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At least 163 records · Page 9

Effect of Solute Elements on Boron Segregation in Boron-Containing Steels

The addition of boron to steel alloys results in an increase in both hardenability and casting defects. The casting difficulties are predicted to stem from a metatectic reaction, δ + γ → L + γ, where a fully solidified material begins to locally remelt as the temperature decreases. Another possible source of casting defects is a boride-rich phase that is predicted to remain liquid at low temperatures. To experimentally determine which reaction is the likely source of the casting defects, the predicted reactions and the effect of solute elements on those reactions are investigated. Levitation zone melting is used to control segregation in a ternary Fe–C–B alloy and a commercial 22MnB5 alloy. Carbon segregation and a peritectic reaction result in a peritectic jump during directional solidification where the first directionally solidified (DS) zone undergoes δ-bcc solidification followed by a peritectic jump to steady state planar solidification of γ-fcc in the second DS zone. The presence of other solute elements in the zone melted 22MnB5 alloy lead to a breakdown in the planar solidification front before steady state solidification could be achieved in the second DS zone. With a cellular solid/liquid interface, boron-rich intercellular liquid formed low melting iron boro-carbide particles. The controlled solidification conditions in a levitation zone melter were unable to prevent ~0.003 wt% boron from segregating to high enough levels to form boride particles. Therefore, it is likely that during commercial casting, the formation of the low melting boride phase from interdendritic segregation is a key source of the casting issues.

36 MATERIALS SCIENCE↗

In-Situ Calibrated Modeling of Residual Stresses Induced in Machining under Various Cooling and Lubricating Environments

Although many functional characteristics, such as fatigue life and damage resistance depend on residual stresses, there are currently no industrially viable ‘Digital Process Twin’ models (DPTs) capable of efficiently and quickly predicting machining-induced stresses. By leveraging advances in ultra-high-speed in-situ experimental characterization of machining and finishing processes under plane strain (orthogonal/2D) conditions, we have developed a set of physics-based semi-analytical models to predict residual stress evolution in light of the extreme gradients of stress, strain and temperature, which are unique to these thermo-mechanical processes. Initial validation trials of this novel paradigm were carried out in Ti-6Al4V and AISI 4340 alloy steel. A variety dry, cryogenically cooled and oil lubricated conditions were evaluated to determine the model’s ability to capture the tribological changes induced due to lubrication and cooling. The preliminarily calibrated and validated model exhibited an average correlation of better than 20% between the predicted stresses and experimental data, with calculation times of less than a second. Based on such fast-acting DPTs, the authors envision future capabilities in pro-active surface engineering of advanced structural components (e.g., turbine blades).

36 MATERIALS SCIENCE↗

The role of creep in high temperature low cycle fatigue.

The significance of the role that creep can play in governing high-temperature, low-cycle fatigue resistance is investigated by conducting strain cycling tests on two high-temperature stainless steel alloys and making concurrent measurements of stress, temperature, and strain at various frequencies. The results are then analyzed in terms of damage imposed by creep and fatigue components. It is shown that creep can play an important and sometimes dominant role in low cycle fatigue at high temperatures. The results of the study include the findings that: (1) the simple life-fraction theory described is adequate for calculating creep damage when the cyclic creep rupture curve is used as a basis for analysis; (2) a method of universal slopes originally developed for room temperature use is sufficiently accurate at high temperature to be used to calculate pure fatigue damage; and (3) a linear creep-fatigue damage rule can explain the transitions observed from one failure mode to another.

Manson, S. S.↗

Materials data handbooks on stainless steels

Two handbooks which summarize latest available data have been published. Two types of stainless steels, alloy A-286 and Type 301, are described. Each handbook is divided into twelve chapters. Scope of information presented includes physical- and mechanical-property data at cryogenic, ambient, and elevated temperatures.

Muraca, R. F.↗

Fracture and crack growth resistance studies of 304 stainless steel weldments relating to retesting of cryogenic vessels

Fracture and crack growth resistance characteristics of 304 stainless steel alloy weldments as relating to retesting of cryogenic vessels were examined. Welding procedures were typical of those used in full scale vessel fabrication. Fracture resistance survey tests were conducted in room temperature air, liquid nitrogen and liquid hydrogen. In air, both surface-flawed and center-cracked panels containing cracks in weld metal, fusion line, heat-affected zone, or parent metal were tested. In liquid nitrogen and liquid hydrogen, tests were conducted using center-cracked panels containing weld centerline cracks. Load-unload, sustained load, and cyclic load tests were performed in air or hydrogen gas, liquid nitrogen, and liquid hydrogen using surface-flawed specimens containing weld centerline cracks. Results were used to evaluate the effectiveness of periodic proof overloads in assuring safe and reliable operation of over-the-road cryogenic dewars.

Hall, L. R.↗

A review of the compatibility of structural materials with oxygen

Consideration of the problem of ignition and combustion of structural materials, particularly metals, which may come in contact with oxygen during its production, transport, and use. Following a review of the historical development of compatibility problems and research, a detailed account is given of compatibility testing methods aimed at detecting probable ignition sources, such as mechanical impact, electric sparks or flashes, heat, sound waves, abrasion, and surface fractures. A summary is presented of the ignition and combustion research reported in the literature, dwelling particularly on papers concerning oxygen-related accidents and the compatibility of metals with high-pressure oxygen. The relative oxygen compatibility of a number of common materials is discussed, including that of nickel and copper alloys, stainless steels, aluminum alloys, and titanium alloys. Finally, an effort is made to pinpoint research areas which would enhance understanding of the compatibility of bulk materials.

Clark, A. F.↗

Stress-corrosion cracking due to hydrazine

Stress corrosion cracking susceptability in presence of hydrazine is examined for 6061-T6, Ti-6A1-4V(STA), Inconel 718, 410 stainless steel, and 4130 steel alloys.

Adamson, M. J.↗

A sharp knife for high temperatures

Electrically heated nickel-chrome-steel alloy knife may be used to cut heat resistant plastic felt and similar materials with relative ease. Blade made of commercially available alloy RA 330 retains edge at temperatures as high as 927 C.

Heisman, R. M.↗

Strainrange partitioning life predictions of the long time metal properties council creep-fatigue tests

The method of strainrange partitioning is used to predict the cyclic lives of the Metal Properties Council's long time creep-fatigue interspersion tests of several steel alloys. Comparisons are made with predictions based upon the time- and cycle-fraction approach. The method of strainrange partitioning is shown to give consistently more accurate predictions of cyclic life than is given by the time- and cycle-fraction approach.

Saltsman, J. F.↗

Strainrange partitioning life predictions of the long time Metal Properties Council creep-fatigue tests

The method of Strainrange Partitioning is used to predict the cyclic lives of the Metal Properties Council's long time creep-fatigue interspersion tests of several steel alloys. Comparisons are made with predictions based upon the Time- and Cycle-Fraction approach. The method of Strainrange Partitioning is shown to give consistently more accurate predictions of cyclic life than is given by the Time- and Cycle-Fraction approach.

Saltsman, J. F.↗

Bellows flow-induced vibrations

Results of theoretical and experimental investigations of bellows typical of those found in space shuttle external tanks are presented. Correlation parameters are identified which generalize the alternating stress calculations cited in an earlier study. Alternating stress amplitudes and mean stress levels form the basis of a fatigue analysis incorporating seven ordinate charts for 347 stainless steel, alloy 21 6-9, and Inco 718. A crack propagation model is included with a program for computing bellows fatigue life. Two phase flow and material hardness properties are discussed.

Johnson, J. E.↗

Signal analysis of voltage noise in welding arcs

Gas tungsten arc welds were made on low alloy steel plates to which intentional defects (discontinuities) were imposed. Disruption of shielding gas, welding over surface films, and tack welds produce changes in what is otherwise a relatively uniform voltage signal. The arc voltage was 15 volts + or - 2 volts with 300 mV ripple noise from the power supply. Changes in this steady noise voltage varied from 50 mV to less than one millivolt depending on the severity and the type of change experienced. In some instances the changes were easily detected by analysis of the signal in real time, while in other cases the signal had to transformed to the frequency domain in order to detect the changes. Discontinuities as small as 1.5 mm in length were detected. The ultimate sensitivity and reproducibility of the technique is still being investigated.

Elis, E.↗

The problem of dimensional instability in airfoil models for cryogenic wind tunnels

The problem of dimensional instability in airfoil models for cryogenic wind tunnels is discussed in terms of the various mechanisms that can be responsible. The interrelationship between metallurgical structure and possible dimensional instability in cryogenic usage is discussed for those steel alloys of most interest for wind tunnel model construction at this time. Other basic mechanisms responsible for setting up residual stress systems are discussed, together with ways in which their magnitude may be reduced by various elevated or low temperature thermal cycles. A standard specimen configuration is proposed for use in experimental investigations into the effects of machining, heat treatment, and other variables that influence the dimensional stability of the materials of interest. A brief classification of various materials in terms of their metallurgical structure and susceptability to dimensional instability is presented.

Wigley, D. A.↗

Influence of deformation behavior, oxydation, and temperature on the long time cyclic stress behavior of high temperature steels

The influence of different parameters on the creep-fatigue behavior of several steel alloys was investigated. The higher the temperature the lower the crack initiation value. Pauses during the cycle reduce the damage. Oxidation reduces and protective gas increases the lifetime. Prior loading and prior deformation reduce the lifetime. Short annealing slightly affects the cycle stress behavior. The test results do not satisfactorily agree with methods of extrapolation and damage accumulation.

Maile, K.↗

LEC System Development

The Lajet Energy Company (LEC) 460 is described. A parabolic dish which incorporates a microprocessor to automatically point it toward the Sun from sunrise to sunset is used. The dish is composed of a set of mirrors (made of reflective polymeric film) which focus and concentrate the Sun's energy on a receiver, producing intense but controlled amounts of heat. The LEC 460 employs a design concept that permits the use of common and low cost materials. All major structural components are fabricated from low carbon, low alloy steel using methods adaptable to mass production. The mirrors are supported on a steel tubing frame. This frame is attached near its center of gravity to a cantilevered support structure. The mirrors and frame are counterbalanced by the weight of the receiver, thus reducing the energy needed to move the collector (parasitic load) and allowing movement on two axes. Each LEC 460 solar concentrator contains a reflective array consisting of twenty four 60 inch diameter mirrors.

Halbert, D. D.↗