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At least 163 records · Page 9

On the efficient calculation of the incomplete Airy function with application to edge diffraction

When the geometrical theory of diffraction (GTD) and its extensions are used to calculate fields across transition regions or in focal areas, various special functions are necessary to create uniform representations. One such transition function is the incomplete Airy function, which is applicable when two reflection points are arbitrarily close to each other and the endpoint of the domain considered. An efficient calculation of the incomplete Airy function is presented and shown to equal known asymptotic expansions when its argument is away from the critical point. By using these expansions, uniform field expressions are found which are consistent with the GTD and maintain its computational efficiency.

Cwik, Tom↗

Advanced High Brilliance X-Ray Source

The possibility to dramatically increase the efficiency of laboratory based protein structure measurements through the use of polycapillary X-ray optics was investigated. This project initiated April 1, 1993 and concluded December 31, 1996 (including a no cost extension from June 31, 1996). This is a final report of the project. The basis for the project is the ability to collect X-rays from divergent electron bombardment laboratory X-ray sources and redirect them into quasiparallel or convergent (focused) beams. For example, a 0.1 radian (approx. 6 deg) portion of a divergent beam collected by a polycapillary collimator and transformed into a quasiparallel beam of 3 millradian (0.2 deg) could give a gain of 6(exp 2)/0.2(exp 2) x T for the intensity of a diffracted beam from a crystal with a 0.2 deg diffraction width. T is the transmission efficiency of the polycapillary diffraction optic, and for T=0.5, the gain would be 36/0.04 x O.5=45. In practice, the effective collection angle will depend on the source spot size, the input focal length of the optic (usually limited by the source spot-to-window distance on the x-ray tube) and the size of the crystal relative to the output diameter of the optic. The transmission efficiency, T, depends on the characteristics (fractional open area, surface roughness, shape and channel diameter) of the polycapillary optic and is typically in the range 0.2-0.4. These effects could substantially reduce the expected efficiency gain. During the course of this study, the possibility to use a weakly focused beam (0.5 deg convergence) was suggested which could give an additional 10-20 X efficiency gain for small samples . Weakly focused beams from double focusing mirrors are frequently used for macromolecular crystallography studies. Furthermore the crystals are typically oscillated by as much as 2 deg during each X-ray exposure in order to increase the reciprocal space (number of crystal planes) sampled and use of a slightly convergent beam could, in principle, provide a similar sampling benefit without oscillation. Although more problematic, because of complications in analyzing the diffraction patterns, it was also suggested that even more extreme beam convergence might be used to give another order of magnitude intensity gain and even smaller focused spot size which could make it possible to study smaller protein crystals than can be studied using standard laboratory based X-ray diffraction systems. This project represents the first systematic investigation of these possibilities. As initially proposed, the contract included requirements for design, purchase, evaluation and delivery of three polycapillary lenses to the Laboratory for Structural Biology at MSFC and demonstration of such optics at MSFC for selected protein crystal diffraction applications.

Gibson, Walter M.↗

A Smart Vision-Aided RICH (Robotic Interface Control and Handling) System for VULCAN

High-flux neutron beams and high-efficiency detectors enable rapid neutron diffraction measurements at the Engineering Materials Diffractometer (VULCAN) at the Spallation Neutron Source (SNS), Oak Ridge National Laboratory (ORNL). To optimize beam time utilization, efficient sample exchange, alignment, and automated measurements are essential. Recent advances in artificial intelligence (AI) have expanded the capabilities of robotic systems. Here, we report the development of a Robotic Interactive Control and Handling (RICH) system for sample handling at VULCAN, designed to support high-throughput experiments and reduce overhead time. The RICH system employs a six-axis desktop robot integrated with AI-based computer vision models capable of recognizing and localizing samples in real time from instrument and depth-resolving cameras. Vision algorithms combine these detections to align samples with designated measurement positions or place them within complex sample environments such as furnaces. This integration of machine learning-assisted vision with robotic handling demonstrates the feasibility of autonomous sample detection and preparation, offering a pathway toward fully unmanned neutron scattering experiments.

automation↗

Super Smooth Optics for Extra-Solar Planet Detection

The goal of imaging planets around the nearby stars has important scientific significance but requires the use of advanced methods of controlling diffracted and scattered light. Over the last three years we have undertaken a study of coronagraphic methods of controlling diffracted light and of figuring hyper-contrast optics. Progress in these two general areas have led to a proposed space-based, 1.9 meter diameter coronagraphic telescope designed specifically for very high performance in the imaging of faint objects near bright sources. This instrument, called the Circumstellar Imaging Telescope (CIT), relies on a new high efficiency coronagraph design and the careful control of scattered light by extremely smooth optics. The high efficiency coronagraph uses focal plane apodization in order to concentrate diffracted light more efficiently in the pupil. This allows convenient removal of the diffracted light by masking off parts of the telescope pupil while not sacrificing the center of the field. Reductions of diffracted light by factors exceeding 1000 are not only possible but are required in order to detect extra-solar planets. Laboratory experiments with this new design have confirmed the theoretical diffraction reductions to the limits of the optics used (factors of about 300) . The extremely high efficiency of this coronagraph puts strong constraints on the narrow angle scattered light due to figure errors in the telescope mirror. Since planets orbiting nearby stars are expected at angular distances of about 1 arcsecond, it is in this small angular range in which scattering must be controlled. The figure errors responsible for scattering in this range come from mid-spatial frequencies corresponding to correlation lengths of about 10 cm on the primary mirror. A primary mirror about 15 times smoother than the Hubble Space Telescope mirror is required for the CIT. Laboratory experiments indicate that small test mirrors can be fabricated with existing technology which come within a factor of two of this requirement.

Terrile, Richard J.↗

High power diode laser Master Oscillator-Power Amplifier (MOPA)

High power multiple quantum well AlGaAs diode laser master oscillator - power amplifier (MOPA) systems were examined both experimentally and theoretically. For two pass operation, it was found that powers in excess of 0.3 W per 100 micrometers of facet length were achievable while maintaining diffraction-limited beam quality. Internal electrical-to-optical conversion efficiencies as high as 25 percent were observed at an internal amplifier gain of 9 dB. Theoretical modeling of multiple quantum well amplifiers was done using appropriate rate equations and a heuristic model of the carrier density dependent gain. The model gave a qualitative agreement with the experimental results. In addition, the model allowed exploration of a wider design space for the amplifiers. The model predicted that internal electrical-to-optical conversion efficiencies in excess of 50 percent should be achievable with careful system design. The model predicted that no global optimum design exists, but gain, efficiency, and optical confinement (coupling efficiency) can be mutually adjusted to meet a specific system requirement. A three quantum well, low optical confinement amplifier was fabricated using molecular beam epitaxial growth. Coherent beam combining of two high power amplifiers injected from a common master oscillator was also examined. Coherent beam combining with an efficiency of 93 percent resulted in a single beam having diffraction-limited characteristics. This beam combining efficiency is a world record result for such a system. Interferometric observations of the output of the amplifier indicated that spatial mode matching was a significant factor in the less than perfect beam combining. Finally, the system issues of arrays of amplifiers in a coherent beam combining system were investigated. Based upon experimentally observed parameters coherent beam combining could result in a megawatt-scale coherent beam with a 10 percent electrical-to-optical conversion efficiency.

Andrews, John R.↗

Time-dependent dynamical Bragg diffraction in deformed crystals by the beam propagation method

Herein, this paper describes how to efficiently solve time-dependent X-ray dynamic diffraction problems in distorted crystals with a fast Fourier transform based beam propagation method. Examples are given of using the technique to simulate the propagation of X-ray beams in deformed crystals in space and time domains relevant to the cavity-based X-ray free-electron lasers and X-ray free-electron laser self-seeding systems.

36 MATERIALS SCIENCE↗

Low-cost iron trichloride cathode for all-solid-state lithium-ion batteries

The dominant chemistries of lithium-ion batteries on the market today still rely on flammable organic liquid electrolytes and cathodes containing scarce metals, such as cobalt or nickel, raising safety, cost and environmental concerns. Here we show a FeCl 3 cathode that costs as little as 1% of the cost of a LiCoO 2 cathode or 2% of a LiFePO 4 cathode. Once coupled with a solid halide electrolyte and a lithium-indium (Li–In) alloy anode, it enables all-solid-state lithium-ion batteries without any liquid components. Notably, FeCl 3 exhibits two flat voltage plateaux between 3.5 and 3.8 V versus Li + /Li, and the solid cell retains 83% of its initial capacity after 1,000 cycles with an average Coulombic efficiency of 99.95%. Combined neutron diffraction and X-ray absorption spectroscopy characterizations reveal a Li-ion (de)intercalation mechanism together with a Fe 2+ /Fe 3+ redox process. Further, our work provides a promising avenue for developing sustainable battery technologies with a favourable balance of performance, cost and safety.

25 ENERGY STORAGE↗

Neutron Positioning and Geometric Distortion Correction on the SNS SiPM Anger Camera

Neutron Anger cameras are scintillator-based thermal neutron detectors that utilize pixelated photosensors to read out visible light signals and position neutrons accurately They are versatile detectors that can cover large areas for diffraction instruments and offer high efficiency and sub-millimeter spatial resolution. Photomultiplier Tube (PMT) based cameras are installed on three instruments at Spallation Neutron Source (SNS). The next generation camera uses Silicon Photomultipliers (SiPMs) instead of PMTs, which allows for a more compact design and higher spatial resolution. In this report, the Gaussian least-squares position fitting method is described in detail, as well as the method used to correct for geometric distortions across the face of the camera. Results from neutron camera tests before and after the distortion correction are shown and the spatial resolution is quantified.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

An aperture-matched compact range feed horn design

The moment method and the uniform geometrical theory of diffraction are used to obtain two separate solutions for the E-plane far field pattern of an aperture-matched horn antenna. This particular horn antenna consists of a standard pyramidal horn with the following modifications: a rolled edge section attached to the aperture edges and a curved throat section. The resulting geometry provides significantly better performance in terms of the pattern, impedance, and frequency characteristics than normally obtainable. The moment method is used to calculate the E-plane pattern and voltage standing-wave ratio (VSWR) of the antenna. However, at higher frequencies, the moment method requires large amounts of computation time. On the other hand, the uniform geometrical theory of diffraction provides a quick and efficient high frequency solution for the E-plane field pattern. This procedure has been successfully applied to design a compact range feed horn.

Heedy, D. J.↗

NASA Tech Briefs, March 2008

Topics covered include: WRATS Integrated Data Acquisition System; Breadboard Signal Processor for Arraying DSN Antennas; Digital Receiver Phase Meter; Split-Block Waveguide Polarization Twist for 220 to 325 GHz; Nano-Multiplication-Region Avalanche Photodiodes and Arrays; Tailored Asymmetry for Enhanced Coupling to WGM Resonators; Disabling CNT Electronic Devices by Use of Electron Beams; Conical Bearingless Motor/Generators; Integrated Force Method for Indeterminate Structures; Carbon-Nanotube-Based Electrodes for Biomedical Applications; Compact Directional Microwave Antenna for Localized Heating; Using Hyperspectral Imagery to Identify Turfgrass Stresses; Shaping Diffraction-Grating Grooves to Optimize Efficiency; Low-Light-Shift Cesium Fountain without Mechanical Shutters; Magnetic Compensation for Second-Order Doppler Shift in LITS; Nanostructures Exploit Hybrid-Polariton Resonances; Microfluidics, Chromatography, and Atomic-Force Microscopy; Model of Image Artifacts from Dust Particles; Pattern-Recognition System for Approaching a Known Target; Orchestrator Telemetry Processing Pipeline; Scheme for Quantum Computing Immune to Decoherence; Spin-Stabilized Microsatellites with Solar Concentrators; Phase Calibration of Antenna Arrays Aimed at Spacecraft; Ring Bus Architecture for a Solid-State Recorder; and Image Compression Algorithm Altered to Improve Stereo Ranging.

Source record↗

Preliminary LISA Telescope Spacer Design

The Laser Interferometric Space Antenna (LISA) mission observes gravitational waves by measuring the separations between freely floating proof masses located 5 million kilometers apart with an accuracy of approximately 10 picometers. The separations are measured interferometrically. The telescope is an afocal Cassegrain style design with a magnification of 80x. The entrance pupil has a 40 cm diameter and will either be centered on-axis or de-centered off-axis to avoid obscurations. Its two main purposes are to transform the small diameter beam used on the optical bench to a diffraction limited collimated beam to efficiently transfer the metrology laser between spacecraft, and to receive the incoming light from the far spacecraft. It transmits and receives simultaneously. The basic optical design and requirements are well understood for a conventional telescope design for imaging applications, but the LISA design is complicated by the additional requirement that the total optical path through the telescope must remain stable at the picometer level over the measurement band during the mission to meet the measurement accuracy. This poster describes the requirements for the telescope and the preliminary work that has been done to understand the materials and mechanical issues associated with the design of a passive metering structure to support the telescope and to maintain the spacing between the primary and secondary mirrors in the LISA on-orbit environment. This includes the requirements flowdown from the science goals, thermal modeling of the spacecraft and telescope to determine the expected temperature distribution,layout options for the telescope including an on- and off-axis design, and plans for fabrication and testing.

Livas, J.↗

LISA Telescope Spacer Design Issues

The LISA mission observes gravitational waves by measuring the separations between freely floating proof masses located 5 million kilometers apart with an accuracy of - 10 picometers. The separations are measured interferometrically. The telescope is an afocal Cassegrain style design with a magnification of 80x. The entrance pupil has a 40 cm diameter and will either be centered on-axis or de-centered off-axis to avoid obscurations. Its two main purposes are to transform the small diameter beam used on the optical bench to a diffraction limited collimated beam to efficiently transfer the metrology laser between spacecraft, and to receive the incoming light from the far spacecraft. It transmits and receives simultaneously. The basic optical design and requirements are well understood for a conventional telescope design for imaging applications, but the LISA design is complicated by the additional requirement that the total optical path through the telescope must remain stable at the picometer level over the measurement band during the mission to meet the measurement accuracy. We describe the mechanical requirements for the telescope and the preliminary work that has been done to understand the materials and mechanical issues associated with the design of a passive metering structure to support the telescope and to maintain the spacing between the primary and secondary mirrors in the LISA on-orbit environment. This includes the requirements flowdown from the science goals, thermal modeling of the spacecraft and telescope to determine the expected temperature distribution, layout options for the telescope including an on- and off-axis design. Plans for fabrication and testing will be outlined.

Livas, Jeff↗

Modelling Sonic Boom Propagation through Planetary Boundary Layer Turbulence near the Lateral Extent of the Carpet

Nonlinear acoustic propagation of sonic booms in the atmospheric boundary layer is considered in the context of a one-way solution to a third order wave equation. A split-step approach is utilized to compute different physical effects efficiently. Unlike previous approaches, the diffraction effects are computed exactly in the forward direction with no restriction on the angle of propagation. This results in more accurate modelling of sonic boom near the carpet edge. Heterogenous flow effects are incorporated with a wide-angle parabolic approximation. Nonlinear propagation is computed with a Burgers-Hayes method. Turbulence in the medium is constructed by the method of random Fourier modes. The turbulence spectra are constructed using an altitude dependent 3-dimensional von Karman spectrum. The turbulence field is considered frozen, as the eddy turnover time in the atmospheric boundary layer is generally much larger than the propagation time of the acoustic wave. Comparisons with benchmark predictions from the PCBoom software are conducted. The benchmark cases provide insight into the accuracy of the current prediction code for non-turbulent atmospheres. Future work is discussed regarding the prediction of shaped booms, boundary conditions, and predictions near the lateral extent of the boom carpet where previous approaches fail to capture the diffraction effects.

sonic boom↗

An Improved Solution for Integrated Array Optics in Quasi-Optical mm and Submm Receivers: the Hybrid Antenna

The hybrid antenna discussed here is defined as a dielectric lens-antenna as a special case of an extended hemi-spherical dielectric lens that is operated in the diffraction limited regime. It is a modified version of the planar antenna on a lens scheme developed by Rutledge. The dielectric lens-antenna is fed by a planar-structure antenna, which is mounted on the flat side of the dielectric lens-antenna using it as a substrate, and the combination is termed a hybrid antenna. Beam pattern and aperture efficiency measurements were made at millimeter and submillimeter wavelengths as a function of extension of the hemi- spherical lens and different lens sizes. An optimum extension distance is found experimentally and numerically for which excellent beam patterns and simultaneously high aperture efficiencies can be achieved. At 115 GHz the aperture efficiency was measured to be (76 4 +/- 6) % for a diffraction limited beam with sidelobes below -17 dB. Results of a single hybrid antenna with an integrated Superconductor-Insulator-Superconductor (SIS) detector and a broad-band matching structure at submillimeter wavelengths are presented. The hybrid antenna is diffraction limited, space efficient in an array due to its high aperture efficiency, and is easily mass produced, thus being well suited for focal plane heterodyne receiver arrays.

Buttgenbach, Thomas H.↗

Heterogeneous reaction of ozone with aluminum oxide

Rates and collision efficiencies for ozone decomposition on aluminum oxide surfaces were determined. Samples were characterized by BET surface area, X-ray diffraction, particle size, and chemical analysis. Collision efficiencies were found to be between 2 times 10 to the -10 power and 2 times 10 to the -9 power. This is many orders of magnitude below the value of 0.000001 to 0.00001 needed for appreciable long-term ozone loss in the stratosphere. An activation energy of 7.2 kcal/mole was found for the heterogeneous reaction between -40 C and 40 C. Effects of pore diffusion, outgassing and treatment of the aluminum oxide with several chemical species were also investigated.

Keyser, L. F.↗

Stratified Volume Diffractive Optical Elements as Low-Mass Coherent Lidar Scanners

Transmissive scanning elements for coherent laser radar systems are typically optical wedges, or prisms, which deflect the lidar beam at a specified angle and are then rotated about the instrument optical axis to produce a scan pattern. The wedge is placed in the lidar optical system subsequent to a beam-expanding telescope, implying that it has the largest diameter of any element in the system. The combination of the wedge diameter and asymmetric profile result in the element having very large mass and, consequently, relatively large power consumption required for scanning. These two parameters, mass and power consumption, are among the instrument requirements which need to be minimized when designing a lidar for a space-borne platform. Reducing the scanner contributions in these areas will have a significant effect on the overall instrument specifications, Replacing the optical wedge with a diffraction grating on the surface of a thin substrate is a straight forward approach with potential to reduce the mass of the scanning element significantly. For example, the optical wedge that will be used for the SPAce Readiness Coherent Lidar Experiment (SPARCLE) is approximately 25 cm in diameter and is made from silicon with a wedge angle designed for 30 degree deflection of a beam operating at approx. 2 micrometer wavelength. The mass of this element could be reduced by a factor of four by instead using a fused silica substrate, 1 cm thick, with a grating fabricated on one of the surfaces. For a grating to deflect a beam with a 2 micrometer wavelength by 30 degrees, a period of approximately 4 micrometers is required. This is small enough that fabrication of appropriate high efficiency blazed or multi-phase level diffractive optical gratings is prohibitively difficult. Moreover, bulk or stratified volume holographic approaches appear impractical due to materials limitations at 2 micrometers and the need to maintain adequate wavefront quality. In order to avoid the difficulties encountered in these approaches, we have developed a new type of high-efficiency grating which we call a Stratified Volume Diffractive Optical Element (SVDOE). The features of the gratings in this approach can be easily fabricated using standard photolithography and etching techniques and the materials used in the grating can be chosen specifically for a given application, In this paper we will briefly discuss the SVDOE technique and will present an example design of a lidar scanner using this approach. We will also discuss performance predictions for the example design.

Chambers, Diana M.↗

High-Efficiency Flexible Multilevel Photon Sieves by Single-Step Laser-Based Fabrication and Optical Analysis

Over the past several decades, the need for high-resolution, high-efficiency, lightweight, high contrast focusing optics has continued to increase due to their applications in fields such as astronomy, spectroscopy, free-space optical communications, defense, and remote sensing. In recent years, photon sieve planar diffractive optics have been developed on flexible, lightweight polyimide substrates. However, transmission efficiencies have continuously been very low (~1-4%), thus impeding the widespread use of photon sieves in practical applications. Here, we present a flexible, lightweight, N = 4 level phase photon sieve with over 25% transmission efficiency; nearly triple that of any other photon sieve reported thus far. In this study, the photon sieve was fabricated via a novel pulsed laser ablation method using an ultraviolet source, and the total time to fabricate a ~3 sq cm sample was tens of seconds. Theoretical analysis of the photon sieve was carried out via the FDTD method, and was in very good agreement with experimental results. We also calculated via FDTD modeling the behavior of higher step (N = 8, 16, 32) photon sieves for further enhanced efficiencies, and show a fundamental limit on photon sieve efficiency of 70% in the limit of increasing step number. This multilevel photon sieve represents a new step in high-resolution diffractive optics, moving towards efficiencies suitable for widespread applications.

Julian, Matthew N.↗

Robust COTS objective for diffraction-limited, high-NA, long front working distance imaging

We present a robust objective lens optimized for applications requiring both high numerical aperture (NA) and long front working distance imaging, comprised of all commercial-off-the-shelf (COTS) spherical singlet lenses. Unlike traditional designs that require separate collimation and refocusing stages, our approach directly converges imaged light to the back focal plane using a single lens group. Our configuration corrects spherical aberrations and efficiently collects light to achieve diffraction-limited performance across a wide range of wavelengths while simplifying alignment and assembly. Using this approach, we design and construct an example objective lens that features a long front working distance of 61 mm and a clipped NA of 0.30 (limited by an aperture in our experimental setup). We experimentally verify that it achieves monochromatic diffraction-limited resolution at wavelengths from 375 nm to 866 nm without requiring replacement of the lenses or changing the inter-lens spacings, and its performance remains robust across a 46 mm range variation in total length (by adjusting mainly the back working distance). Additionally, we develop a quantitative method to measure the field of view (FOV) using an experimentally calibrated pinhole target. Under 397 nm illumination (i.e., from 40 Ca + ion fluorescence), the objective achieves a resolution of 0.87 μm with a 540 μm FOV. This robust, all-COTS, and versatile design is well-suited for a broad range of experiments, supporting high-precision measurements and exploring quantum phenomena.

Cui, Jiafeng [Oak Ridge National Laboratory (ORNL)↗