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DOE OSTI2020

Supercritical Treatment Technology for Water Purification (Annual Final Report)

This project continued the development of the Supercritical Water Extraction – Enhanced Targeted Recovery (SWEETR™) technology, a novel desalination process for treating hypersaline brines. The overall objective is to demonstrate the technical and economic feasibility of an innovative, energy efficient, and robust supercritical desalination technology to treat hypersaline solutions and separating saltwater into a pure water stream and valuable recovered solids, resulting in zero liquid discharge (ZLD). The proposed technology, focuses on innovative methods of applying supercritical water to treat highly concentrated brine solutions without incurring a high energy penalty. Integrating the technology with solar energy reduces the energy cost for the system. The results obtained during the proof-of-concept testing demonstrate that the SWEETR™ concept is technically feasible and that supercritical water treatment is a viable option with strong merit for treating high salinity waters. The strategic design of the system provides the opportunity to localize the supercritical zone, which helps reduce the overall energy cost associated with the desalination process. The process can be tuned to remove only the amount of salts required to make the treated water “fit for purpose”, providing further opportunities to minimize energy costs. The ability to destroy organic compounds associated with the water while simultaneously being able to desalinate makes SWEETR™ uniquely fitted for treating aqueous streams such as produced water from oil and gas extraction which contain small amounts of organics. Such mixed contaminant streams pose an extreme challenge for other treatment options. Future work will further develop the SWEETR™ technology to take it from the bench-scale to the pilot-scale, and ready the technology for commercial application.

04 OIL SHALES AND TAR SANDS↗

DOE OSTI2021

The Energizer Bunny: Dual-Use Photovoltaic and Pasture-Raised Rabbit Farms (Final Report)

This case study project lays the groundwork for the broader realization of agrivoltaics by considering the techno-economic, environmental, and social aspects of system development and assessing a novel rabbit-based concept. Research on the social and political barriers to agrivoltaic development is sparse, which emphasizes the importance of this project as it provides key insight into the consequential socio-political challenges that may hinder the diffusion of agrivoltaic technology. Additionally, the rabbit agrivoltaic concept is novel and has not been applied in experimental or commercial applications to date. This project advances our understanding of the viability of this co-location scheme through empirical assessment of integrating grazing rabbits with solar. A total of five manuscripts (3 published in peer-reviewed journals, 2 under review) have resulted from this project. The techno-economic component of the project included a) a pilot test study investigating the feasibility of the rabbit agrivoltaic concept and b) an economic analysis of the advantages available to solar operators who leverage grazing animals for lawn maintenance and a dual-revenue stream. Our calculations indicate that the co-location of solar and rabbit farms is a viable form of agrivoltaics, increasing overall site revenue by 2.5%-24.0% above projected electricity revenue. The environmental component of the project entailed an ISO 14040 and 14044 compliant life cycle assessment to quantify the impacts of the rabbit agrivoltaic concept. The results indicate pasture-based agrivoltaic systems provide a dual synergy that produces 69.3% less emissions and demands 82.9% less fossil energy per functional unit of cumulative MWh output of electricity and cumulative kg of meat compared to non-integrated production. The social component of the project included conducting two separate interview studies with agriculture and solar industry professionals and the distribution of a public survey. The interview findings identify the key socio-political opportunities for agrivoltaics include: the retention of agricultural land and rural interests, and increased local level acceptance of solar development. The key barriers to agrivoltaics include: ensuring long term agricultural productivity is not compromised, and subnational zoning strategies. The survey results indicate that support for local solar projects increase by 10% when an agricultural function is incorporated. Survey respondents prefer agrivoltaic projects that are a) designed to provide economic opportunities for farmers and the local community b) located on private property or existing agricultural land, and c) do not threaten local interests. Cumulatively, this project can inform agrivoltaic decision making, solar development practices, rabbit-based applications, land use management, and policy making in a way that supports the furtherance of the renewable energy transition, conserves arable land, and utilizes innovative solar photovoltaic technologies.

14 SOLAR ENERGY↗

DOE OSTI2021

PHOENIX Electrostatic Design

PHOENIX (Portable, High-efficiency, Optimal ENergy Imaging X-rays) is a quasi-DC, electrostatic, vacuum-diode designed as a portable x-ray source with national defense and commercial applications. The patent-pending PHOENIX concept combines a megavoltage, Cockroft-Walton voltage multiplier with a Van de-Graaff electrostatic charge-storage dome to create a vacuum-diode suitable for x-ray production. Naturally this structure must minimize internal electric fields to reduce electrical breakdown while simultaneously reducing size and weight to enhance portability. In this paper we describe the optimization process and model results obtained using the COMSOL multi-physics code. We describe three models: a prototype model built to demonstrate the PHOENIX concept as part of Laboratory Directed Research and Development (LDRD) Mission Foundation Research (MFR) Phase-I , a “back-of-the-envelope” design used as a starting point for further COMSOL optimization, and finally, the optimized geometry implemented in the MFR Phase-II. In all cases compromises resulting from cost, schedule, and manufacturing constraints were taken into account as the design progressed.

42 ENGINEERING↗

DOE OSTI2022

Evaluation of Improvements in Storage Efficiencies, Containment, Assurance, CO 2 Plume Movement, and Verification of Storage Technologies

This report summarizes some of the evolving improvements in key technical skills that are developing to support a large-scale commercial application of CCS as well as support rapidly increasing interest in carbon negative technologies. It does not attempt to review relatively well-known processes and procedures that are familiar to many CCS experts; rather focuses on novel concepts that have the potential to provide breakthroughs and add high benefit as projects evolve. Some elements described are in development or not yet proven ideas for which we provide an expression of status of confidence at the time of writing. Topics covered are evaluation of improvements in storage efficiency estimation, containment assurance methods, CO 2 plume movement and pressure prediction, and monitoring and verification of storage methods.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2023

Bio-Based Phase Change Materials (PCMs) for Thermal Energy Storage (Final Scientific/Technical Report)

The goal of this project is to develop a novel bio-based phase change material (PCM) derived from squid ring teeth (SRT) proteins, and design a prototype heat exchanger based on these bio-based PCMs for energy storage and dynamic heat exchange for building thermal energy storage systems. The PCMs, derived from SRT proteins, will demonstrate room temperature energy storage capacities and switchable thermal conductivities that redefine the current state-of-the-art (SOA) for building thermal energy storage. Further, in a single material and with a single manufacturing processes, our proposed thermal battery will be developed with “on demand” thermal conductivity for rapid charging/discharging but superior insulation during energy storage periods. More specifically, our bio-based PCMs have demonstrated: 1) the potential for increased energy storage capacity (i.e., greater than paraffines at room temperature); 2) tunability in thermal conductivity with the largest thermal conductivity switching ratios for an intrinsic material reported to date, and 3) a 100% recyclable and biodegradable PCM with low volatility and toxicity and scalability in its manufacture for both residential and commercial applications. The already established ability for roll-to-roll processing of these non-toxic, non-flammable SRT composites along with their carbon-neutral manufacturing processes that has been pioneered by our team make this solution a disruptive and impactful technology to redefine the current SOA of energy storage technologies. The outcomes of this effort have been: 1) the identification of new bio-based PCM that establishes a new SOA for thermal conductivity and energy storage density at room temperature and 2) the development of a new experimental technique to measure the energy storage density via latent heat measurements during melting of thin films. This new technique can be applied to thin films (as thin as < 1 micrometer), and represents a novel approach for thin film energy storage density measurements. Dynamic thermal energy storage is the missing technology that will enable a grid- interactive efficient building (GEB). For a “smart” building capable of connecting with the power grid, the media must be inexpensive and possess thermal switching capabilities to control the time-dependent heat flow into (and out of) the PCM on demand. Unique to the material system in this program, programmable SRT-based PCM show improvements as compared to traditionally used PCMs, and thus its technical performance will represent a leap forward for the future GEB concept.

25 ENERGY STORAGE↗

DOE OSTI2023

Grating-Based Imaging-Scattering with Portable Neutron Generator

Company: Adelphi Technology, Inc. Title: Grating-Based Imaging-Scattering with Portable Neutron Generator PI: Dr. Jay Theodore Cremer, Jr. Topic: 26a Statement of the problem or situation that is being addressed. Successful plant growth depends upon an efficient and robust root system. The plant root is part of a larger system of water and microbial flows in the soil system. While much effort has been exerted to develop an imaging system for water, microbes, and roots, the problem is challenging, and no widely accepted imaging method currently exists. The optical solutions use a highly modified soil system. X-ray imaging methods are insensitive to the soft tissues in the presence of sand. Thermal neutron imaging has been often tested, but found inadequate, due to limited access and low image resolution. This project will develop a new strategy for neutron imaging of plant/soil systems. The project will allow long duration experiments in greenhouse environments and increase the image information content to the micron scale. General statement of how this problem is being addressed. Portable, rugged thermal and fast neutron sources are being developed where portable means a two-soldier team can carry the source and power unit to survey rough terrain for explosives. In the past decade, microfabrication of X-ray and thermal/cold neutron optics has opened a new imaging strategy. The standard transmission image is now supplemented with simultaneous acquisition of a phase contrast image and an image revealing scattering features. In materials science, the interferometric neutron scattering image has been used to detect early crack formation in stressed additive manufacturing test samples. The detection requires sensitivity to scattering features at the 1-micron scale. By addition of our proposed grating-optic to Adelphi Technology’s radiographic/tomographic imaging system, which is based on portable thermal neutron source, the resulting thermal neutron scatter image of the plant/soil system, will reveal details at 1-micron. Commercial Applications and Other Benefits Neutron interferometry imaging has greater penetration through large metal components compared to industrial X-ray imaging. The low-cost, large area optics developed for greenhouse applications, combined with the robust, portable neutron generator, can then be marketed as a system for inspection of additive manufactured components. In the aerospace industry, all freshly printed components are validated with X-ray CT. Scheduled maintenance again requires X-ray CT as the ability to predict aerospace component lifetime does not yet exist. Large aerospace components are only partially observed with X-ray imaging. Key Words Neutron radiography/tomography, grating interferometry, thermal neutron generator imaging, plant root and soil imaging, rhizosphere imaging, deployable neutron imaging systems Summary for Members of Congress A rugged, portable source of thermal neutrons is adapted for neutron interferometry imaging with the addition of low-cost, 3D printed optics. The first application of our proposed deployable, compact thermal neutron generator imaging system, using a grating optic, is plant root/soil science in greenhouse settings and agricultural laboratories.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2022

Environmentally Sound One-Step Solar Silicon From Natural Quartzite

This project aimed to demonstrate a new molten salt electrodeposition process to go straight from low-cost silica at $200/tonne ($40¢/kg Si basis) to polysilicon in a single step using less than 30 kWh/kg. This would eliminate the carbothermic reduction step and all direct greenhouse emissions, along with 90% of the energy. It would also eliminate the chemical hazards of chlorosilane handling which have resulted in multiple fatalities in the polysilicon industry – in Japan, the US and China. This project had the following major accomplishments: Stakeholder engagement indicated that the solar silicon market is very sensitive to price, provided quality is sufficient. The most important measure of silicon quality is not purity but carrier lifetime, as many impurities can reduce performance at concentrations too small to measure; Experiments set a baseline of current efficiency which is too low for commercial application (~3%), with electronic current ruled out as a mechanism for reduced current efficiency; A scale-up plant narrative narrative described a potential plant and formed the basis for the TEA components; TEA showed that current efficiency, large cell size, and zirconia membrane lifetime are key factors which determine capital and operating costs for the process.

14 SOLAR ENERGY↗

DOE OSTI2024

Inaugural Symposium of the Institute for Sustainable Energy and Environment, Virginia Commonwealth University

The Inaugural Symposium of the Institute for Sustainable Energy and Environment (ISEE) was held in Virginia Commonwealth University, Richmond, Virginia during April 26 – 28, 2023. The symposium addressed issues and challenges in energy and environment and highlighted the use of clean renewable energy to mitigate the adverse effects of fossil fuels and the greenhouse gases it produces. These issues are complex as the involve educating the public that the climate change is real, it is caused by the use of fossil fuels, it requires scientists and engineers to understand the fundamental science in the production and storage of renewable energy, it requires industries to manufacture and distribute the equipment necessary for commercial application of these technologies, it requires policy makers to put together policies and guidelines to make the transition from fossil fuels to renewable energies efficient, and it requires social scientists and educators to address environmental justice issues and create a workforce to sustain the transition. The symposium considered all the above issues with a diverse list of speakers from the federal and state government, industrial partners, and experts from science and technology to social sciences and public policy. Speakers from the White House Office of Science and Technology Policy, Department of Energy, universities, and non-governmental agencies discussed the challenges and solutions in Plenary as well as Panel sessions. The talks were recorded with permission from the speakers and the panelists and were put in the ISEE website. The participants included students, postdoctoral fellows, and professors from Virginia Commonwealth University and local area Historically Black College and Universities (HBCU) such as Virginia State University and Norfolk State University. The $5000 fund awarded by the Department of Energy were used to support the participation of students, postdoctoral fellows, and faculty from the HBCU institutions. The technical program the list of participants is provided later in the document.

08 HYDROGEN↗

DOE OSTI2024

Preliminary Reactor Fueling Support Equipment Recommendation

The National Reactor Innovation Center (NRIC) is a national program that was established as part of the Nuclear Energy Innovation Capabilities Act (NEICA). NRIC’s mission is to accelerate the demonstration and deployment of advanced nuclear energy through its mission to inspire stakeholders and the public, empower innovators, and deliver successful outcomes through efficient coordination of partners and resources. NRIC is designed to bridge the gap between research, development, and the marketplace to help convert some of the nation’s most promising advanced nuclear reactors into commercial applications.

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

DOE OSTI2024

Domestication of Algae for Increasing Biomass Productivity

Microalgae cultivation processes have been developed for the production of a variety of bioproducts, however currently only a few species are used in commercial applications. Their domestication, that is strain improvements, is still in its infancy, with major advances required, specifically to maximize biomass productivity a limiting factor in microalgae production. This requires a deep understanding of algal biology, in particular to develop superior strains without the need of genetic technologies that would require lengthy regulatory permits, and often limit consumer acceptance. Adaptive Laboratory Evolution techniques, alone or in conjunction with sexual recombination, can allow for rapid develop of improved strains and their industrial production. Light harvesting antenna reduction has been a major approach to achieve increased photon utilization efficiency by cultures operating under full sunlight conditions due to higher light saturation levels, allowing for higher productivities under outdoor conditions. Decades of research yielded some promising results under controlled conditions with a few specific mutant strains. However, these failed to achieve the anticipated higher productivities in actual algal mass cultures, in part due to the inability of single mutations to overcome photoinhibition, reactive oxygen species, and other pleiotropic impacts on the complex metabolic processes of photosynthesis. Higher productivity strains will require multiple genetic improvements. We report on recent Adaptive Laboratory Evolution with the green alga Scenedesmus obliquus resulting in higher biomass productivity in open pond cultivation. Coupling our approach with sexual recombination and genome sequencing provides a path to algal domestication suitable for large-scale, low-cost biomass production.

09 BIOMASS FUELS↗

DOE OSTI2024

Condenser Enclosure Vibration Isolation Mount Selection

A mini split cooling system will be used to maintain temperature requirements in a mobile secure transport system. While the split cooling system was designed to be used in static residential or commercial applications, it was selected for this transportation application due to a unique set of security requirements. However, the system’s ability maintain reliability and survive prolonged long-term shock and vibration is a significant concern. The mitigation strategy is to select vibration isolation mounts and perform lifetime shock and vibration testing to demonstrate survivability. The goal of this study is to generate a finite element model of the system and perform modal analysis to inform selection of vibration mounts to minimize the amount of vibrational energy transferred to the split cooling system. The scope of this report is limited to study of the condensing unit only, and geometric variation of the assembly will not be allowed.

42 ENGINEERING↗

DOE OSTI2023

Energy Transitions Initiative Partnership Project: Alaska Longline Fishermen’s Association Alternative Fuels Review

This report provides information about additional options in electrifying the Alaska Longline Fishermen’s Association (ALFA) fishing fleet. Currently, the Energy Transitions Initiative Partnership Project is prioritizing electric hybrid and battery electric options for retrofit of select fishing vessels in the fleet. However, there are other options for reducing carbon emissions among the fleet, namely hydrogen, ammonia, and biofuels. The use of these alternative fuels may be an option for the fleet in the future as ALFA addresses its vulnerabilities. A literature review of available resources on these fuels was conducted to provide information on several topics associated with implementation of these technologies, including current applications, commercially available power modules, necessary components, infrastructure, and safety codes and standards. An additional aspect that this report investigates is general sizing and refueling schedule based on operating records of multiple ships in the fleet.

29 ENERGY PLANNING, POLICY, AND ECONOMY↗

DOE OSTI2023

Energy Transitions Initiative Partnership Project: Alaska Longline Fishermen’s Association Alternative Fuels Review

29 ENERGY PLANNING, POLICY, AND ECONOMY↗

DOE OSTI2024

Novel ceramic capacitors with ultrahigh energy density and efficiency (Final Technical Report)

Antiferroelectric ceramics are a special class of material that have shown great potential as the dielectric in electrical capacitors due to their high energy- and power-density. During each charge-discharge cycle, the ceramic undergoes transformation to a ferroelectric phase and resumes its antiferroelectric phase. The hysteresis associated with the transitions leads to a mediocre energy efficiency and service lifetime of antiferroelectric capacitors and, hence, their almost absence in commercial products. Under the support of this research project, we first formulated a universal lattice-compatibility theory that included electrostatic polarization energy along with elastic energy and thermal energy to understand the origin of the hysteresis in antiferroelectric oxides. Guided by this compatibility theory, we conducted high-throughput density functional theory (DFT) calculations to assess chemical modifiers and their effect on crystal structures of 400+ PbZrO 3 -based compositions. Down-selected compositions were experimentally validated for their suppressed hysteresis and higher energy efficiency. The verified low-hysteresis compositions were then expanded to an antiferroelectric ceramic library with nearly 500 new compositions (more than 1,500 samples) using high-throughput experiments involving ceramic synthesis and property screening. The large quantity of data generated (theory and experimental) in these tasks were processed by machine-learning techniques and identified trends were fed to the next iteration. In the end, we successfully discovered four compositions with near-zero hysteresis, yielding a world-record energy efficiency of 98.2% at an energy density of 3.0 J/cm 3 . Furthermore, our antiferroelectric ceramic capacitor reaches 79.5 million charge-discharge cycles lifetime, a factor of 80 enhancement over previous antiferroelectric ceramics with large hysteresis. These research accomplishments have not only met the milestones set in the SOPO, but also led to two patent filings, three journal publications (one of them was in Advanced Materials, impact factor 29.4), and nine oral presentations at various venues. Through the course of the project, three postdocs, four Ph.D. students, and one M.S. student were trained. In short, our project established a new methodology in searching next-generation functional ceramics on the fundamental side and discovered several high-efficiency antiferroelectric compositions for capacitors on the applied side. Once fabricated into the multilayer form for commercial applications, these ceramic capacitors can potentially enable the high temperature high power density DC-link capacitors that are critical for the next generation inverters in electric vehicles. The project also significantly contributed to the nation’s workforce development in the STEM fields.

36 MATERIALS SCIENCE↗

DOE OSTI2024

Domesticating the green alga Scenedesmus obliquus

Microalgae cultivation processes exist only for a few species used in commercial applications. Their domestication is still in its infancy, with major advances required, specifically to overcome limiting factors in microalgae production. The goal is to develop superior strains without the need of genetic technologies that would require lengthy regulatory permits, and often limit consumer acceptance. Adaptive Laboratory Evolution techniques, alone or in conjunction with sexual recombination, can allow for rapid develop of improved strains and their industrial production. Approaches include increased photon utilization efficiency by cultures operating under full sunlight conditions due to higher light saturation levels, allowing for higher productivities under outdoor conditions. Decades of research yielded some promising results under controlled conditions with a few specific mutant strains. However, these failed to achieve the anticipated higher productivities in actual algal mass cultures, in part due to the inability of mutations to overcome photoinhibition, reactive oxygen species, and other pleiotropic impacts on photosynthesis.

09 BIOMASS FUELS↗

DOE OSTI2025

Technology Transfer from Fermi Research Alliance to Itasca Plastics for the purpose of Commercializing Scintillator Material

Researchers at the Fermi National Accelerator Laboratory (Fermilab) developed extruded plastic scintillator in the late 1990s, which was first used in the D-Zero experiment. Extruded plastic scintillator is currently produced at Fermilab and is used in particle detectors worldwide. The purpose of this CRADA is to transfer the knowledge related to the Fermilab extrusion process to Itasca Plastics, Inc. (Itasca Plastics). Much of this knowledge is contained in documentation that is in the public domain, although it is distributed over several communications (papers, conference records, etc.) and over several years. Under this CRADA Fermilab will assemble the information, provide it to Itasca Plastics and provide limited consulting to complete the knowledge transfer. If the transfer is successful, Itasca Plastics will be able to establish a U.S. commercial manufacturing capability for extruded scintillator material that can be used for high energy physics and commercial applications.

36 MATERIALS SCIENCE↗

DOE OSTI2025

Updated Natural Gas Pathways in R&D GREET 2024 Rev.1

Natural gas (NG) is a relatively low-cost fossil fuel with vast infrastructure in the United States (U.S.) making it easier to transport and store compared to other fossil fuels such as coal and petroleum. In 2023, the U.S. consumed 32.5 trillion cubic feet or 33.6 Quad Btu of NG, accounting for 36% of the nation’s total primary energy consumption. NG is commonly used for electricity generation, industrial applications, commercial and residential activities and transportation purposes, as shown in Figure 1. This widespread reliance on NG underscores the need to assess its full environmental impact, requiring careful analysis of the entire supply chain from production (i.e., recovery, gathering and boosting [G&B], and processing of raw gas) to final delivery to end users (e.g., via pipelines).

03 NATURAL GAS↗

DOE OSTI2025

Updated Guidance on Sensitivity/Uncertainty Methods Use for Nuclear Criticality Safety Validation

The use of sensitivity/uncertainty (S/U) methods in nuclear criticality safety (NCS) was established more than 25 years ago and has been increasing ever since. Recent interest in commercial applications involving uranium enrichments above 5 wt% 235 U has increased focus on demonstrating the applicability of existing critical experiments to this enrichment range. S/U techniques can also be particularly useful in assessing the similarity of new fuel forms in relation to those documented in existing published evaluations of benchmark critical experiments. Publishing updated recommendations for the use of these methods is thus important to ensure that new S/U practitioners can benefit from the years of development and application invested in generating a set of best practices to maximize the utility of these tools.

NCS↗