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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 163 records · Page 9

Isolation and characterization of microalgae strains able to grow on complex biomass hydrolysate for industrial application

Producing algae biomass economically remains one of the chief bottlenecks for commercializing algae products. The aim of this work is to identify new strains of algae that can grow on cost effective media derived from cellulosic waste streams, characterize the potential of these strains to produce compounds of high industrial value, and identify those strains capable of facile genetic transformation. Here we report, out of 45 strains initially isolated, three were selected based on their ability to efficiently grow on organic waste material (corn stover hydrolysate) as a carbon source; Chlorococcum sp., Desmodesmus sp., and Chlamydomonas debaryana. Untargeted metabolomics was performed on each strain, identifying several metabolites of high relative abundances that are of commercial interest, such as lactic acid, butane-2,3-diol, amino acids, tartaric acid, triacylglycerols, and lipid species containing different, mono- and polyunsaturated fatty acids, depending on the strain and growth condition. The strains also produced carbohydrates of industrial relevance. Chlorococcum sp. was found to be genetically transformable using standard simple transformation protocols. These results suggest that with further development, these strains could open the door to economic production of high value commercial compounds utilizing waste streams from cellulosic biomass.

09 BIOMASS FUELS↗

Utah FORGE: 16B(78)-32 RFS DSS Strain Change Rate vs. Depth During 16A(78)-32 Stimulation

This dataset contains strain change rate versus depth data acquired using a Rayleigh frequency shift (RFS) distributed strain sensing (DSS) system during hydraulic stimulation of well 16A(78)-32 at the Utah FORGE site in April 2024. The data were collected from an optical fiber installed in the annulus of production well 16B(78)-32, approximately 300 feet from the injection well. The dataset includes tabulated strain data and an explanation of the methodology used to generate the frac log, which integrates strain change rate signals over selected time windows to identify fracture events.

15 GEOTHERMAL ENERGY↗

Selection of experimental modal data sets for damage detection via model update

When using a finite element model update algorithm for detecting damage in structures, it is important that the experimental modal data sets used in the update be selected in a coherent manner. In the case of a structure with extremely localized modal behavior, it is necessary to use both low and high frequency modes, but many of the modes in between may be excluded. In this paper, we examine two different mode selection strategies based on modal strain energy, and compare their success to the choice of an equal number of modes based merely on lowest frequency. Additionally, some parameters are introduced to enable a quantitative assessment of the success of our damage detection algorithm when using the various set selection criteria.

Doebling, S. W.↗

Highly efficient semi-hydrogenation in strained ultrathin PdCu shell and the atomic deciphering for the unlocking of activity-selectivity

Excellent ethylene selectivity in acetylene semi-hydrogenation is often obtained at the expense of activity. To break the activity-selectivity trade-off, precise control and in-depth understanding of the three-dimensional atomic structure of surfacial active sites are crucial. Here, we designed a novel Au@PdCu core–shell nanocatalyst featuring diluted and stretched Pd sites on the ultrathin shell (1.6 nm), which showed excellent reactivity and selectivity, with 100% acetylene conversion and 92.4% ethylene selectivity at 122 °C, and the corresponding activity was 3.3 times higher than that of the PdCu alloy. The atomic three-dimensional decoding for the activity-selectivity balance was revealed by combining pair distribution function (PDF) and reverse Monte Carlo simulation (RMC). The results demonstrate that a large number of active sites with a low coordination number of Pd–Pd pairs and an average 3.25% tensile strain are distributed on the surface of the nanocatalyst, which perform a pivotal function in the simultaneous improvement of hydrogenation activity and ethylene selectivity. Our work not only develops a novel strategy for unlocking the linear scaling relation in heterogeneous catalysis but also provides a paradigm for atomic 3D understanding of lattice strain in core–shell nanocatalysts.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

MHOST: An efficient finite element program for inelastic analysis of solids and structures

An efficient finite element program for 3-D inelastic analysis of gas turbine hot section components was constructed and validated. A novel mixed iterative solution strategy is derived from the augmented Hu-Washizu variational principle in order to nodally interpolate coordinates, displacements, deformation, strains, stresses and material properties. A series of increasingly sophisticated material models incorporated in MHOST include elasticity, secant plasticity, infinitesimal and finite deformation plasticity, creep and unified viscoplastic constitutive model proposed by Walker. A library of high performance elements is built into this computer program utilizing the concepts of selective reduced integrations and independent strain interpolations. A family of efficient solution algorithms is implemented in MHOST for linear and nonlinear equation solution including the classical Newton-Raphson, modified, quasi and secant Newton methods with optional line search and the conjugate gradient method.

Nakazawa, S.↗

Influence of defect characteristics on tensile deformation of an additively manufactured stainless steel: Evolutions of texture and intergranular strain

The micromechanics of plastic deformation behavior of a selective laser melt processed austenitic stainless steel were studied by investigating the evolutions of texture and intergranular strain using in situ high-energy synchrotron x-ray diffraction (sXRD). The effects of defect characteristics on tensile behavior were studied using three different samples: a near full-density sample with elliptical closed voids and two samples with lack-of-fusion (LOF) defects tensile loaded either perpendicular or parallel to their major axes. The evolutions of pole figures and inverse pole figures show that the full-density specimen develops a strong (111)/(200) fiber texture along the loading direction. For both LOF specimens, the evolution of texture is qualitatively similar to the full-density counterpart, but the development of the fiber texture was much slower, indicating a limited plasticity at a given macroscopic strain. The intergranular strain evolution in the full-density specimen is similar to that of a wrought 316L stainless steel. Conversely, a significantly different intergranular strain development was observed in a LOF specimen, where tensile strain development was observed in both the axial and transverse directions. Finally, the influence of defect type, density, and orientation on the local stress states in the steel matrix and the evolutions of intergranular strains is discussed.

36 MATERIALS SCIENCE↗

Use of photostress to analyze behavior of an aft skirt test specimen

Strains at twenty-one selected points in the critical lower weld region of a aft skirt of a solid rocket booster of the shuttle were measured using photoelastic coatings and stress separator gages. Data were taken at loads of 5, 14, 20, 28, 42, 56, and 70 percent of the design limit load. Results indicate that general yielding occurred in the weld metal and for a short distance outside the fusion boundaries on either side of the weld metal. The fusion boundaries did not yield at the 70 percent load. Slight non-linearity in the load strain curves were observed at several points above the 20 percent load level. Maximum measured strains occurred at points in the forged metal of the holddown post along a line 0.50 inches from the centerline of the weld. Maximum shearing strains within the area covered by the photoelastic coating occurred at points approximately 0.33 inches to the right of the weld centerline near points 6 and 7 and lying along a yellow vertical line extending from just below point 6 to point 11. Photoelastic coatings were shown to be an excellent method to provide the whole field strain distribution in the region of the critical weld and to enhance the overall understanding of the behavior of the welded joint.

Gambrell, S. C., Jr.↗

Ground/Flight Correlation of Aerodynamic Loads with Structural Response

United States Air Force Research Laboratory (AFRL) ground tests at the NASA Transonic Dynamics Tunnel (TDT) and NASA flight tests provide a basis and methodology for in-flight characterization of the aeroelastic performance through the monitoring of the fluid-structure interaction using surface flow sensors. NASA NF-15B flight tests provided a unique opportunity to test the correlation of aerodynamic loads with sectional flow attachment/detachment points, also known as flow bifurcation points (FBPs), as observed in previous wind tunnel tests. The NF-15B tail was instrumented with hot-film sensors and strain gages for measuring root-bending strains. These data were gathered via selected sideslip maneuvers performed at level flight and subsonic speeds. The aerodynamic loads generated by the sideslip maneuver resulted in root-bending strains and hot-film sensor signals near the stagnation region that were highly correlated. For the TDT tests, a flexible wing section developed under the AFRL SensorCraft program was instrumented with strain gages, accelerometers, and hot-film sensors at multiple span stations. The TDT tests provided data showing a gradual phase change between the FBP and the structural mode occurred during a resonant condition as the wings structural modes were excited by the tunnel-generated gusts.

Mangalam, Arun S.↗

Interlaminar fracture toughness: Three-dimensional finite element modeling for end-notch and mixed-mode flexure

A computational procedure is described for evaluating End-Notch-Flexure (ENF) and Mixed-Mode-Flexure (MMF) interlaminar fracture toughness in unidirectional fiber composites. The procedure consists of a three-dimensional finite element analysis in conjunction with the strain energy release rate concept and with composite micromechanics. The procedure is used to analyze select cases of ENF and MMF. The strain energy release rate predicted by this procedure is in good agreement with limited experimental data. The procedure is used to identify significant parameters associated with interlaminar fracture toughness. It is also used to determine the critical strain energy release rate and its attendant crack length in ENF and/or MMF. This computational procedure has considerable versatility/generality and provides extensive information about interlaminar fracture toughness in fiber composites.

Murthy, P. L. N.↗

DISCOVR: Development of Integrated Screening, Cultivar Optimization, and Verification Research

The DISCOVR consortium has developed and is applying an integrated platform and workflow for standardized, deep characterization of highly productive and resilient microalgae strains. New strains are screened using three consecutive tiers in a conceptual down-selection funnel to arrive at the most promising strains. At tier I, strains are screened on gradient incubators to determine their temperature and salinity tolerance range, and to evaluate their resistance to infectious agents (e.g., chytrids). At tier II, the strains’ winter and summer season biomass productivities are quantified in Laboratory Environmental Algae Pond Simulator (LEAPS) photobioreactors, and biomass composition is determined under N-replete and N-deplete conditions. At tier III, the best winter and summer season strains are evaluated in indoor crash ponds to determine their resilience to induced infections, and strains are tested in outdoor raceway ponds to confirm high biomass productivity and culture stability. The top strains are then evaluated in seasonal SOT outdoor pond culture trials at AzCATI, the dedicated Department of Energy SOT (State of Technology) testbed. Additional research is carried out on evaluating growth promoting molecules, reducing the impact of oxygen inhibition, optimizing pond operational conditions, measuring compositional shift dynamics, developing integrated pest management strategies, analysing culture health using 96 well-plate tools, implementing spectroradiometric monitoring and using machine learning to predict culture crashes.

Huesemann, Michael H↗

Finite element mesh refinement criteria for stress analysis

This paper discusses procedures for finite-element mesh selection and refinement. The objective is to improve accuracy. The procedures are based on (1) the minimization of the stiffness matrix race (optimizing node location); (2) the use of h-version refinement (rezoning, element size reduction, and increasing the number of elements); and (3) the use of p-version refinement (increasing the order of polynomial approximation of the elements). A step-by-step procedure of mesh selection, improvement, and refinement is presented. The criteria for 'goodness' of a mesh are based on strain energy, displacement, and stress values at selected critical points of a structure. An analysis of an aircraft lug problem is presented as an example.

Kittur, Madan G.↗

Effect of Applied Stress on the Selective Oxidation of Alloy 600 Exposed to PWR Primary Water and Rhines Pack Environments

A mechanistic understanding of corrosion and oxidation processes is crucial to ensure long-term resistance to stress corrosion cracking of Ni-base structural alloys in pressurized water reactor (PWR) primary and secondary systems. Aqueous corrosion of Ni-base alloys under PWR primary water conditions was previously compared to gaseous oxidation with comparable oxygen potentials. However, those studies considered only stress-free conditions, which removes a critical parameter for understanding stress corrosion behaviors. A significant knowledge gap exists for the role of applied stresses on selective internal oxidation in gaseous environments. A micro-4-point-bend jig was designed to facilitate stress in a Rhines Pack set-up. Selective oxidation at different stress and strain conditions was investigated in a series of Rhines Pack experiments for Alloy 600. Focused ion beam milling enabled the extraction of site-specific specimens containing selected high-energy grain boundaries from tensile and compressive stress regions. Analytical transmission electron microscopy was employed to analyze the microstructure and chemical composition of the resulting oxides. Protective surface oxide films and selective intergranular oxides were observed at different conditions. The implications of these fundamental differences are discussed relative to intergranular attack and stress corrosion cracking mechanisms in PWR primary water.

stress, 4-point-bend, selective oxidation, Alloy 6↗

NASA LaRC Strain Gage Balance Design Concepts

The NASA Langley Research Center (LaRC) has been designing strain-gage balances for more than fifty years. These balances have been utilized in Langley's wind tunnels, which span over a wide variety of aerodynamic test regimes, as well as other ground based test facilities and in space flight applications. As a result, the designs encompass a large array of sizes, loads, and environmental effects. Currently Langley has more than 300 balances available for its researchers. This paper will focus on the design concepts for internal sting mounted strain-gage balances. However, these techniques can be applied to all force measurement design applications. Strain-gage balance concepts that have been developed over the years including material selection, sting, model interfaces, measuring, sections, fabrication, strain-gaging and calibration will be discussed.

Rhew, Ray D.↗

Quasi-static and dynamic response of a Cu/Nb composite following equal channel angular extrusion

The article presents a study of the plastic properties of a Cu–18%Nb composite following equal channel angular extrusion under both low- and high-strain rate loadings. The microstructures are characterized by optical and scanning electron microscopy as well as electron backscatter diffraction. Comparisons are also made with a Cu–50%Nb laminate made by accumulative roll bonding. Textures obtained within the respective phases in the extruded composite closely mimic those previously reported for the pure components alone (Cu, Nb). Grain sizes of the major phase (Cu) exhibit broad distributions, due largely to partial recrystallization during the extrusion process. Further re-crystallization is obtained within localized deformation bands produced at high strain rates (3 × 10 3 s –1 ). While the degree of anisotropy and the strain rate sensitivity of the composite response are similar to those of pure Cu after extrusion, the strength levels of the composite are somewhat greater, falling broadly between those obtained in the pure components after extrusion to comparable plastic strains. Furthermore, the implications for selection of composite composition and processing for achieving higher strengths are briefly discussed.

36 MATERIALS SCIENCE↗

Environmentally Assisted Fatigue in Light Water Reactor Environment

This report summarizes the Environmentally Assisted Fatigue (EAF) research conducted at ANL under the US DOE Light Water Reactor Sustainability (LWRS) program. Starting from a rich background in theoretical and experimental EAF, ANL previously developed an approach to evaluate fatigue performance of reactor materials in light water reactor environments with the correction factor F en . The approach was based on a large body of experimental work performed at ANL and elsewhere, and was consistent with American Society of Mechanical Engineers (ASME)’s methodology governing the design and construction of reactor components. In recent years, the program was focused on component fatigue prediction and made several major and fundamental contributions in this area. These accomplishments help meet the needs identified by the industry concerning component level fatigue predictions in complex, transient conditions. The main contribution of the ANL program involved the development of a system-level model for estimating residual strain and life of nuclear reactor coolant system components under connected-system-thermal-mechanical boundary conditions. The goal was to predict the stress hotspots, strain residuals, strain amplitudes and the resulting fatigue lives. Thermal-mechanical stress analysis was performed considering thermal stratification and a design-basis reactor loading cycle. Based on the finite element (FE) model results, the strain residuals, strain amplitudes and resulting fatigue lives of reactor coolant system (RCS) components were predicted. The results show that some of the RCS components can have significantly different strain amplitudes, residual strain, and fatigue lives, despite having similar geometry and material. In addition, the simulated component-level strain profile can guide the selection of appropriate test inputs for conducting laboratory-scale EAF tests. Building upon the system-level model, ANL developed a digital twin (DT) framework to predict the structural states and associated fatigue life of components in real-time. This framework is a comprehensive system designed to predict the structural states and fatigue lives of reactor components. It includes multiple models and integrates artificial intelligence (AI), machine learning (ML), and FE based modeling tools to evaluate the structural states and fatigue lives.

22 GENERAL STUDIES OF NUCLEAR REACTORS↗

Effect of type of load on stress analysis of thin-walled ducts

The standard procedure for qualifying the design of duct (pipe) systems in the Space Shuttle Main Engine (SSME) has been fairly well defined. However, since pipe elbows are quite common and important in the SSME duct systems, a clear understanding of the detailed stress profile of the components is necessary for accurate structural and life assessments. This study was initiated to predict the stress profile at/near the tangent point along the cross section of the duct under various types of loads. Also, this study was further extended to understand the stiffening effect on stresses due to pressure at the tangent point. The intention of this study was to identify the importance of selecting proper locations for mounting strain gauges and to utilize the obtained results to anchor dynamic models for accurate structural and life assessments of the SSME ducts under a dynamic environment. The finite element method was utilized in this study.

Min, J. B.↗

Stresses In And Near A Bend In A Thin-Walled Duct

Report describes computational study of distributions of stresses in and near 90 degrees bend in thin-walled duct subject to various applied loads. Purpose of study to help satisfy need for more accurate knowledge of local concentrations of stresses caused by loads: such knowledge makes possible to design light-weight ducts to survive reasonably foreseeable operating conditions with some degree of reliability. Also guides selection of locations for mounting strain gauges to measure local stresses for comparison with computed values, contributing to refinement of theoretical concepts and computational techniques.

Min, J. B.↗