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DOE OSTI2021

Potential Activities and Long Lifetimes of Organic Carbon-Degrading Extracellular Enzymes in Deep Subsurface Sediments of the Baltic Sea

Heterotrophic microorganisms in marine sediments produce extracellular enzymes to hydrolyze organic macromolecules, so their products can be transported inside the cell and used for energy and growth. Therefore, extracellular enzymes may mediate the fate of organic carbon in sediments. The Baltic Sea Basin is a primarily depositional environment with high potential for organic matter preservation. The potential activities of multiple organic carbon-degrading enzymes were measured in samples obtained by the International Ocean Discovery Program Expedition 347 from the Little Belt Strait, Denmark, core M0059C. Potential maximum hydrolysis rates (V max ) were measured at depths down to 77.9mbsf for the following enzymes: alkaline phosphatase, β- d -xylosidase, β- d -cellobiohydrolase, N-acetyl-β- d -glucosaminidase, β-glucosidase, α-glucosidase, leucyl aminopeptidase, arginyl aminopeptidase, prolyl aminopeptidase, gingipain, and clostripain. Extracellular peptidase activities were detectable at depths shallower than 54.95mbsf, and alkaline phosphatase activity was detectable throughout the core, albeit against a relatively high activity in autoclaved sediments. β-glucosidase activities were detected above 30mbsf; however, activities of other glycosyl hydrolases (β-xylosidase, β-cellobiohydrolase, N-acetyl-β-glucosaminidase, and α-glucosidase) were generally indistinguishable from zero at all depths. These extracellular enzymes appear to be extremely stable: Among all enzymes, a median of 51.3% of enzyme activity was retained after autoclaving for an hour. We show that enzyme turnover times scale with the inverse of community metabolic rates, such that enzyme lifetimes in subsurface sediments, in which metabolic rates are very slow, are likely to be extraordinarily long. A back-of-the-envelope calculation suggests enzyme lifetimes are, at minimum, on the order of 230days, and may be substantially longer. These results lend empirical support to the hypothesis that a population of subsurface microbes persist by using extracellular enzymes to slowly metabolize old, highly degraded organic carbon.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2018

Bootstrap inversion technique for atmospheric trace gas source detection and quantification using long open-path laser measurements

Advances in natural gas extraction technology have led to increased activity in the production and transport sectors in the United States and, as a consequence, an increased need for reliable monitoring of methane leaks to the atmosphere. We present a statistical methodology in combination with an observing system for the detection and attribution of fugitive emissions of methane from distributed potential source location landscapes such as natural gas production sites. We measure long (> 500 m), integrated open-path concentrations of atmospheric methane using a dual frequency comb spectrometer and combine measurements with an atmospheric transport model to infer leak locations and strengths using a novel statistical method, the non-zero minimum bootstrap (NZMB). The new statistical method allows us to determine whether the empirical distribution of possible source strengths for a given location excludes zero. Using this information, we identify leaking source locations (i.e., natural gas wells) through rejection of the null hypothesis that the source is not leaking. The method is tested with a series of synthetic data inversions with varying measurement density and varying levels of model–data mismatch. It is also tested with field observations of (1) a non-leaking source location and (2) a source location where a controlled emission of 3.1 × 10 -5 kg s -1 of methane gas is released over a period of several hours. This series of synthetic data tests and outdoor field observations using a controlled methane release demonstrates the viability of the approach for the detection and sizing of very small leaks of methane across large distances (4 + km 2 in synthetic tests). The field tests demonstrate the ability to attribute small atmospheric enhancements of 17 ppb to the emitting source location against a background of combined atmospheric (e.g., background methane variability) and measurement uncertainty of 5 ppb (1 σ ), when measurements are averaged over 2 min. The results of the synthetic and field data testing show that the new observing system and statistical approach greatly decreases the incidence of false alarms (that is, wrongly identifying a well site to be leaking) compared with the same tests that do not use the NZMB approach and therefore offers increased leak detection and sizing capabilities.

03 NATURAL GAS↗

DOE OSTI2016

Performance Evaluation of Spectroscopic Detectors for LEU Hold-up Measurements

The hold-up measurement of low-enriched uranium materials may require use of alternate detector types relative to the measurement of highly enriched uranium. This is in part due to the difference in process scale (i.e., the components are generally larger for low-enriched uranium systems), but also because the characteristic gamma-ray lines from 235 U used for assay of highly enriched uranium will be present at a much reduced intensity (on a per gram of uranium basis) at lower enrichments. Researchers at Oak Ridge National Laboratory examined the performance of several standard detector types, e.g., NaI(Tl), LaBr3(Ce), and HPGe, to select a suitable candidate for measuring and quantifying low-enriched uranium hold-up in process pipes and equipment at the Portsmouth gaseous diffusion plant. Detector characteristics, such as energy resolution (full width at half maximum) and net peak count rates at gamma ray energies spanning a range of 60–1332 keV, were measured for the above-mentioned detector types using the same sources and in the same geometry. Uranium enrichment standards (Certified Reference Material no. 969 and Certified Reference Material no. 146) were measured using each of the detector candidates in the same geometry. The net count rates recorded by each detector at 186 keV and 1,001 keV were plotted as a function of enrichment (atom percentage). Background measurements were made in unshielded and shielded configurations under both ambient and elevated conditions of 238 U activity. The highly enriched uranium hold-up measurement campaign at the Portsmouth plant was performed on process equipment that had been cleaned out. Therefore, in most cases, the thickness of the uranium deposits was less than the “infinite thickness” for the 186 keV gamma rays to be completely self-attenuated. Because of this, in addition to measuring the 186 keV gamma, the 1,001 keV gamma ray from 234m Pa—a daughter of 238 U in secular equilibrium with its parent—will also need to be measured. Based on the performance criteria of detection efficiency, energy resolution, peak-to-continuum ratios, minimum detectable limits, and the weight of the shielded probe, a shielded (0.5 in. thick lead shield) 2 × 2 in. NaI(Tl) detector is recommended for use. The recommended approach is to carry out analysis using data from both 186 keV and 1,001 keV gamma rays, and select a best result based on propagated uncertainty estimates. It is also highly recommended that a two-point gain stabilization scheme based on an 241 Am seed embedded in the probe be implemented. Shielding configurations to reduce the impact of background interference on the measurement of 1,001 keV gamma-ray are discussed.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2018

Effect of betulinic acid and its ionic derivatives on M-MuLV replication

Murine leukemia virus (MuLV) is a retrovirus known causing leukemia and neurological disorders in mice, and its viral life cycle and pathogenesis have been investigated extensively over the past decades. As a natural antiviral agent, betulinic acid is a pentacyclic triterpenoid that can be found in the bark of several species of plants (particularly the white birch). One of the hurdles for betulinic acid to release its antiviral potency is its poor water solubility. In this study, we synthesized more water-soluble ionic derivatives of betulinic acid, and examined their activities against Moloney MuLV (M-MuLV). The mouse fibroblast cells stably infected with M-MuLV, 43D cells, were treated with various doses of betulinic acids and its derivatives, and the viral structural protein Gag in cells and media were detected by western blots. Two ionic derivatives containing the benzalkonium cation were found to inhibit the virus production into media and decreased Gag in cells. However, a cell proliferation assay showed that the benzalkonium cation inhibited the growth of 43D cells, suggesting that our ionic derivatives limited virus production through the inhibition of metabolism in 43D cells. Interestingly, all of these betulinic acid compounds exhibited a minimum impact on the processing and release of Gag from 43D cells, which outlines the differences of viral maturation between MuLV and human immunodeficiency virus.

60 APPLIED LIFE SCIENCES↗

DOE OSTI2010

IDENTIFICATION OF FAINT CHANDRA X-RAY SOURCES IN THE CORE-COLLAPSED GLOBULAR CLUSTER NGC 6397: EVIDENCE FOR A BIMODAL CATACLYSMIC VARIABLE POPULATION

We have searched for optical identifications for 79 Chandra X-ray sources that lie within the half-mass radius of the nearby, core-collapsed globular cluster NGC 6397, using deep Hubble Space Telescope Advanced Camera for Surveys Wide Field Channel imaging in H{alpha}, R, and B. Photometry of these images allows us to classify candidate counterparts based on color-magnitude diagram location. In addition to recovering nine previously detected cataclysmic variables (CVs), we have identified six additional faint CV candidates, a total of 42 active binaries (ABs), two millisecond pulsars, one candidate active galactic nucleus, and one candidate interacting galaxy pair. Of the 79 sources, 69 have a plausible optical counterpart. The 15 likely and possible CVs in NGC 6397 mostly fall into two groups: a brighter group of six for which the optical emission is dominated by contributions from the secondary and accretion disk and a fainter group of seven for which the white dwarf dominates the optical emission. There are two possible transitional objects that lie between these groups. The faintest CVs likely lie near the minimum of the CV period distribution, where an accumulation is expected. The spatial distribution of the brighter CVs is much more centrally concentrated than those of the fainter CVs and the ABs. This may represent the result of an evolutionary process in which CVs are produced by dynamical interactions, such as exchange reactions, near the cluster center and are scattered to larger orbital radii, over their lifetimes, as they age and become fainter.

79 ASTRONOMY AND ASTROPHYSICS↗

DOE OSTI2016

SAR11 bacteria linked to ocean anoxia and nitrogen loss

Bacteria of the SAR11 clade constitute up to one half of all microbial cells in the oxygen-rich surface ocean. SAR11 bacteria are also abundant in oxygen minimum zones (OMZs), where oxygen falls below detection and anaerobic microbes have vital roles in converting bioavailable nitrogen to N 2 gas. Anaerobic metabolism has not yet been observed in SAR11, and it remains unknown how these bacteria contribute to OMZ biogeochemical cycling. Here in this paper, genomic analysis of single cells from the world's largest OMZ revealed previously uncharacterized SAR11 lineages with adaptations for life without oxygen, including genes for respiratory nitrate reductases (Nar). SAR11 nar genes were experimentally verified to encode proteins catalysing the nitrite-producing first step of denitrification and constituted ~40% of OMZ nar transcripts, with transcription peaking in the anoxic zone of maximum nitrate reduction activity. Finally, these results link SAR11 to pathways of ocean nitrogen loss, redefining the ecological niche of Earth's most abundant organismal group.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2011

MODEL SPECTRA OF THE FIRST POTENTIALLY HABITABLE SUPER-EARTH-Gl581d

Gl581d has a minimum mass of 7 M{sub Earth} and is the first detected potentially habitable rocky Super-Earth. Our models confirm that a habitable atmosphere can exist on Gl581d. We derive spectroscopic features for atmospheres assuming an Earth-like composition for this planet, from high-oxygen atmosphere analogous to Earth's to high-CO{sub 2} atmospheres with and without biotic oxygen concentrations. We find that a minimum CO{sub 2} partial pressure of about 7 bar, in an atmosphere with a total surface pressure of 7.6 bar, is needed to maintain a mean surface temperature above freezing on Gl581d. We model transmission and emergent synthetic spectra from 0.4 {mu}m to 40 {mu}m and show where indicators of biological activities in such a planet's atmosphere could be observed by future ground- and space-based telescopes. The model we present here only represents one possible nature-an Earth-like composition-of a planet like Gl581d in a wide parameter space. Future observations of atmospheric features can be used to examine if our concept of habitability and its dependence on the carbonate-silicate cycle is correct, and assess whether Gl581d is indeed a habitable Super-Earth.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DOE OSTI2019

CY2018 Annual Closure Monitoring Report for Corrective Action Unit 98, Frenchman Flat, Underground Test Area, Nevada National Security Site, Nevada (January 2018–December 2018, Revision 1)

Corrective Action Unit (CAU) 98: Frenchman Flat on the Nevada National Security Site was the location of 10 underground nuclear tests. CAU 98 underwent a series of investigations and actions in accordance with the Federal Facility Agreement and Consent Order to assess contamination of groundwater by radionuclides from the tests. A Closure Report completed that process in 2016 and called for long-term monitoring, use restrictions (URs), and institutional controls to protect the public and environment from potential exposure to contaminated groundwater. Three types of monitoring are performed for CAU 98: water quality, water level, and institutional control. These are monitored to determine whether the URs remain protective of human health and the environment, and to ensure that the regulatory boundary objectives are being met. Monitoring data will be used in the future, once multiple years of data are available, to evaluate consistency with the groundwater flow and contaminant transport models because the contaminant boundaries calculated with the models are the primary basis of the UR boundaries. Six wells were sampled for water-quality monitoring in 2018. Contaminants of concern were detected only in the two source/plume wells already known to contain contamination as a result of a radionuclide migration experiment. Tritium concentrations in both of these wells, RNM-2S and UE-5n, remain above the Safe Drinking Water Act maximum contaminant level of 20,000 picocuries per liter but declined in 2018 as compared to measurements in 2017. All other contaminants of concern are below the minimum detection level plus analytical error. The water-level monitoring network includes 16 wells. Depth to water measured in 2018 is generally consistent with recent measurements for all wells. Many wells continue to exhibit a long-term downward trend in water level, despite small increases in measured water levels in 2018. The sharp 2016 decline in water level in Well ER-5-3-2 remains unexplained, with the lower level persisting through 2018. Rising water-level trends continue to be observed in two relatively deep wells (ER-5-3 deep piezometer and ER-5-4-2), and also in former supply Well WW-5A. The current supply wells exhibit relatively erratic water levels associated with pumping activities. Institutional control monitoring confirmed the URs are recorded in U.S. Department of Energy and U.S. Air Force land management systems, and that no activities within Frenchman Flat basin are occurring that could potentially affect the contaminant boundaries. Survey of groundwater resources in basins surrounding Frenchman Flat similarly identify no current or pending development that would indicate the need to increase monitoring activities or would otherwise cause concern for the closure decision. The URs continue to prevent exposure of the public, workers, and the environment to contaminants of concern by preventing use of potentially contaminated groundwater.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2010

Investigation of the solar influence on the cosmic muon flux using WILLI detector

A fesibility study to explore the capability of the WILLI detector to observe the solar events/activity by recording the muon intensity at ground level is presented.The WILLI detector, set up in National Institute of Physics and Nuclear Engineering, Bucharest, is a 1 m{sup 2} incident area sampling calorimeter. It can measure simultaneously muon events with the muon energy {>=}0.4 GeV and, if the muons are stopped in the detector, and muon energy between 0.4<E{sub {mu}<}0.6 GeV, if the muons pass the minimum of 2 plates of the detector stack.Taking into account muon events with energy {>=}0.4 GeV, a modulation of the muon intensity as a diurnal variation is observed. Muon events for a smaller energy range (0.4-0.6 GeV) seem to exhibit an aperiodic variation of the muon intensity, which could be correlated with magnetic activity indicated by the planetary K{sub p} index.

79 ASTRONOMY AND ASTROPHYSICS↗

DOE OSTI2011

TURBULENT DIFFUSION IN THE PHOTOSPHERE AS DERIVED FROM PHOTOSPHERIC BRIGHT POINT MOTION

On the basis of observations of solar granulation obtained with the New Solar Telescope of Big Bear Solar Observatory, we explored proper motion of bright points (BPs) in a quiet-sun area, a coronal hole, and an active region plage. We automatically detected and traced BPs and derived their mean-squared displacements as a function of time (starting from the appearance of each BP) for all available time intervals. In all three magnetic environments, we found the presence of a super-diffusion regime, which is the most pronounced inside the time interval of 10-300 s. Super-diffusion, measured via the spectral index, {gamma}, which is the slope of the mean-squared displacement spectrum, increases from the plage area ({gamma} = 1.48) to the quiet-sun area ({gamma} = 1.53) to the coronal hole ({gamma} = 1.67). We also found that the coefficient of turbulent diffusion changes in direct proportion to both temporal and spatial scales. For the minimum spatial scale (22 km) and minimum time scale (10 s), it is 22 and 19 km{sup 2} s{sup -1} for the coronal hole and the quiet-sun area, respectively, whereas for the plage area it is about 12 km{sup 2} s{sup -1} for the minimum time scale of 15 s. We applied our BP tracking code to three-dimensional MHD model data of solar convection and found the super-diffusion with {gamma} = 1.45. An expression for the turbulent diffusion coefficient as a function of scales and {gamma} is obtained.

79 ASTRONOMY AND ASTROPHYSICS↗

DOE OSTI2015

SOLAR CYCLE VARIATION OF THE INTER-NETWORK MAGNETIC FIELD

The solar inter-network magnetic field is the weakest component of solar magnetism, but it contributes most of the solar surface magnetic flux. The study of its origin has been constrained by the inadequate tempospatial resolution and sensitivity of polarization observations. With dramatic advances in spatial resolution and detecting sensitivity, the solar spectropolarimetry provided by the Solar Optical Telescope on board Hinode in an interval from the solar minimum to maximum of cycle 24 opens an unprecedented opportunity to study the cyclic behavior of the solar inter-network magnetic field. More than 1000 Hinode magnetograms observed from 2007 January to 2014 August are selected in the study. It has been found that there is a very slight correlation between sunspot number and magnetic field at the inter-network flux spectrum. From solar minimum to maximum of cycle 24, the flux density of the solar inter-network field is invariant, at 10 ± 1 G. The observations suggest that the inter-network magnetic field does not arise from flux diffusion or flux recycling of solar active regions, thereby indicating the existence of a local small-scale dynamo. Combining the full-disk magnetograms observed by the Solar and Heliospheric Observatory/Michelson Doppler Imager and the Solar Dynamics Observatory/Helioseismic and Magnetic Imager in the same period, we find that the area ratio of the inter-network region to the full disk of the Sun apparently decreases from solar minimum to maximum but always exceeds 60%, even in the phase of solar maximum.

79 ASTRONOMY AND ASTROPHYSICS↗

DOE OSTI2016

Integrated PET/MR breast cancer imaging: Attenuation correction and implementation of a 16-channel RF coil

Purpose: This study aims to develop, implement, and evaluate a 16-channel radiofrequency (RF) coil for integrated positron emission tomography/magnetic resonance (PET/MR) imaging of breast cancer. The RF coil is designed for optimized MR imaging performance and PET transparency and attenuation correction (AC) is applied for accurate PET quantification. Methods: A 16-channel breast array RF coil was designed for integrated PET/MR hybrid imaging of breast cancer lesions. The RF coil features a lightweight rigid design and is positioned with a spacer at a defined position on the patient table of an integrated PET/MR system. Attenuation correction is performed by generating and applying a dedicated 3D CT-based template attenuation map. Reposition accuracy of the RF coil on the system patient table while using the positioning frame was tested in repeated measurements using MR-visible markers. The MR, PET, and PET/MR imaging performances were systematically evaluated using modular breast phantoms. Attenuation correction of the RF coil was evaluated with difference measurements of the active breast phantoms filled with radiotracer in the PET detector with and without the RF coil in place, serving as a standard of reference measurement. The overall PET/MR imaging performance and PET quantification accuracy of the new 16-channel RF coil and its AC were then evaluated in first clinical examinations on ten patients with local breast cancer. Results: The RF breast array coil provides excellent signal-to-noise ratio and signal homogeneity across the volume of the breast phantoms in MR imaging and visualizes small structures in the phantoms down to 0.4 mm in plane. Difference measurements with PET revealed a global loss and thus attenuation of counts by 13% (mean value across the whole phantom volume) when the RF coil is placed in the PET detector. Local attenuation ranging from 0% in the middle of the phantoms up to 24% was detected in the peripheral regions of the phantoms at positions closer to attenuating hardware structures of the RF coil. The position accuracy of the RF coil on the patient table when using the positioning frame was determined well below 1 mm for all three spatial dimensions. This ensures perfect position match between the RF coil and its three-dimensional attenuation template during the PET data reconstruction process. When applying the CT-based AC of the RF coil, the global attenuation bias was mostly compensated to ±0.5% across the entire breast imaging volume. The patient study revealed high quality MR, PET, and combined PET/MR imaging of breast cancer. Quantitative activity measurements in all 11 breast cancer lesions of the ten patients resulted in increased mean difference values of SUV{sub max} 11.8% (minimum 3.2%; maximum 23.2%) between nonAC images and images when AC of the RF breast coil was applied. This supports the quantitative results of the phantom study as well as successful attenuation correction of the RF coil. Conclusions: A 16-channel breast RF coil was designed for optimized MR imaging performance and PET transparency and was successfully integrated with its dedicated attenuation correction template into a whole-body PET/MR system. Systematic PET/MR imaging evaluation with phantoms and an initial study on patients with breast cancer provided excellent MR and PET image quality and accurate PET quantification.

60 APPLIED LIFE SCIENCES↗

DOE OSTI2017

Electrooptical effect in the plasmon structure glass–In{sub 2}O{sub 3}: Sn–ferroelectric–Al with a subwavelength grating

The spectral features of the electrooptical effect, in which an applied voltage changes the refractive index of a ferroelectric copolymer, are studied. Three nanostructures are investigated: two nanostructures play an auxiliary role, and the basic structure consists of a glass substrate, a transparent ITO (In{sub 2}O{sub 3}: Sn) layer, active copolymer layer, and an Al layer with a nanograting. This grating with a period of 400 nm meets the conditions of excitation of plasmon resonances. The light transmission coefficients of all structures are analyzed in the spectral range 400–900 nm. The transmission spectra have two characteristic plasmon dips, one of which is related to the copolymer–ITO interface and the other, to the copolymer–Al interface. The aluminum and ITO layers play the role of electrodes, which supply voltage pulses (from 0 to 15 V) to the copolymer layer. When studying the electrooptical effect, we detected spectral shifts in plasmon resonance bands when the amplitudes of both positive and negative voltage pulses (quadratic effect) increase. These shifts change the effective refractive indices (n{sub eff}) of the structural elements, reaching the minimum negative increment Δ{sub eff} =–0.06.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

DOE OSTI2010

STATISTICAL STUDY OF CORONAL MASS EJECTIONS WITH AND WITHOUT DISTINCT LOW CORONAL SIGNATURES

Taking advantage of the two viewpoints of the STEREO spacecraft, we present a statistical study of coronal mass ejections (CMEs) with and without distinct low coronal signatures (LCSs) from 2009 January 1 to August 31. During this period, the lines of sight from STEREO A and B are almost perpendicular and nearly a quarter of the Sun was observed by both. We identified 34 CMEs that originated from around this area and find that (1) about 1 out of 3 CMEs that were studied during 8 months of solar minimum activity are stealth CMEs; a CME is stealth if no distinct LCS (such as coronal dimming, coronal wave, filament eruption, flare, post-eruptive arcade) can be found on the disk. (2) The speeds of the stealth CMEs without LCSs are typically below 300 km s{sup -1}. Comparing with the slow CMEs with LCSs, the stealth CMEs did not show any clear differences in their velocity and acceleration evolution. (3) The source regions of the stealth CMEs are usually located in the quiet Sun rather than active regions. Detailed study indicates that more than half of the stealth CMEs in this paper showed some faint change of the coronal structures (likely parts of flux ropes) when they could be observed over the solar limb before or during the CME evolution. Finally, we note that space weather detection systems based on LCSs totally independent of coronagraph data may fail to detect a significant proportion of CMEs.

79 ASTRONOMY AND ASTROPHYSICS↗

DOE OSTI2014

TENTATIVE EVIDENCE FOR RELATIVISTIC ELECTRONS GENERATED BY THE JET OF THE YOUNG SUN-LIKE STAR DG Tau

Synchrotron emission has recently been detected in the jet of a massive protostar, providing further evidence that certain jet formation characteristics for young stars are similar to those found for highly relativistic jets from active galactic nuclei. We present data at 325 and 610 MHz taken with the Giant Metrewave Radio Telescope of the young, low-mass star DG Tau, an analog of the Sun soon after its birth. This is the first investigation of a low-mass young stellar object at such low frequencies. We detect emission with a synchrotron spectral index in the proximity of the DG Tau jet and interpret this emission as a prominent bow shock associated with this outflow. This result provides tentative evidence for the acceleration of particles to relativistic energies due to the shock impact of this otherwise very low-power jet against the ambient medium. We calculate the equipartition magnetic field strength B {sub min} ≈ 0.11 mG and particle energy E {sub min} ≈ 4 × 10{sup 40} erg, which are the minimum requirements to account for the synchrotron emission of the DG Tau bow shock. These results suggest the possibility of low energy cosmic rays being generated by young Sun-like stars.

79 ASTRONOMY AND ASTROPHYSICS↗

DOE OSTI2019

Earthquake Arrival Association with Backprojection and Graph Theory

The association of seismic-wave arrivals with causative earthquakes becomes progressively more challenging as arrival detection methods become more sensitive, and particularly when earthquake rates are high. For instance, seismic waves arriving across a monitoring network from several sources may overlap in time, false arrivals may be detected, and some arrivals may be of unknown phase (e.g., P or S waves). We propose an automated method to associate arrivals with earthquake sources and obtain source locations applicable to such situations. To do so, we use a pattern detection metric based on the principle of back-projection to reveal candidate sources followed by graph-theory-based clustering and an integer linear optimization routine to associate arrivals with the minimum number of sources necessary to explain the data. We find that this method solves for all sources and phase assignments simultaneously, rather than in a sequential greedy procedure as is common in other association routines. We demonstrate our method on both synthetic and real data from the Integrated Plate Boundary Observatory Chile seismic network of northern Chile. For the synthetic tests, we report results for cases with varying complexity, including rates of 500 earthquakes/day and 500 false arrivals/station/day, for which we measure true positive detection accuracy of >95%. For the real data, we develop a new catalog between 1 January 2010 and 31 December 2017 containing 817,548 earthquakes, with detection rates on average 279 earthquakes/day and a magnitude-of-completion of M~1.8. A subset of detections are identified as sources related to quarry and industrial site activity, and we also detect thousands of foreshocks and aftershocks of the 1 April 2014 Mw 8.2 Iquique earthquake. During the highest rate of aftershock activity, >600 earthquakes/day are detected in the vicinity of the Iquique earthquake rupture zone.

58 GEOSCIENCES↗

DOE OSTI2017

A novel approach to criticality accident detection for a legacy facility

For operations on the Sellafield site involving fissile material a Criticality Accident Alarm System (CAAS) has traditionally been installed unless an omission case can be made. An omission case would examine if, in the absence of all controls, a criticality could reasonably be expected or whether the potential dose to an operator would remain below a maximum acceptable dose. It is a UK legal requirement for adequate emergency arrangements to be in place for hazards on a nuclear licensed site. For facilities where criticality is credible there is a regulatory expectation that a -Criticality Warning System- should be in place. A -Criticality Warning System- is not necessarily a full CAAS and alternative means of criticality detection may be part of an adequate emergency plan. The Sellafield site has a Magnox fuel reprocessing facility which has been operated since the 1960's. Evaporation of the Medium Active (MA) liquid waste from this process is undertaken in an associated building. Following extensive review of the plant and process a number of maloperations which can route fissile material to the MA evaporator were identified. Adequate controls to prevent these scenarios were shown to be in place. In the unlikely event of a failure of controls leading to sustained loss of fissile material a criticality incident may occur and hence an emergency plan was determined to be necessary. The novel emergency arrangements which were developed utilized the existing gamma monitor network located across multiple building floors. These gamma monitors are present for radiological safety. This emergency arrangement would require rapid interpretation of the gamma alarms by an operator and the manual triggering of a criticality evacuation alarm. The gamma monitors were demonstrated to be able to detect the minimum incident of concern (10{sup 15} fissions) as well as being able to alarm during the ramp up in power of a large criticality incident (10{sup 18} fissions). It was shown that a criticality accident could readily be distinguished from a radiological event (e.g. loss of containment). To support this work, criticality excursion analysis was used to examine the likely characteristics of a criticality in the MA evaporator. This novel arrangement was justified due to a number of factors including: the limited remaining operational lifetime of this facility (<5 years), the low frequency of maloperation coupled with a failure of controls and the crucial risk reduction provided by the continued reprocessing of Magnox fuel. Furthermore, the time and cost involved with design and installation of a standard CAAS would be substantially greater than a plan based upon existing instrumentation. These arguments were accepted by the UK regulator the Office for Nuclear Regulation (ONR). (author)

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

DOE OSTI2020

Survey of Technologies to Meet PAG limits for Detection of Cesium-137 in Water

The goal of this report is to evaluate the process of adding a sorbent to the sampling process to preconcentrate Cs-137 and then analyze the sorbent to provide a rapid assessment of results to guide decisions on drinking water sources and the protection of the public. Multiple unit design variables were considered: sample configuration/geometry, sorbent efficiency, sample volume. Model simulations demonstrated through these unit design efficiencies that 10 L of sample volume processed through a sorbent provides nearly two orders of magnitude improvement in sample counting time to provide results to a decision maker than the current process. Over 60 publications and reports concerning Cs-137 and sorbents were evaluated. The key attributes were readiness of sorbent to be deployed in a mobile laboratory environment, and minimum sample preparation and conditioning. Examples of sorbents not considered further included nanomaterials, which have not been evaluated at a commercial scale and are limited in availability. The recommended sorbents for further consideration include: ferrocyanide salts, zeolite, and chemically modified granular activated carbon.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗