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DOE OSTI2023

Cinematic reflectometry using QIKR, the quite intense kinetics reflectometer

The Quite Intense Kinetics Reflectometer (QIKR) will be a general-purpose, horizontal-sample-surface neutron reflectometer. Reflectometers measure the proportion of an incident probe beam reflected from a surface as a function of wavevector (momentum) transfer to infer the distribution and composition of matter near an interface. The unique scattering properties of neutrons make this technique especially useful in the study of soft matter, biomaterials, and materials used in energy storage. Exploiting the increased brilliance of the Spallation Neutron Source Second Target Station, QIKR will collect specular and off-specular reflectivity data faster than the best existing such machines. It will often be possible to collect complete specular reflectivity curves using a single instrument setting, enabling “cinematic” operation, wherein the user turns on the instrument and “films” the sample. Samples in time-dependent environments (e.g., temperature, electrochemical, or undergoing chemical alteration) will be observed in real time, in favorable cases with frame rates as fast as 1 Hz. Cinematic data acquisition promises to make time-dependent measurements routine, with time resolution specified during post-experiment data analysis. This capability will be deployed to observe such processes as in situ polymer diffusion, battery electrode charge–discharge cycles, hysteresis loops, and membrane protein insertion into lipid layers.

47 OTHER INSTRUMENTATION↗

DOE OSTI2020

SENA Hydro Battery Systems Catalog Development

The Hydro Battery catalog development project started in 2017 with the objective of developing a collection of modular engineering design elements, repurposing oil & gas industry techniques and materials, that can be replicated for smaller, lower cost, and faster deploying pumped storage projects in the United States. One notable design element of the catalog involved a floating membrane containment system to achieve closed loop configurations in naturally open body environments. The intent of this particular system is to provide an option to mitigate environmental impacts at sites with technoeconomic merits but aquatics and water quality sensitivities to an alternative open-loop design.

13 HYDRO ENERGY↗

NASA NTRS2004

Flexible electronics for space applications

NASA is currently developing a host of deployable structures for the exploration of space. These include balloons, solar sails, space-borne telescopes and membrane-based synthetic aperture radar.

Crawford, Robert↗

NASA NTRS2018

Testing and Development of NEA Scout Solar Sail Deployer Mechanism

The Near Earth Asteroid (NEA) Scout is a deep space CubeSat designed to use an 86 square meter solar sail to navigate to a near earth asteroid called VG 1991. The solar sail deployment mechanism aboard NEA Scout has gone through numerous design cycles and ground tests since its conception in 2014. An engineering development unit (EDU) was constructed in the spring of 2016 and since then, the NEA Scout team has completed numerous ground deployments aiming to mature the deployment system and the ground test methods used to validate that system. Testing a large, non-rigid gossamer system in 1G environments has presented its difficulties to numerous solar sailing programs before, but NEA Scout’s size, sail configuration, and budget has led the team to develop new deployment techniques and uncover new practices while improving their test methods. NEA Scout’s spooled sail and boom design differs from any solar sail design to date: a single square sail membrane spooled upon a non-circular mandrel and the booms are spooled on two separate coils. This configuration was necessitated by the 6U footprint and is not common among other solar sailing missions. The program has planned and completed 3 separate full scale sail deployments to date, with a flight sail deployment test scheduled for FY18. The sail deployment tests have helped mature flight operations plans and developed preliminary off-nominal deployment mitigation strategies. The paper entitled “Design and Development of NEA Scout Solar Sail Deployer Mechanism” was presented at the 43rd Aerospace Mechanisms Symposium. Since then, the system has matured and completed ascent vent, random vibration, boom deployment and sail deployment tests. This paper will discuss the lessons learned and advancements made while working on solar sail testing and redesign cycles.

Few, Alex↗

NASA NTRSDate not supplied

Design and Testing of the BionicWingSat in a Zero-g Flight Campaign - A 2U-CubeSat with Deployable, Biologically-Inspired Wings

In this paper, recent developments in the design, manufacturing, and testing of a novel deployable structure with several potential applications in space will be described. Through a cooperative effort of the German Aerospace Center (DLR) and the National Aeronautics and Space Administration (NASA), a biologically inspired structurally integrated membrane featuring distributed functional elements has been developed and tested in a 2U CubeSat called BionicWingSat. Such a membrane structure could be useful for several applications in which a relatively flat area is desirable such as solar sails, drag sails, or solar shades. For SmallSats and CubeSats, the design proposed also has the desirable property of being self-deploying without the need for powered deployment mechanisms. Building on previous work inspired by the wings of earwigs, the research presented in this paper includes structural design of self-deploying hinges, a survey of various advanced additive layer manufacturing (ALM) methods for making hinges, mechanical characterization of the hinges, and finite element analysis (FEA) of the hinges. In this work, the conflicting goals of maximizing deployed structural stiffness, maximizing deployed area, maximizing stowed packaging efficiency, and maximizing resistance to creep when stowed must be considered. The resulting design concept is a gossamer structure that cannot support its own weight in gravity. For this reason, a focus in this paper is on a parabolic flight test campaign in which 24 fully integrated wings on two BionicWingSats were tested in a microgravity environment. From this test campaign, several lessons were learned regarding the wing design and procedures for carrying out microgravity tests of this manner.

CubeSat↗

NASA NTRSDate not supplied

Design and Testing of the BionicWingSat in a Zero-g Flight Campaign - A 2U-CubeSat with Deployable, Biologically-Inspired Wings

CubeSat↗

NASA NTRSDate not supplied

The Adaptable, Deployable, Entry and Placement Technology (ADEPT) Enabling Advanced Entry, Descent, and Landing Capabilities for SmallSat Missions

The Adaptable, Deployable Entry and Placement Technology (ADEPT) is a mechanically deployable low-ballistic coefficient aeroshell entry system which performs entry, descent, and landing (EDL) functions for a broad range of planetary destinations including Mars, Venus, Titan and Earth. The deployable system allows mission planners to develop an aeroshell design that is stowed like a folded umbrella, and yet prior to the EDL mission segment, transforms into a deployed, near-rigid low ballistic coefficient configuration. The ADEPT architecture is scalable from a sub-1m class to 6m diameter entry vehicles for Venus and and it has been studied at up to 15m – 20m scale for human exploration class missions. There has been growing interest in performing interplanetary missions with small spacecraft as secondary payloads and ADEPT offers small satellite mission designers the ability to consider Aeroassist technologies to expand mission applications. The ADEPT architecture introduces a new approach for entry vehicle design. It deploys a flexible 3D woven carbon fabric as the primary drag surface. It is capable of surviving high aerothermal heating during entry, while maintaining a robust impermeable membrane that provides high drag for vehicle deceleration. The ADEPT project team has advanced this decelerator technology via systems-level testing at the one meter diameter (nano-ADEPT) scale. A subsonic aeroloads test (May 2015) and a pathfinder arc-jet aeroheating test (Sept 2015) and a successful sounding rocket flight (SR-1) launch of a 0.7 meter deployed diameter ADEPT (September 2018). The SR-1 flight experiment demonstrated most of the primary end-to-end mission stages including: launch in a stowed configuration, separation and deployment in zero-g, exo-atmospheric conditions, and passive ballistic re-entry of a 70 degree half-angle cone geometry. The ADEPT SR-1 sounding rocket flight experiment had to address challenges such as stowing within the constrained payload envelope, fabric folding, and packaging concerns.

Paul Wercinski↗

DOE OSTI2026

Impact of anion-exchange membrane degradation on long-term CO 2 electrolysis to ethylene

Electrochemical CO 2 reduction (eCO2R) to ethylene offers a unique opportunity to diversify domestic supply chains for chemical manufacturing. Large-scale deployment of eCO2R to ethylene reactors is currently limited by low energy efficiencies and poor durability. Herein, we demonstrate >100 h of continuous electrolysis at an industrially relevant current density of 200 mA cm −2 in a 25 cm 2 geometric area zero-gap reactor with a full-cell voltage <3.1 V and ethylene Faradaic efficiency >30%. Incorporating expanded polytetrafluoroethylene (PTFE)-supported electrodes into zero-gap reactors allows for durable electrode catalysts that are resistant to flooding, and this enables wider ranges of operating parameters not typically accessible in CO 2 electrolysis. Finally, we identify membrane degradation, evidenced by a loss of membrane ion-exchange capacity, as the leading cause of performance loss over 144 h of electrolysis.

Energy - Conversion↗

NASA NTRSDate not supplied

Zero-G Experiments of the BionicWingsat - A 2U-Cubesat with Deployable, Biologically-Inspired Wings

In this paper, recent testing of a novel deployable structure with several potential applications in space will be described, with the focus on performed deployment experiments in a DLR Zero-g flight campaign and in ground tests. Through a cooperative effort of the German Aerospace Center (DLR) and the National Aeronautics and Space Administration (NASA), a biologically-inspired structurally-integrated membrane featuring distributed functional elements has been developed and integrated into the 2U CubeSat called BionicWingSat. Such a membrane structure could be useful for all sorts of applications in which a relatively flat area is desirable such as solar sails, drag sails, or solar shades. For SmallSats and CubeSats, the design proposed also has the desirable property of being self-deploying without the need for powered deployment mechanisms. Building on previous work inspired by the wings of earwigs, the research presented in this paper focuses on testing of developed design concepts for such structural systems. To do so 24 fully integrated wings on two BionicWingSats in 2U Cubesat format were experimentally deployed in a microgravity environment during a dedicated DLR Zero-g flight campaign in 2021. The results of these experiments, the built hardware and test articles, the test arrangement, as well as a comparison to ground tests are discussed in this paper.

Spacecraft structures↗

DOE OSTI2024

Maximizing Marine Carbon Removal by Coupling Electrochemical and Biological Methods

Integrated development of emerging marine decarbonization strategies offers the possibility of lowering CO2 removal costs and enabling their widespread deployment. In this study we examine the feasibility and benefits of coupling electrochemical and biological marine carbon removal strategies. Bipolar membrane electrodialysis (BPMED) is used to generate acid and alkalinity from seawater and electricity, and the alkalinity is returned to the ocean for indirect CO2 removal from the atmosphere, but the acid stream is a waste product. Considering the large-scale of CO2 removal necessary, the acid storage, neutralization, and disposal have prohibitive costs and carbon footprint. Here we investigate the feasibility to valorize the acid stream to enhance the growth and CO2 uptake through photosynthesis in the fast-growing marine phytoplankter Picochlorum celeri. When added to active algae cultures, the BPMED-generated acidified seawater alters the carbonate-bicarbonate equilibrium thereby increasing the bioavailability of CO2 and the observed growth rates. Additions of up to 2 mM H+ from BPMED effluent streams increased algal productivity up to 3-fold. A high-level analysis conducted based on experimental data to estimate the potential of sequestered CO2 emissions when compared to conventional commercial means of acid utilization or disposal, is estimated to be ~30 kgCO2 / kgacid. Through further development and optimization in terms of choice of algal species, growth conditions, acid addition rates, etc. the combined electrochemical-biological approach has the potential to achieve higher net CO2 removal.

carbon dioxide, marine, marine algae↗

DOE OSTI2022

Microbial sensor system for monitoring the environment and surfaces

A microbial sensor, system and method that can be used to determine the biochemical conditions of waters, saturated sediments, unsaturated soils, rhizosphere and other environments is disclosed. The flexibility of the microbial sensor design allows for the monitoring of surfaces (skin, ventilation conduits, etc.). An electrochemical microbial sensor system is composed of an indicator electrode(s) and a reference electrode. The reference electrode employs a hydrogen permeable membrane. The electrochemical system is interfaced into a signal/communication module allowing the manual or automated collection of data from field deployments and laboratory investigations. The data is transmitted using various communication technologies including Bluetooth™, cellular, satellite and radio telemetry to cloud-based data management systems. The stored data may be downloaded by users using open-source dashboard and visualization software to image the various environments and/or surfaces investigated.

Burge, Scott R.↗

NASA NTRS2008

NASA Tech Briefs, May 2008

Topics covered inclde: Deployable Wireless Camera Penetrators; Hand-Held Units for Short-Range Wireless Biotelemetry; Wearable Wireless Telemetry System for Implantable BioMEMS Sensors; Electronic Escape Trails for Firefighters; Architecture for a High-to-Medium-Voltage Power Converter; 24-Way Radial Power Combiner/Divider for 31 to 36 GHz; Three-Stage InP Submillimeter-Wave MMIC Amplifier; Fast Electromechanical Switches Based on Carbon Nanotubes; Solid-State High-Temperature Power Cells; Fast Offset Laser Phase-Locking System; Fabricating High-Resolution X-Ray Collimators; Embossed Teflon AF Laminate Membrane Microfluidic Diaphragm Valves; Flipperons for Improved Aerodynamic Performance; System Estimates Radius of Curvature of a Segmented Mirror; Refractory Ceramic Foams for Novel Applications; Self-Deploying Trusses Containing Shape-Memory Polymers; Fuel-Cell Electrolytes Based on Organosilica Hybrid Proton Conductors; Molecules for Fluorescence Detection of Specific Chemicals; Cell-Detection Technique for Automated Patch Clamping; Redesigned Human Metabolic Simulator; Compact, Highly Stable Ion Atomic Clock; LiGa(OTf)(sub 4) as an Electrolyte Salt for Li-Ion Cells; Compact Dielectric-Rod White-Light Delay Lines; Single-Mode WGM Resonators Fabricated by Diamond Turning; Mitigating Photon Jitter in Optical PPM Communication; MACOS Version 3.31; Fiber-Optic Determination of N2, O2, and Fuel Vapor in the Ullage of Liquid-Fuel Tanks; Spiking Neurons for Analysis of Patterns; Symmetric Phase-Only Filtering in Particle-Image Velocimetry; Efficient Coupler for a Bessel Beam Dispersive Element; and Attitude and Translation Control of a Solar Sail Vehicle.

Source record↗

NASA NTRS2003

NASA Tech Briefs, January 2003

Topics covered include: Optoelectronic Tool Adds Scale Marks to Photographic Images; Compact Interconnection Networks Based on Quantum Dots; Laterally Coupled Quantum-Dot Distributed-Feedback Lasers; Bit-Serial Adder Based on Quantum Dots; Stabilized Fiber-Optic Distribution of Reference Frequency; Delay/Doppler-Mapping GPS-Reflection Remote-Sensing System; Ladar System Identifies Obstacles Partly Hidden by Grass; Survivable Failure Data Recorders for Spacecraft; Fiber-Optic Ammonia Sensors; Silicon Membrane Mirrors with Electrostatic Shape Actuators; Nanoscale Hot-Wire Probes for Boundary-Layer Flows; Theodolite with CCD Camera for Safe Measurement of Laser-Beam Pointing; Efficient Coupling of Lasers to Telescopes with Obscuration; Aligning Three Off-Axis Mirrors with Help of a DOE; Calibrating Laser Gas Measurements by Use of Natural CO2; Laser Ranging Simulation Program; Micro-Ball-Lens Optical Switch Driven by SMA Actuator; Evaluation of Charge Storage and Decay in Spacecraft Insulators; Alkaline Capacitors Based on Nitride Nanoparticles; Low-EC-Content Electrolytes for Low-Temperature Li-Ion Cells; Software for a GPS-Reflection Remote-Sensing System; Software for Building Models of 3D Objects via the Internet; "Virtual Cockpit Window" for a Windowless Aerospacecraft; CLARAty Functional-Layer Software; Java Library for Input and Output of Image Data and Metadata; Software for Estimating Costs of Testing Rocket Engines; Energy-Absorbing, Lightweight Wheels; Viscoelastic Vibration Dampers for Turbomachine Blades; Soft Landing of Spacecraft on Energy-Absorbing Self-Deployable Cushions; Pneumatically Actuated Miniature Peristaltic Vacuum Pumps; Miniature Gas-Turbine Power Generator; Pressure-Sensor Assembly Technique; Wafer-Level Membrane-Transfer Process for Fabricating MEMS; A Reactive-Ion Etch for Patterning Piezoelectric Thin Film; Wavelet-Based Real-Time Diagnosis of Complex Systems; Quantum Search in Hilbert Space; Analytic Method for Computing Instrument Pointing Jitter; and Semiselective Optoelectronic Sensors for Monitoring Microbes.

Source record↗

DOE OSTI2025

Engineered Membrane Vesicle Production via oprF or oprI Deletion Has Distinct Phenotypic Effects in Pseudomonas putida

Membrane vesicle (MV) production is a natural phenomenon in Gram-negative bacteria and represents an emerging synthetic biology tool for the secretion of biomolecules or bioproducts. Manipulation of membrane components has proven successful in enhancing MV production. However, the impact of membrane disruptions on strain fitness and protein composition warrants further investigation for the use of MVs in industrial bioprocesses. Here, we identify and characterize two genetic engineering strategies for inducing hypervesiculation-deletion of genes for the outer membrane porin OprF or the lipoprotein OprI-in the commonly used platform Pseudomonas putida KT2440. Deletion of oprI generated up to a 1.5-fold increase in MVs, larger MVs with a greater proportion of outer membrane proteins, and no significant impact on strain fitness compared to wild type. In contrast, deletion of oprF, relative to wild type, generated up to a 4-fold increase in MVs but diminished growth, permeabilized membranes, and increased cytosolic protein packaging. Both hypervesiculation phenotypes increased nontargeted and MV-targeted mNeonGreen extracellular signal by up to 6-fold, demonstrating vesiculation as a mechanism for protein secretion. Despite increased blebbing of MVs from gene deletions, proteins involved in membrane biosynthesis were not elevated relative to wild type. Overexpression of gpsA, which initiates glycerophospholipid biosynthesis, in the ΔoprF background improved the membrane integrity by 37% and maintained MV formation, highlighting the importance of membrane biosynthesis in restoring the membrane in hypervesiculating strains. Together, this study provides genetic engineering strategies with corresponding phenotypic outcomes toward providing a synthetic biology toolset for MV deployment in P. putida.

59 BASIC BIOLOGICAL SCIENCES↗

NASA NTRS1994

Aerodynamic surface distension system for high angle of attack forebody vortex control

A deployable system is introduced for assisting flight control under certain flight conditions, such as at high angles of attack, whereby two inflatable membranes are located on the forebody portion of an aircraft on opposite sides thereof. The members form control surfaces for effecting lateral control forces if one is inflated and longitudinal control forces if both are inflated.

Zell, Peter T.↗

NASA NTRS2000

Analysis and Ground Testing for Validation of the Inflatable Sunshield in Space (ISIS) Experiment

The Next Generation Space Telescope (NGST) design requires a large sunshield to protect the large aperture mirror and instrument module from constant solar exposure at its L2 orbit. The structural dynamics of the sunshield must be modeled in order to predict disturbances to the observatory attitude control system and gauge effects on the line of site jitter. Models of large, non-linear membrane systems are not well understood and have not been successfully demonstrated. To answer questions about sunshield dynamic behavior and demonstrate controlled deployment, the NGST project is flying a Pathfinder experiment, the Inflatable Sunshield in Space (ISIS). This paper discusses in detail the modeling and ground-testing efforts performed at the Goddard Space Flight Center to: validate analytical tools for characterizing the dynamic behavior of the deployed sunshield, qualify the experiment for the Space Shuttle, and verify the functionality of the system. Included in the discussion will be test parameters, test setups, problems encountered, and test results.

Lienard, Sebastien↗

DOE OSTI2025

Manufacturing Cost Analysis for PEM Electrolyzers and Perspectives for Future Cost Reduction

Electrolyzer capital costs strongly influence the total levelized cost of hydrogen production and have implications for hydrogen deployment. Current electrolyzer costs are high, and large cost reductions may be needed to achieve competitive hydrogen costs and targets. Understanding pathways for cost reduction via R&D and deployment is a critical research area for informed energy planning and enabling hydrogen use. This work presents bottom-up cost estimates of polymer electrolyte membrane (PEM) electrolyzer systems tied to design specifications and discusses perspectives for cost reduction opportunities based on ongoing research. We use a detailed manufacturing and process model for a 1 MW PEM electrolyzer stack and balance of plant (BOP) for rigorous cost estimation. This allows for robust estimates of component and manufacturing costs and examination of key cost contributors. Stack costs are dominated by material costs such as iridium and platinum catalysts, especially at high manufacturing rates; power electronics and hydrogen purification equipment are the largest contributors to BOP cost. At higher manufacturing rates, better equipment utilization could reduce stack costs significantly, and we estimate that experience and bulk purchasing will allow for cost reductions to some BOP components. Still, many well-established BOP technologies and stack material costs are less likely to see significant cost reductions at high manufacturing rates. As such, manufacturing scale is limited in how much it can reduce electrolyzer costs, and additional advances for cost reduction may be needed to achieve cost targets. It will likely take many combined strategies to achieve significant cost reductions for electrolyzers and enable low-cost hydrogen production. We can use our manufacturing cost model to quantify potential cost reductions from the considerations described above and demonstrate pathways to lower cost electrolyzers. This allows for better understanding of cost reduction strategies and enables more informed research, development, and deployment for electrolyzers.

cost↗

DOE OSTI2024

Cooperative Atomically Dispersed Fe–N 4 and Sn–N x Moieties for Durable and More Active Oxygen Electroreduction in Fuel Cells

One grand challenge for deploying porous carbons with embedded metal–nitrogen–carbon (M–N–C) moieties as platinum group metal (PGM)-free electrocatalysts in proton-exchange membrane fuel cells is their fast degradation and inferior activity. Here, we report the modulation of the local environment at Fe–N 4 sites via the application of atomic Sn–N x sites for simultaneously improved durability and activity. We discovered that Sn–N x sites not only promote the formation of the more stable D2 FeN 4 C 10 sites but also invoke a unique D3 SnN x –Fe II N 4 site that is characterized by having atomically dispersed bridged Sn–N x and Fe–N 4 . This new D3 site exhibits significantly improved stability against demetalation and several times higher turnover frequency for the oxygen reduction reaction (ORR) due to the shift of the reaction pathway from a single-site associative mechanism to a dual-site dissociative mechanism with the adjacent Sn site facilitating a lower overpotential cleavage of the O–O bond. This mechanism bypasses the formation of the otherwise inevitable intermediate that is responsible for demetalation, where two hydroxyl intermediates bind to one Fe site. Lastly, a mesoporous Fe/Sn-PNC catalyst exhibits a positively shifted ORR half-wave potential and more than 50% lower peroxide formation. This, in combination with the stable D3 site and enriched D2 Fe sites, significantly enhanced the catalyst’s durability as demonstrated in membrane electrode assemblies using complementary accelerated durability testing protocols.

36 MATERIALS SCIENCE↗