System analysis of gelled space-storable propellants Summary report, May 1967 - Apr. 1968
Structure and flow properties of liquid nitrogen and liquid oxygen difluoride gelled with solid chlorine trifluoride
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Incipient and developed cavitation in liquid cryogens
Cavitational flow of liquid nitrogen and liquid hydrogen in Venturi tube
Edmonds, D. K.↗
Bipropellant shut-off valve
An advanced design of an all metal, fast response, bipropellant, shut-off valve for use on long duration space missions is reported. The valve provides the flow control capability for a 1,000 lb thrust, bipropellant engine using oxygen difluoride and diborane as propellants. The shutoff seal selection is a soft-on-hard metal concept. The soft seal is a spherical shell that seats against a hard conical seat. Beryllium copper and beryllium nickel seals were selected to seal against an electrolyzed Inconel 718 seat. Poppet shaft sealing is achieved by use of hydroformed, Inconel 718 bellows. Two valve assemblies were fabricated and subjected to a series of tests including leak, response time, flow capacity, dry cycles, water cycles, liquid nitrogen cycles, liquid fluorine cycles, and lead-lag operation cycles. These tests demonstrated the ability of the valve to meet design goals.
Smith, J. V.↗
Energy distribution among reaction products. V.
Discussion of three reactions, one point of theoretical interest being the predicted correlation between barrier height and barrier location. The H + Br 2 reaction having a lower activation barrier than H + Cl 2, should have an earlier barrier, and hence a greater percentage attractive energy release and higher efficiency of vibrational excitation. Information is developed concerning the effect of isotopic substitution in the pair of reactions H + Cl 2 and D + Cl 2. The 'arrested relaxation' method was used. Essentially, the method involves reacting two diffuse reagent beams in a reaction vessel with background pressure less than 0.001 torr, and with walls cooled by liquid nitrogen or liquid helium.
Anlauf, K. G.↗
NERVA irradiation program. GTR 23, volume 1: Combined effects of reactor radiation and cryogenic temperature on NERVA structural materials
Specimens fabricated from structural materials that were candidates for certain NERVA applications were irradiated in liquid nitrogen (LN2), liquid hydrogen (LH2), water, and air. The specimens irradiated in LN2 were stored in LN2 and finally tested in LN2, or at some higher temperature in a few instances. The specimens irradiated in LH2 underwent an unplanned warmup while in storage so this portion of the test was lost; some specimens were tested in LN2 but none were tested in LH2. The Ground Test Reactor was the radiation source. The test specimens consisted mainly of tensile and fracture toughness specimens of several different materials, but other types of specimens such as tear, flexure, springs, and lubricant were also irradiated. Materials tested include Hastelloy X, Al, Ni steel, steel, Be, ZrC, Ti-6Al-4V, CuB, and Ti-5Al-2.5Sn.
Mcdaniel, R. H.↗
Boiling heat transfer to LN2 and LH2 - Influence of surface orientation and reduced body forces
The quantitative determination of the influence of heater surface orientation and gravity on nucleate pool boiling of liquid nitrogen and liquid hydrogen is described. A transient calorimeter technique, well suited for obtaining pool boiling data under reduced gravity and used earlier by Clark and Merte (1963), was employed after being adapted to flat a surface whose orientation could be varied. The obtained determination results are reviewed.
Merte, H., Jr.↗
Advanced development of Pb-salt semiconductor lasers for the 8.0 to 15.0 micrometer spectral region
The technology was studied for producing Pb-salt diode lasers for the 8-51 micron spectral region suitable for use as local oscillators in a passive Laser Heterodyne Spectrometer (LHS). Consideration was given to long range NASA plans for the utilization of the passive LHS in a space shuttle environment. The general approach was to further develop the method of compositional interdiffusion (CID) recently reported, and used successfully at shorter wavelength. This technology was shown to provide an effective and reproducible method of producing a single-heterostructure (SH) diode of either the heterojunction or single-sided configuration. Performance specifications were exceeded in several devices, with single-ended CW power outputs as high as 0.88 milliwatts in a mode being achieved. The majority of the CID lasers fabricated had CW operating temperatures of over 60K; 30% of them operated CW above the boiling temperature of liquid nitrogen. CW operation above liquid nitrogen temperature was possible for wavelengths as long as 10.3 microns. Operation at 77K is significant with respect to space shuttle operations since its allows considerable simplification of cooling method.
Linden, K. J.↗
Design of a horizonal liquid helium cryostat for refrigerating a flying superconducting magnet in a wind tunnel
The design of a horizontal liquid helium cryostat for refrigerating a flying superconducting magnet in a wind tunnel is presented. The basic principles of magnetic suspension theory are described and theoretical calculations of the superconducting magnet are provided. The experimental results of the boil-off of liquid nitrogen and liquid helium in the cryostat are reported.
Wu, Y. Y.↗
Silicon Nitride Balls For Cryogenic Bearings
Resistance to wear greater than that of 440C steel. Experiments show lives of ball bearings immersed in liquid nitrogen or liquid oxygen increased significantly when 440C steel balls (running on 440C steel races) replaced by balls of silicon nitride. Developed for use at high temperatures, where lubrication poor or nonexistent. Best wear life of any bearing tested to date and ball material spalls without fracturing. Plans for future tests call for use of liquid oxygen as working fluid.
Butner, Myles F.↗
Test program, helium II orbital resupply coupling
The full scope of this program was to have included development tests, design and production of custom test equipment and acceptance and qualification testing of prototype and protoflight coupling hardware. This program was performed by Ball Aerospace Systems Division, Boulder, Colorado until its premature termination in May 1991. Development tests were performed on cryogenic face seals and flow control devices at superfluid helium (He II) conditions. Special equipment was developed to allow quantified leak detection at large leak rates up to 8.4 x 10(exp -4) SCCS. Two major fixtures were developed and characterized: The Cryogenic Test Fixture (CTF) and the Thermal Mismatch Fixture (Glovebox). The CTF allows the coupling hardware to be filled with liquid nitrogen (LN2), liquid helium (LHe) or sub-cooled liquid helium when hardware flow control valves are either open or closed. Heat leak measurements, internal and external helium leakage measurements, cryogenic proof pressure tests and external load applications are performed in this fixture. Special reusable MLI closures were developed to provide repeatable installations in the CTF. The Thermal Mismatch Fixture allows all design configurations of coupling hardware to be engaged and disengaged while measuring applied forces and torques. Any two hardware components may be individually thermally preconditioned within the range of 117 deg K to 350 deg K prior to engage/disengage cycling. This verifies dimensional compatibility and operation when thermally mismatched. A clean, dry GN2 atmosphere is maintained in the fixture at all times. The first shipset of hardware was received, inspected and cycled at room temperature just prior to program termination.
Hyatt, William S.↗
Experimental study of foam-insulated liquified-gas tanks
Experiments with liquid nitrogen and liquid hydrogen is styrofoam-insulated tanks have indicated good agreement between measured and calculated heat-leak rates when the insulation was formed from a single block of material. In a large tank installation where the insulation was applied in sections without sealing the joints, the measured heat leak was about 2 and 1/2 times the calculated value.
Reynolds, Thaine W↗
Cryogenic probe station for use in automated microwave and noise figure measurements
A cryogenic measurement system capable of performing on-wafer RF testing of semiconductor devices and circuits has been developed. This 'CryoProbe Station' can wafer-probe devices and circuits at cryogenic temperatures, thus eliminating the need for wire bonds. The system operates under vacuum created by a sorption pump. It uses an open cycle cooling system that can be cooled with either liquid nitrogen or liquid helium. Presently, it can reach temperatures, as low as 80 K and 37 K for each of the coolants, respectively. The temperature can be raised using a heater and it is stabilized to within 0.2 K by use of a temperature controller. The CryoProbe Station features a 1 by 2 inch stage that can hold large circuits and calibration standards simultaneously. The system is used with a Hewlett Packard 8510C Automatic Network Analyzer (ANA) to obtain S-parameter data over the frequency range 0.045-26.5 GHz. S-parameter data on HEMT (high electron mobility transistors) devices has been obtained with this station. With the use of DEEMBED software from NIST, detailed transmission line studies have been performed. Although the CryoProbe Station is designed for frequencies up to 26.5 GHz, useful transmission line data has been obtained for frequencies as high as 40 GHz. The CryoProbe station has also been used with the ATN noise figure measurement system to perform automatic, temperature dependent noise figure measurements.
Taub, Susan R.↗
Polymer Matrix Composite Lines and Ducts
Since composite laminates are beginning to be identified for use in reusable launch vehicle propulsion systems, a task was undertaken to assess the feasibility of making cryogenic feedlines with integral flanges from polymer matrix composite materials. An additional level of complexity was added by having the feedlines be elbow shaped. Four materials, each with a unique manufacturing method, were chosen for this program. Feedlines were to be made by hand layup (HLU) with standard autoclave cure, HLU with electron beam cure, solvent-assisted resin transfer molding (SARTM), and thermoplastic tape laying (TTL). A test matrix of fill and drain cycles with both liquid nitrogen and liquid helium, along with a heat up to 250 F, was planned for each of the feedlines. A pressurization to failure was performed on any feedlines that passed the cryogenic cycling testing. A damage tolerance subtask was also undertaken in this study. The effects of foreign object impact to the materials used was assessed by cross-sectional examination and by permeability after impact testing. At the end of the program, the manufacture of the electron beam-cured feedlines never came to fruition. All of the TTL feedlines leaked heavily before any cryogenic testing, all of the SARTM feedlines leaked heavily after one cryogenic cycle. Thus, only the HLU with autoclave cure feedlines underwent the complete test matrix. They passed the cyclic testing and were pressurized to failure.
Nettles, A. T.↗
Simulations of Cavitating Cryogenic Inducers
Simulations of cavitating turbopump inducers at their design flow rate are presented. Results over a broad range of Nss, numbers extending from single-phase flow conditions through the critical head break down point are discussed. The flow characteristics and performance of a subscale geometry designed for water testing are compared with the fullscale configuration that employs LOX. In particular, thermal depression effects arising from cavitation in cryogenic fluids are identified and their impact on the suction performance of the inducer quantified. The simulations have been performed using the CRUNCH CFD[R] code that has a generalized multi-element unstructured framework suitable for turbomachinery applications. An advanced multi-phase formulation for cryogenic fluids that models temperature depression and real fluid property variations is employed. The formulation has been extensively validated for both liquid nitrogen and liquid hydrogen by simulating the experiments of Hord on hydrofoils; excellent estimates of the leading edge temperature and pressure depression were obtained while the comparisons in the cavity closure region were reasonable.
Dorney, Dan↗
Liquid Acquisition Device Testing with Sub-Cooled Liquid Oxygen
When transferring propellant in space, it is most efficient to transfer single phase liquid from a propellant tank to an engine. In earth s gravity field or under acceleration, propellant transfer is fairly simple. However, in low gravity, withdrawing single-phase fluid becomes a challenge. A variety of propellant management devices (PMD) are used to ensure single-phase flow. One type of PMD, a liquid acquisition device (LAD) takes advantage of capillary flow and surface tension to acquire liquid. Previous experimental test programs conducted at NASA have collected LAD data for a number of cryogenic fluids, including: liquid nitrogen (LN2), liquid oxygen (LOX), liquid hydrogen (LH2), and liquid methane (LCH4). The present work reports on additional testing with sub-cooled LOX as part of NASA s continuing cryogenic LAD development program. Test results extend the range of LOX fluid conditions examined, and provide insight into factors affecting predicting LAD bubble point pressures.
Jurns, John M.↗
Pumping and Depressurizing of Insulation Materials
The Fluids Testing and Technology Branch is a group that researches and tests efficient ways to use various Cryogenic Fluids, such as Liquid Nitrogen or Liquid Helium, in ground and space systems. Their main goal is to develop new technologies involving Cryogenic temperatures as well as making sure the existing technologies are understood. During my time here a lot of insulation testing has been done which is where insulation systems are tested for cryogenic systems that are in space for long durations.
Porter, Amber↗
Hybrid Composite Cryogenic Tank Structure
A hybrid lightweight composite tank has been created using specially designed materials and manufacturing processes. The tank is produced by using a hybrid structure consisting of at least two reinforced composite material systems. The inner composite layer comprises a distinct fiber and resin matrix suitable for cryogenic use that is a braided-sleeve (and/or a filamentwound layer) aramid fiber preform that is placed on a removable mandrel (outfitted with metallic end fittings) and is infused (vacuum-assisted resin transfer molded) with a polyurethane resin matrix with a high ductility at low temperatures. This inner layer is allowed to cure and is encapsulated with a filamentwound outer composite layer of a distinct fiber resin system. Both inner and outer layer are in intimate contact, and can also be cured at the same time. The outer layer is a material that performs well for low temperature pressure vessels, and it can rely on the inner layer to act as a liner to contain the fluids. The outer layer can be a variety of materials, but the best embodiment may be the use of a continuous tow of carbon fiber (T-1000 carbon, or others), or other high-strength fibers combined with a high ductility epoxy resin matrix, or a polyurethane matrix, which performs well at low temperatures. After curing, the mandrel can be removed from the outer layer. While the hybrid structure is not limited to two particular materials, a preferred version of the tank has been demonstrated on an actual test tank article cycled at high pressures with liquid nitrogen and liquid hydrogen, and the best version is an inner layer of PBO (poly-pphenylenebenzobisoxazole) fibers with a polyurethane matrix and an outer layer of T-1000 carbon with a high elongation epoxy matrix suitable for cryogenic temperatures. A polyurethane matrix has also been used for the outer layer. The construction method is ideal because the fiber and resin of the inner layer has a high strain to failure at cryogenic temperatures, and will not crack or produce leaks. The outer layer serves as more of a high-performance structural unit for the inner layer, and can handle external environments.
DeLay, Thomas↗
Computing Thermal Effects of Cavitation in Cryogenic Liquids
A computer program implements a numerical model of thermal effects of cavitation in cryogenic fluids. The model and program were developed for use in designing and predicting the performances of turbopumps for cryogenic fluids. Prior numerical models used for this purpose do not account for either the variability of properties of cryogenic fluids or the thermal effects (especially, evaporative cooling) involved in cavitation. It is important to account for both because in a cryogenic fluid, the thermal effects of cavitation are substantial, and the cavitation characteristics are altered by coupling between the variable fluid properties and the phase changes involved in cavitation. The present model accounts for both thermal effects and variability of properties by incorporating a generalized representation of the properties of cryogenic fluids into a generalized compressible-fluid formulation for a cavitating pump. The model has been extensively validated for liquid nitrogen and liquid hydrogen. Using the available data on the properties of these fluids, the model has been shown to predict accurate temperature-depression values.
Hosangadi, Ashvin↗