node, is the zero-lag cross-correlation (ZLCC) of the time-reversed incident wave signal and the time reversal wave signal from the sensor nodes. This damage imaging process is computationally efficient since only the ZLCC values of a small amount of nodes in the neighborhood of the identified damage location are computed instead of those of the full model.

Wang, John T.↗

Risk of Crew Adverse Health Event Due to Altered Immune Response

Determining the effect of space travel on the human immune system has proven to be extremely challenging. Limited opportunities for in-flight studies, varying mission durations, technical and logistical obstacles, small subject numbers, and a broad range of potential assays have contributed to this problem. Additionally, the inherent complexity of the immune system, with its vast array of cell populations, sub-populations, diverse regulatory molecules, and broad interactions with other physiological systems, makes determining precise variables to measure very difficult. There is also the challenge of determining the clinical significance of any observed immune alterations. Will such a change lead to disease, or is it a transient subclinical observation related to short-term stress? The effect of this problem may be observed by scanning publications associated with immunity and spaceflight, which began to appear during the 1970s. Although individually they are each valid studies, the comprehensive literature to date suffers from widely varying sampling methods and assay techniques, low subject counts, and sometimes a disparate focus on narrow aspects of immunity. The most clinically relevant data are derived from in-flight human studies, which have demonstrated altered cell-mediated immunity and reactivation of latent herpes viruses. Much more data are available from post-flight testing of humans, with clear evidence of altered cytokine production patterns, altered leukocyte distribution, continued latent viral reactivation, and evidence of dramatically altered virus-specific immunity. It is unknown if post-flight assessments relate to the in-flight condition or are a response to landing stress and readaptation. In-flight culture of cells has clearly demonstrated that immune cells are gravity-sensitive and display altered functional characteristics. It is unknown if these data are related to in vivo immune cell function or are an artifact of microgravity culture. Ground analog testing of humans and animals, as well as microgravity-analog cell culture, has demonstrated utility. However, in all cases, it is not known with certainty if these data would reflect similar testing during space travel. Given their ready availability, ground analogs may be extremely useful for assay development and the evaluation of potential countermeasures. In general, the evidence base suffers from widely disparate studies on small numbers of subjects that do not directly correlate well with each other or spaceflight itself. Also lacking are investigations of the effect of gender on adaption to spaceflight. This results in significant knowledge 'gaps' that must be filled by future studies to completely determine any clinical risk related to immunity for human exploration-class space missions. These gaps include a significant lack of in-flight data, particularly during long-duration space missions. The International Space Station represents an excellent science platform with which to address this knowledge gap. Other knowledge gaps include lack of a single validated ground analog for the phenomenon and a lack of flight-compatible laboratory equipment capable of monitoring astronauts (for either clinical or research purposes). However, enough significant data exist, as described in this manuscript, to warrant addressing this phenomenon during the utilization phase of the ISS. A recent Space Shuttle investigation has confirmed the 31 in-flight nature of immune dysregulation, demonstrating that it is not merely a post-flight phenomenon. Several current studies are ongoing onboard the ISS that should thoroughly characterize the phenomenon. NASA recognizes that if spaceflight-associated immune dysregulation persists during exploration flights in conjunction with other dangers, such as high-energy radiation, the result may be a significant clinical risk. This emphasizes the need for a continued integrated comprehensive approach to determining the effect of prolonged spaceflight, separated from transient launch and landing stresses, on human immunity. After such studies, the phenomenon will be understood, and, hopefully, a monitoring strategy will have been developed that could be used to monitor the effectiveness of countermeasure

Crucian, Brian↗

Portable Anthrax Testing with Lab-in-a-Pocket

BaDx (Bacillus anthracis Diagnostics) is a lab-in-a-pocket device to sample, sense, and diagnose bacteria that cause anthrax. It accomplishes these tasks in environments with no power, refrigerated storage, or laboratory equipment. BaDx was designed to be used with minimal or no training, and to keep handlers safe.

59 BASIC BIOLOGICAL SCIENCES↗

Fueling Nuclear Research at MFC: The Environmental Backbone of Nuclear Operations

The National Environmental Policy Act (NEPA) review guidelines are an essential part of the approval process of any construction or modification being done at Idaho National Laboratory (INL). The Material and Fuels Complex (MFC) Environmental team is responsible for writing and reviewing Environmental Impact Statements (EISs), Environmental Assessments (EAs), Environmental Compliance Permits (ECPs), Air Permitting Applicability Determinations (APADs), and other NEPA compliance documentation. This documentation allows for innovation in MFC research by permitting the introduction of new laboratory equipment, research facilities, and materials for researchers to use in their experiments. Without the work of the Environmental team, nuclear research and operations at MFC would not be possible.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Recent development of the Multi-Grid detector for large area neutron scattering instruments

Most of the Neutron Scattering facilities are committed in a continuous program of modernization of their instruments, requiring large area and high performance thermal neutron detectors. Beside scintillators detectors, {sup 3}He detectors, like linear PSDs (Position Sensitive Detectors) and MWPCs (Multi-Wires Proportional Chambers), are the most current techniques nowadays. Time Of Flight instruments are using {sup 3}He PSDs mounted side by side to cover tens of m{sup 2}. As a result of the so-called '{sup 3}He shortage crisis{sup ,} the volume of 3He which is needed to build one of these instruments is not accessible anymore. The development of alternative techniques requiring no 3He, has been given high priority to secure the future of neutron scattering instrumentation. This is particularly important in the context where the future ESS (European Spallation Source) will start its operation in 2019-2020. Improved scintillators represent one of the alternative techniques. Another one is the Multi-Grid introduced at the ILL in 2009. A Multi-Grid detector is composed of several independent modules of typically 0.8 m x 3 m sensitive area, mounted side by side in air or in a vacuum TOF chamber. One module is composed of segmented boron-lined proportional counters mounted in a gas vessel; the counters, of square section, are assembled with Aluminium grids electrically insulated and stacked together. This design provides two advantages: First, magnetron sputtering techniques can be used to coat B{sub 4}C films on planar substrates, and second, the neutron position along the anode wires can be measured by reading out individually the grid signals with fast shaping amplifiers followed by comparators. Unlike charge division localisation in linear PSDs, the individual readout of the grids allows operating the Multi-Grid at a low amplification gain, hence this detector is tolerant to mechanical defects and its production accessible to laboratories equipped with standard equipment. Prototypes of different configurations and sizes have been developed and tested. A demonstrator, with a sensitive area of 0.8 m x 3 m, has been studied during the CRISP European project; it contains 1024 grids, and a surface of isotopically enriched B{sub 4}C film close to 80 m{sup 2}. Its size represented a challenge in terms of fabrication and mounting of the detection elements. Another challenge was to make the gas chamber mechanically compatible with operation in a vacuum TOF chamber. Optimal working condition of this detector was achieved by flushing Ar-CO{sub 2} at a pressure of 50 mbar, and by applying 400 Volts on the anodes. This unusual gas pressure allows to greatly simplifying the mechanics of the gas vessel in vacuum. The detection efficiency has been measured with high precision for different film thicknesses. 52% has been measured at 2.5 Angstrom, in good agreement with the MC simulation. A high position resolution has been achieved by centre of gravity measurement of the TOT (Time-Over-Threshold) signals between neighbouring grids. These results, as well as other detection parameters, including gamma sensitivity and spatial uniformity, will be presented. (author)

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗