Molecular beam surface interaction Final report
Momentum transfer and spatial distribution of gas molecules reflected from solid surfaces, for satellite drag calculations
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Application of molecular beams to the study of gas surface interactions at low and moderate energies
Low and moderate energy gas molecule-solid surface interactions using molecular beams
Falcovitz, J.↗
Surface interactions relevant to space station contamination problems
The physical and chemical processes at solid surfaces which can contribute to Space Station contamination problems are reviewed. Suggested areas for experimental studies to provide data to improve contamination modeling efforts are presented.
Dickinson, J. T.↗
Evaluation of lattice sums by the Poisson sum formula
The Poisson sum formula was applied to the problem of summing pairwise interactions between an observer molecule and a semi-infinite regular array of solid state molecules. The transformed sum is often much more rapidly convergent than the original sum, and forms a Fourier series in the solid surface coordinates. The method is applicable to a variety of solid state structures and functional forms of the pairwise potential. As an illustration of the method, the electric field above the (100) face of the CsCl structure is calculated and compared to earlier results obtained by direct summation.
Ray, R. D.↗
Planetary spectroscopy
Infrared spectroscopic studies of the solar system in support of spacecraft investigations were researched. The studies include the physical behavior of comets, the atmospheres of the gaseous planets, and the solid surfaces of satellites and asteroids. Studies of the gaseous and solid emanations of comets using the techniques of CCD spectroscopy and imaging were focused on. An intensive observational effort was mounted, to observe comet Halley with the recently developed state of the art CCD camera system. Comet P/Giacobini-Zinner was observed. The major emphasis was placed on spectroscopy and a synoptic spectrum at least once a month was obtained. A large number of images of Halley for particular emission species and continuum regions were also obtained. The species in vestigated were: C3 (4060 A), CO+ (4505), C2 (5139), NH2 (5980), H2O+ (6185), OI (6300) and CN (9180).
Fink, U.↗
Modeling of Carbon Nanotube Schottky Barrier Reduction for Holes in Air
A model is proposed for the recently observed lower Schottky barrier for holes in air than in vacuum at a metallic electrode - semiconducting carbon nanotube (CNT) junction. In air, the CNT is oxidized. The oxygen molecules on the CNT surface will attract negative charges and will be negatively charged. The negative charges on the solid surface generally enhance the surface dipole and provide stronger electron confinement within the solid. Thus the CNT work function will increase in air. Then the Schottky barrier for holes will have to increase in air according to the standard band-alignment theory, but this is against the experiment. In order to overcome this difficulty, we propose a new Schottky barrier model, assuming that there is a transition region between the electrode and the CNT, where an appreciable potential can drop. We assume that electrodes are placed at the side of the CNT and the contact is formed via the van der Waals interaction. Since the electrode surface is not atomically flat in practical situations, the contact will not be intimate and there will be a transition region before the usual metallic bulk structure starts. In this view, the Schottky barrier is determined not only by the work function difference of the electrodes and the CNT, but also by the potential drop in the transition region. The oxidation increases the potential drop and leads to a lower Schottky barrier for holes. This relation will be demonstrated in a graphical manner by expressing the potential drop as a function of CNT band bending. The potential drop is comparable to the CNT band gap when, e.g., the transition region is about a few Angstroms thick, the oxygen molecule coverage is about 10 %, and an oxygen molecule is charged by about 0.01-0.1 of the unit charge (1-10 % of molecules are charged). The proposed mechanism prevails for both p - and n-CNTs. The model consistently explains the CNT oxidation experiments reported so far.
Yamada, Toshishige↗
High energy scattering of inert gases from well-characterized surfaces. II - Theoretical
Three dimensional model for high energy scattering of inert gas atoms from solid surfaces, calculating trapping, accommodation and flux and velocity distributions
French, J. B.↗
Dye penetrant for surfaces subsequently contacted by liquid oxygen Patent
Dye penetrant and technique for nondestructive tests of solid surfaces contacted by liquid oxygen
Giles, R. M. F.↗
The investigation of flame spreading over the surface of igniting solid propellants Final summary report
Flame spreading over surface of igniting solid propellants in different gas mixtures at various pressures
Magee, R. S.↗
Minor planets and related objects. XVI - Polarimetric diameters
Polarimetric observations of 43 asteroids are presented. All objects show a well-developed negative polarization branch as an indicator of unconsolidated surface regoliths. The empirical slope-albedo law for diffusely reflecting solid surfaces is reexamined and used to compute polarimetric albedos and diameters for 30 asteroids. In many cases the results are in good agreement with infrared-radiometric diameters; the older visual diameter measurements were systematically too small. Radiometric albedos below 5%, however, are not confirmed by the polarimetry. Bimodal frequency distributions are noted for asteroid color, albedo, and the depth of the negative polarization branch. Correlations between B - V color and polarimetric parameters suggest that most of the asteroid population can be divided into silicaceous and carbonaceous opacity classes.
Zellner, B.↗
Investigation to optimize the passive shock wave-boundary layer control for supercritical airfoil drag reduction
The optimization of passive shock wave/boundary layer control for supercritical airfoil drag reduction was investigated in a 3 in. x 15.4 in. Transonic Blowdown Wind Tunnel. A 14% thick supercritical airfoil was tested with 0%, 1.42% and 2.8% porosities at Mach numbers of .70 to .83. The 1.42% case incorporated a linear increase in porosity with the flow direction while the 2.8% case was uniform porosity. The static pressure distributions over the airfoil, the wake impact pressure data for determining the profile drag, and the Schlieren photographs for porous surface airfoils are presented and compared with the results for solid-surface airfoils. While the results show that linear 1.42% porosity actually led to a slight increase in drag it was found that the uniform 2.8% porosity can lead to a drag reduction of 46% at M = .81.
Nagamatsu, H. T.↗
Fundamentals of tribology at the atomic level
Tribology, the science and engineering of solid surfaces in moving contact, is a field that encompasses many disciplines: solid state physics, chemistry, materials science, and mechanical engineering. In spite of the practical importance and maturity of the field, the fundamental understanding of basic phenomena has only recently been attacked. An attempt to define some of these problems and indicate some profitable directions for future research is presented. There are three broad classifications: (1) fluid properties (compression, rheology, additives and particulates); (2) material properties of the solids (deformation, defect formation and energy loss mechanisms); and (3) interfacial properties (adhesion, friction chemical reactions, and boundary films). Research in the categories has traditionally been approached by considering macroscopic material properties. Recent activity has shown that some issues can be approached at the atomic level: the atoms in the materials can be manipulated both experimentally and theoretically, and can produce results related to macroscopic phenomena.
Ferrante, John↗
Adhesion Between Particles And Surfaces In A Vacuum
Report discusses experimental study of adhesion between several kinds of particles and solid surfaces. Purpose of investigation to extend available data on adhesion of contaminant particles and to contribute to understanding of ways in which acceleration redistributes contaminant particles, causing increases or decreases in contamination.
Barengoltz, Jack B.↗
Contact angle determination procedure and detection of an invisible surface film
The contact angle value, i.e., the tangent angle of liquid resting on a planar solid surface, is a basic parameter which can be applied to a wide range of applications. The goal is to provide a basic understanding of the contact angle measurement technique and to present a simple illustration that can be applied as a quality control method; namely, detection of a surface contaminant which exists on a surface that appears clean to the unaided eye. The equipment and experimental procedures are detailed.
Meyer, G.↗
Surface Bacterial-Spore Assay Using Tb3+/DPA Luminescence
Equipment and a method for rapidly assaying solid surfaces for contamination by bacterial spores are undergoing development. The method would yield a total (nonviable plus viable) spore count of a surface within minutes and a viable-spore count in about one hour. In this method, spores would be collected from a surface by use of a transparent polymeric tape coated on one side with a polymeric adhesive that would be permeated with one or more reagent(s) for detection of spores by use of visible luminescence. The sticky side of the tape would be pressed against a surface to be assayed, then the tape with captured spores would be placed in a reader that illuminates the sample with ultraviolet light and counts the green luminescence spots under a microscope to quantify the number of bacterial spores per unit area. The visible luminescence spots seen through the microscope would be counted to determine the concentration of spores on the surface. This method is based on the chemical and physical principles of methods described in several prior NASA Tech Briefs articles, including Live/Dead Spore Assay Using DPA-Triggered Tb Luminescence (NPO-30444), Vol. 27, No. 3 (March 2003), page 7a. To recapitulate: The basic idea is to exploit the observations that (1) dipicolinic acid (DPA) is present naturally only in bacterial spores; and (2) when bound to Tb3+ ions, DPA triggers intense green luminescence of the ions under ultraviolet excitation; (3) DPA can be released from the viable spores by using L-alanine to make them germinate; and (4) by autoclaving, microwaving, or sonicating the sample, one can cause all the spores (non-viable as well as viable) to release their DPA. One candidate material for use as the adhesive in the present method is polydimethysiloxane (PDMS). In one variant of the method for obtaining counts of all (viable and nonviable) spores the PDMS would be doped with TbCl3. After collection of a sample, the spores immobilized on the sticky tape surface would be lysed by heating or microwaving to release their DPA. Tb3+ ions from the TbCl3 would become bound to the released DPA. The tape would then be irradiated with ultraviolet and examined as described above. In another variant of the method - for obtaining counts of viable spores only - the PDMS would be doped with L-alanine in addition to TbCl3. As now envisioned, a fully developed apparatus for implementing this method would include a pulsed source of ultraviolet light and a time-gated electronic camera to record the images seen through the microscope during a prescribed exposure interval at a prescribed short time after an ultraviolet pulse. As in the method of the second-mentioned prior article, the pulsing and time-gating would be used to discriminate between the longer-lived Tb3+/DPA luminescence and the shorter-lived background luminescence in the same wavelength range. In a time-gated image, the bright luminescence from bacterial spores could easily be seen against a dark background.
Ponce, Adrian↗
Optical polarimetry of particulate surfaces
Reflection polarimetry is a remote-sensing tool sensitive to the refractive index and microtexture of solid surfaces. Mechanisms producing linear polarization within a rough, porous, or particulate surface are discussed, and laboratory techniques for precise measurements are described in some detail. Polarimetry of atmosphereless solar-system bodies provides valuable indications of albedo for objects too small and distant for direct diameter determinations, and reveals that even quite small asteroids and satellites have particulate surfaces
Zellner, B.↗
Chemical analysis of metal and polymer surfaces on the front and rear LDEF
The University of Alabama in Huntsville experiment AO114 contained 128 solid surface samples, half of which were exposed on the front and half on the rear of the Long Duration Exposure Facility (LDEF). Each sample is being subject to a battery of analysis methods. In poster form, details of the x-ray photoelectron spectra, Auger electron spectra, Fourier Transform Infrared and ATR infrared spectra, high resolution profilometry, and scanning electron microscope imagery will be presented from a selection of metal and non-metal surfaces.
Christi, L.↗
Experimental Studies of Hydrogenation and Other Reactions on Surfaces Under Astrophysically Relevant Conditions
The goal of our project is to study hydrogen recombination reactions on solid surfaces under conditions that are relevant in astrophysics. Laboratory experiments were conducted using low-flux, cold atomic H and D beams impinging on a sample kept under ultra high vacuum conditions. Realistic analogues of interstellar dust grains were used. Our results show that current models for hydrogen recombination reactions have to be modified to take into account the role of activated diffusion of H on surfaces even at low temperature.
Vidali, Gianfranco↗