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DOE OSTI2020

Broadband and omnidirectional polymer antireflection coatings

A method for generating antireflective coatings for polymeric substrates using a deposition process and/or a dissolving process can provide a coating onto the outer surface of the substrate. Some embodiments can include a GLAD generated fluoropolymer coating or a co-evaporated fluoropolymer coating on a substrate that may achieve ultralow refractive index as well as improved adhesion and durability properties on polymeric substrates. In some embodiments, the deposition process is performed such that a fluoropolymer can be evaporated to form chain fragments of the fluoropolymer. The chain fragments diffused into the substrate can subsequently re-polymerize, interlocking with the polymer chains of the substrate. In some embodiments, the co-evaporation process can form a nanoporous polymer chain scaffold of the fluoropolymer, from which a sacrificial material can be dissolved out. The formed coating can be a multilayer or continuously-graded antireflective coating that has strong adhesion with the substrate.

36 MATERIALS SCIENCE↗

DOE OSTI2022

Broadband and omnidirectional polymer antireflection coatings

Wang, Baomin↗

DOE OSTI2022

Ultra efficient turbo-compression cooling systems

Aspects of the present disclosure include a system for turbo-compression cooling. The system may be aboard a marine vessel. The system includes a power cycle and a cooling cycle. The power cycle includes a first working fluid, a waste heat boiler configured to evaporate the working fluid, a turbine, and a condenser. The condenser condenses the working fluid to a saturated or subcooled liquid. The cooling cycle includes a second working fluid, a first compressor configured to increase the pressure of the second working fluid, a condenser configured to condense the second working fluid to a saturated or subcooled liquid after exiting the first compressor, an expansion valve, and an evaporator. The turbine and first compressor are coupled one to the other. The waste heat boiler receives waste heat from engine jacket water and lubricating oil from a ship service generator. The evaporator cools water in a shipboard cooling loop.

Bandhauer, Todd M.↗

DOE OSTI2023

Simulations of Fuel-Air Mixing in a 7 Element Lean Direct Injection (LDI) Aviation Combustor

The increased accessibility of commercial aviation to the general population has in-creased the conventional jet fuel consumption, thereby causing increased CO2 emissions. One of the strategies to reduce the environmental impact is to use sustainable aviation fuels (SAFs). SAFs are jet fuels obtained from renewable resources such as biomass and waste streams such as plastics/municipal solid wastes. Even though the use of SAFs has been gaining importance over the last two decades, only a few numerical studies on their usage have been reported so far. In this study, two SAFs namely, Alcohol to Jet (ATJ) and Hydrotreated Esters and Fatty Acids (HEFA), are chosen and their use in a simple, Lead Direct Injection (LDI) combustor is studied. The focus of this study is limited to the thermo-chemical properties of the fuels and their impact on fuel distribution and evaporation. Hence, only non-reactive simulations are performed. A high accuracy, adaptive mesh refinement based low-Mach solver, PeleLMeX, is used for performing the simulations. The time-averaged flow results indicate faster evaporation of HEFA when compared to ATJ and Jet-A. The difference in fuel evaporation rates is attributed to the differences in fuel viscosity and surface tension properties and the concomitant variations in the fuel droplet size distributions.

adaptive mesh refinement↗

DOE OSTI2023

Simulations of Fuel-Air Mixing in a 7 Element Lean Direct Injection (LDI) Aviation Combustor: Preprint

The increased accessibility of commercial aviation to the general population has in-creased the conventional jet fuel consumption, thereby causing increased CO2emissions. One of the strategies to reduce the environmental impact is to use sustainable aviation fuels (SAFs). SAFs are jet fuels obtained from renewable resources such as biomass and waste streams such as plastics/municipal solid wastes. Even though the use of SAFs has been gaining importance over the last two decades, only a few numerical studies on their usage have been reported so far. In this study, two SAFs namely, alcohol to jet (ATJ) and hydrotreated esters and fatty acids (HEFA), are chosen and their use in a simple, lead direct injection (LDI) combustor is studied. The focus of this study is limited to the thermo-chemical properties of the fuels and their impact on fuel distribution and evaporation. Hence, only non-reactive simulations are performed. A high accuracy, adaptive mesh refinement based low-Mach solver, PeleLMeX, is used for performing the simulations. The time-averaged flow results indicate faster evaporation of HEFA when compared to ATJ and Jet-A. The difference in fuel evaporation rates is attributed to the differences in fuel viscosity and surface tension properties and the concomitant variations in the fuel droplet size distributions.

adaptive mesh refinement↗

DOE OSTI2017

A novel approach to criticality accident detection for a legacy facility

For operations on the Sellafield site involving fissile material a Criticality Accident Alarm System (CAAS) has traditionally been installed unless an omission case can be made. An omission case would examine if, in the absence of all controls, a criticality could reasonably be expected or whether the potential dose to an operator would remain below a maximum acceptable dose. It is a UK legal requirement for adequate emergency arrangements to be in place for hazards on a nuclear licensed site. For facilities where criticality is credible there is a regulatory expectation that a -Criticality Warning System- should be in place. A -Criticality Warning System- is not necessarily a full CAAS and alternative means of criticality detection may be part of an adequate emergency plan. The Sellafield site has a Magnox fuel reprocessing facility which has been operated since the 1960's. Evaporation of the Medium Active (MA) liquid waste from this process is undertaken in an associated building. Following extensive review of the plant and process a number of maloperations which can route fissile material to the MA evaporator were identified. Adequate controls to prevent these scenarios were shown to be in place. In the unlikely event of a failure of controls leading to sustained loss of fissile material a criticality incident may occur and hence an emergency plan was determined to be necessary. The novel emergency arrangements which were developed utilized the existing gamma monitor network located across multiple building floors. These gamma monitors are present for radiological safety. This emergency arrangement would require rapid interpretation of the gamma alarms by an operator and the manual triggering of a criticality evacuation alarm. The gamma monitors were demonstrated to be able to detect the minimum incident of concern (10{sup 15} fissions) as well as being able to alarm during the ramp up in power of a large criticality incident (10{sup 18} fissions). It was shown that a criticality accident could readily be distinguished from a radiological event (e.g. loss of containment). To support this work, criticality excursion analysis was used to examine the likely characteristics of a criticality in the MA evaporator. This novel arrangement was justified due to a number of factors including: the limited remaining operational lifetime of this facility (<5 years), the low frequency of maloperation coupled with a failure of controls and the crucial risk reduction provided by the continued reprocessing of Magnox fuel. Furthermore, the time and cost involved with design and installation of a standard CAAS would be substantially greater than a plan based upon existing instrumentation. These arguments were accepted by the UK regulator the Office for Nuclear Regulation (ONR). (author)

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

DOE OSTI2024

High Performance Heat Pipe Power Transient Testing at SPHERE Facility

Microreactors are being researched, designed, and built at Idaho National Laboratory (INL). Microreactors are small reactors defined at less than 20MW of power. These reactor concepts are also being looked at throughout industry for various applications. An important aspect of these reactor designs is economic feasibility i.e. lower overnight capital cost. The driving factors for implementing microreactors are quick setup and takedown, minimal operators, and the ability to manufacture them readily and to fit in mid-sized containers for transport. A specific area of research to aid in successful integration of these factors within the designs is passive heat removal of the core’s thermal power. Interest in heat pipes to achieve this passive heat removal has been shown across multiple industry partners. Because of this interest, INL has developed a test facility to facilitate experimental tests for sodium filled heat pipes. INL has developed the Single Primary Heat Extraction and Removal Emulator (SPHERE) facility to run experiments on high performance, sodium filled heat pipes. As mentioned above, heat pipes are passive heat transfer devices. Radially, heat pipes are broken up into an outer wall, a small annular gap, a wick structure, and a centerline gap. They function by utilizing latent heat transfer. Heat pipes are traditionally separated into three regions, an evaporator (heat input), an adiabatic region, and finally a condenser region (heat removal). As heat is being applied to the evaporator, the working fluid undergoes a phase change to a vapor. This phase change causes a differential pressure across the axial length of the pipe driving flow down the center gap of the heat pipe. The vapor flows down past the adiabatic region to the condenser where the heat is removed. This heat removal forces the working fluid to phase change back to a liquid. The wick structure is then utilized to drive the flow back towards the evaporator by capillary forces. This backflow is aided by the annular gap. Because this heat transfer mechanism functions with latent heat transfer, the heat pipe is close to isothermal down the axial length. Heat pipes can operate under a wide range of working fluids. Considerations for these working fluids are primarily driven by operating temperatures amongst other important factors based around overall performance. Sodium filled heat pipes operate from 450°C up to 900°C. This temperature range works well for the current microreactor designs. In conjunction with this experimental capability, INL has developed a modeling software to simulate heat pipe physics within reactor cores. This modeling software is called Sockeye and functions under the established INL Multiphysics Object Oriented Simulation Environment (MOOSE). SPHERE also supports Sockeye development by providing the modeling team with experimental data on an array of setups and operating parameters to support validation efforts. A power transient experiment was performed utilizing the SPHERE facility to continue to aid with Sockeye development. The testing followed a proposed test plan to ramp up and down the temperature of the heat pipe. Sockeye models steady state heat pipe operation with high accuracy, the data provided by the power transient testing aims to assist with the validation efforts and further enhance transient modeling capability of the tool [2].

22 GENERAL STUDIES OF NUCLEAR REACTORS↗

DOE OSTI2024

, Experimental Investigation of Electrically Charged Water Droplets Two-Phase Cross-Flow Interactions with Humid

Electrically charged water droplets can capture water vapor molecules in surrounding moist air and promote vapor condensation. This concept unfolds an alternative to mechanical cooling-based air dehumidification systems that separate sensible and latent cooling loads in HVAC applications. The effect of dielectrophoresis, electro-hydrodynamic, and micro-diffusive flows due to highly electrically charged water droplets traveling through moist air were investigated as new methods to reduce the air’s water vapor content. This paper presents new experimental data on humidification and power consumption for a system consisting of highly energized electrosprays in combination with mist eliminators. Electrosprays produced highly charged water spray cones crossing the air perpendicularly and upwardly. The moist air stream was circulated in a horizontal duct at 22C, 80% relative humidity, and 0.24 ms-1 airspeed. Mist eliminators made of stainless wire clothes of 36 and 25 μm pore diameter were used to screen the droplets growing during their flight trajectory. The mist eliminators blocked some of the largest diameter droplets. Still, they could not prevent re-evaporation of the droplets into the bulk air from the droplets deposited on their wire clothes. The equilibrium between the dielectrophoresis condensation from the electrosprays and the droplets’ re-evaporation phenomena resulted in reduced humidification when compared to conventional-type spray evaporative cooling systems. However, to dehumidify the air, the droplets injected by the electrosprays must be separated entirely and promptly removed from the bulk airflow at the end of their flight trajectory.

Electrostatic droplets, Electrospray, humidificati↗

DOE OSTI2026

Flow Boiling Pressure Drop Characteristics of Next-generation Refrigerants in a Micro‑fin Copper Tube

This paper presents experimental frictional pressure-drop data for flow boiling of R-410A, R-134a, and next-generation alternatives R-454C, R-455A, R-1234yf, and R-1234ze(E) in a horizontal micro-fin copper tube. Tests were conducted over a range of mass fluxes and evaporation temperatures to characterize refrigerant-dependent two-phase pressure-drop behavior. The results show that frictional pressure gradient increased with mass flux and vapor quality and generally increased as evaporation temperature decreased, with liquid viscosity strongly affecting the observed trends. Among the evaluated correlations, the Goto et al. (2001) model gave the best overall agreement with the measurements before optimization. Further optimization of the Kuo and Wang (1996) and Goto et al. (2001) models reduced the overall mean absolute deviation to below 15%, with the optimized Goto (2001) model providing the most consistent predictions across all six refrigerants. The results support improved pressure-drop prediction and evaporator design for next-generation refrigerants in micro-fin tubes.

Hu, Yifeng [ORNL] (ORCID:0000000242875185)↗

DOE OSTI2018

Epitaxial Growth of Cadmium Selenide Films on Silicon with a Silicon Carbide Buffer Layer

An epitaxial cubic 350-nm-thick cadmium selenide has been grown on silicon for the first time by the method of evaporation and condensation in a quasi-closed volume. It is revealed that, in this method, the optimum substrate temperature is 590°C, the evaporator temperature is 660°C, and the growth time is 2 s. To avoid silicon etching by selenium with formation of amorphous SiSe{sub 2}, a high-quality ~100-nm-thick buffer silicon carbide layer has been synthesized on the silicon surface by substituting atoms. The powder diffraction pattern and the Raman spectrum unambiguously correspond to cubic cadmium selenide crystal. The ellipsometric, Raman, and electron diffraction analyses demonstrate high structural perfection of the cadmium selenide layer and the absence of a polycrystalline phase.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

DOE OSTI2026

Daily evapotranspiration changes during heatwaves at 32 NEON sites, 2019-2021

This dataset provides partitioned evapotranspiration (ET, the combined loss of water from soil and plant surfaces) anomalies during heatwave events—soil evaporation (E) and transpiration (T)—for 268 heatwave events across 32 National Ecological Observatory Network (NEON) flux sites in the contiguous United States from 2019–2021. Using an ensemble of four high-frequency turbulence methods (Flux-variance Similarity, Conditional Eddy Covariance [CEC], CEC with Water-Use Efficiency, and Conditional Eddy Accumulation; see Zahn and Bou-Zeid 2024), half-hourly transpiration-to-evapotranspiration (T/ET) ratios were derived from 20 hertz (Hz, cycles per second) eddy covariance measurements of carbon dioxide (CO₂) and water vapor (H₂O) concentrations. The dataset spans six vegetation types including evergreen and deciduous forests, grasslands, cultivated crops, shrublands, and emergent herbaceous wetlands. Data Package Contents: The dataset includes a single CSV (comma-separated values) file containing daily anomalies (deviations from baseline conditions) for transpiration (Delta_T), evaporation (Delta_E), total evapotranspiration (Delta_ET), and T/ET ratio (Delta_T_ET) during each day of identified heatwave events. The file also includes site codes, dates, heatwave event identifiers, and day-of-heatwave indicators. The CSV file can be opened with spreadsheet software (Microsoft Excel, Google Sheets) or programming environments (Python, R, MATLAB). This resource enables researchers to investigate ecosystem-specific responses to thermal extremes, validate land surface model partitioning of ET fluxes, and examine feedbacks between water cycling and surface energy balance during heatwaves. The dataset is particularly valuable for studies linking vegetation hydraulic strategies to climate resilience, as it captures the divergent responses of shallow-rooted versus deep-rooted ecosystems. Potential applications include improving drought early warning systems, informing irrigation management strategies, and advancing our mechanistic understanding of land-atmosphere interactions under extreme heat conditions.

Day of Heatwave↗

DOE OSTI2026

Data and scripts associated with a manuscript analyzing ELM-FATES parameter sensitivity under pre-fire and postfire scenarios using machine learning

NOTE: The manuscript associated with this data package is currently in review. The data may be revised based on reviewer feedback. Upon manuscript acceptance, this data package will be updated with the final dataset and additional metadata. This data package is associated with the manuscript “Fire Severity-Dependent Shifts in Vegetation Parameter Sensitivity: A Pre- and Post-Fire Analysis Using ELM-FATES and Explainable AI” submitted to Journal of Advances in Modeling Earth Systems (Zahura et al. 2026). The study examines vegetation physiological parameters controlling pre-fire and post-fire vegetation dynamics. To support this analysis, 73 vegetation parameters in Functionally Assembled Terrestrial Ecosystem Simulator (FATES) (Fisher et al., 2018) , which is coupled with E3SM (Energy Exascale Earth System Model) land model (ELM, ELM-FATES), were perturbed using a Sobol sequence to generate 1,024 ensemble members for two plant functional types: needleleaf evergreen extratropical trees (NEET) and C3 grass. Simulations were conducted for the pre-fire period (2016) and post-fire period (2018–2023). Burn severity was represented by modifying the Nesterov index in FATES to 75,000, 150,000, and 300,000 for low, moderate, and high severity, respectively. A no-fire scenario was also included. Simulations were performed for 16 grid cells in the American River Watershed across different burn severities and plant functional types. XGBoost (eXtreme Gradient Boosting) models were trained using the parameter ensembles and ELM-FATES-simulated outputs, including leaf area index (LAI), gross primary productivity (GPP), aboveground biomass, vegetation evaporation, transpiration, and soil evaporation. Models were trained separately for each year and burn severity, followed by SHAP (SHapley Additive exPlanations) analysis to identify changes in dominant parameters after fire disturbance. For details on how to navigate data packages generated by this project, see https://data.ess-dive.lbl.gov/portals/PNNLRiverCorridorSFA/About. The data package contains the ELM-FATES simulation data. The scripts and data related to the analysis will be added later. The inputs and outputs from ELM-FATES are inside the “FATES” folder. “FATES_domain_surface” contains the domain and surface netcdfs that were used to run ELM-FATES in the study area. “FATES_parameters” contains the 1024 ensembles that were generated using Sobol sequence. “FATES_outputs” folder contains ELM-FATES simulated variables. All files are .csv and .nc (NetCDF).

Aboveground biomass↗

DOE OSTI2018

Mercury Recovery at Former Lithium Production Site at the Miramas in France - 18529

The former Lithium production facility located at Miramas in the South-East of France recently completed a 10-year program of process equipment removal, building demolition and soil remediation to recover mercury (Hg) that had been lost during operations at the site. After over 100 years ago chemical production, all production activities stopped in 2009, and immediately afterwards the clean-up project began. The main project focused on the demolition of all facilities and the decontamination of building materials and soil clean-up, with the goal of remediating the site for future industrial purposes. Prior to starting the decommissioning and clean-up work at the site a detailed site survey was conducted to identify the extent of the contamination of the site. After investigations into available technologies, the decision was made to install on-site treatment processes. This resulted in fewer residual environmental effects (trucking pollution, shipping containers, volume of materials, etc), a reduction in logistic complications, and, importantly, was cost effective compared to sending all untreated material to external processing facilities. This decision resulted in a need to optimize demolition waste management, while ensuring the highest clean-up and safety levels. A variety of treatment processes were investigated and compared and two technologies were finally selected and implemented. The first process was a 'thermal desorption unit (TDU),' which heated excavated soils and captured the vaporized mercury. The second was a washing process that was used to remove surface contamination. After the contaminated areas were excavated, materials were crushed, screened and sorted into different sizes, with each pile being routed to the appropriate process. The smaller-sized particles were treated in the TDU. A batch of around 12 MT was fed into a moisture evaporator and then into a mercury evaporator. The soils were then cooled, sampled to ensure no residual Hg contamination before being mixed with a binding agent, and returned to the excavation site. Larger materials with surface contamination were washed to remove the contamination. The liquid effluents were sent to a tank where the contaminated fines were removed, dried, pressed and sent for processing. If the washed, coarse materials failed to reach acceptable mercury levels, they were crushed again and sent to be treated in the TDU. The washing fluid was recycled for the next batch. (author)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

DOE OSTI2019

Development of New Antifoam for High Level Waste Processing in DWPF

During processing in the Defense Waste Processing Facility (DWPF), the evaporation of sludge leads to large amounts of foaming. This foaming can cause a foam-over, which contaminates other parts of the facility, most importantly the condensate. Currently, the antifoam being used is not sufficient at more extreme pH values and relatively high concentrations are required to minimize foaming. This means that a foam-over is more likely in parts of the process where the pH moves away from the neutral point and antifoam is needed in large quantities to prevent such occurrences. Adding this antifoam can also double processing time. The current antifoam also degrades into flammable byproducts, which creates a hazard in the processing. There are two main ideas proposed in order to solve the problems with the current antifoam: A new antifoam; A mechanical solution (sprays, agitator, etc). The focus of this summer was to develop a new antifoam that works across a broader range of pH values, can be added in lower concentrations, and does not degrade into flammable byproducts. This solution was pursued by obtaining different superspreaders and antifoams from companies across the country in order to perform a series of tests on them; these tests include superspreader testing, Foamscan testing, boiling testing, and Sludge Receipt and Adjustment Tank (SRAT) and Slurry Mix Evaporator (SME) process testing. To begin testing, four different superspreaders were tested on their ability to spread. The four superspreaders include: Y-17112, Y-17309, Antifoam 747 (the old antifoam), and Silwet L77 (the main component in Antifoam 747). These superspreaders were tested across a range of pH values and concentrations from 100 ppm to 5000 ppm. After completion of the tests, the results indicated that Y-17112 spread across a wider pH range than the others, even at lower concentrations. This is ideal for developing a new antifoam, as the pH throughout processing in DWPF varies and the lower the necessary concentration, the less antifoam that must be added per cycle. In order to test whether or not the superspreaders work as an antifoam, they have to be tested on real foam. In order to test this, a foamy simulant similar to the foaminess of the sludge in DWPF needed to be developed. This required testing many different sludges and designing our own simulant with different concentrations of insoluble solids. Eventually, a simulant similar enough to what is seen in DWPF was identified. Each superspreader will be tested on the simulant at different pH values and at different concentrations. The simulant will be allowed to foam and small amounts of the superspreader will be added while the Foamscan software tracks the height of the foam column; this allows us to know if the superspreader decreased the foam or not. Next, boiling testing in the Foamscan will be completed. This is testing identical to the Foamscan testing at room temperature, only at boiling conditions similar to DWPF. After boiling testing, the superspreader that is deemed most successful will be tested in a real, scaled-down SRAT/SME cycle. This will ensure it works with all the real chemicals that are added in DWPF and that it will remain successful in all the conditions that it may face. After the SRAT/SME testing, a decision will be made on whether or not the superspreader is successful and it may or may not be chosen as the new antifoam for DWPF.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

DOE OSTI2026

Localized Heterogeneous Nucleation for Vapor‐Assisted Sequential Deposition of Metal Halide Perovskites

Vapor-assisted hybrid two-step deposition, which combines thermally evaporated inorganic layers with solution-processed organic halides to form halide perovskites, has emerged as a scalable and industry-compatible route for textured tandem photovoltaics. However, this process is often hindered by reaction-limited phase formation, particularly when compact, non-porous, and highly crystalline inorganic layers formed by thermal evaporation restrict subsequent conversion, resulting in incomplete reaction and pronounced depth-dependent heterogeneity. In this study, we introduce a strategy to regulate the inorganic precursor layer by incorporating localized heterogeneous nucleation sites. Sparsely distributed hydrophilic metal oxide species serve as effective nucleation centers during vapor deposition, enabling effective control over film morphology and crystal orientation from the early stages of growth. This tailored inorganic framework facilitates the subsequent incorporation of organic halides, alleviating reaction limitations and suppressing residual unreacted precursors. Consequently, the perovskite films exhibit improved stoichiometric uniformity and enhanced optoelectronic quality, enabling wide-bandgap perovskite solar cells with markedly improved performance and operational stability. This work provides important mechanistic insight into crystal growth engineering of vapor-deposited perovskite thin films.

nucleation↗

DOE OSTI2018

Seasonal variability of oxygen and hydrogen isotopes in a wetland system of the Yunnan-Guizhou Plateau, southwest China: a quantitative assessment of groundwater inflow fluxes

The Caohai Wetland serves as an important ecosystem on the Yunnan–Guizhou Plateau and as a nationally important nature reserve for migratory birds in China. In this study, surface water, groundwater and wetland water were collected for the measurement of environmental isotopes to reveal the seasonal variability of oxygen and hydrogen isotopes (δ{sup 18}O, δD), sources of water, and groundwater inflow fluxes. Results showed that surface water and groundwater are of meteoric origin. The isotopes in samples of wetland water were well mixed vertically in seasons of both high-flow (September) and low-flow (April); however, marked seasonal and spatial variations were observed. During the high-flow season, the isotopic composition in surface wetland water varied from −97.13 to −41.73‰ for δD and from −13.17 to −4.70‰ for δ{sup 18}O. The composition of stable isotopes in the eastern region of this wetland was lower than in the western region. These may have been influenced by uneven evaporation caused by the distribution of aquatic vegetation. During the low-flow season, δD and δ{sup 18}O in the more open water with dead aquatic vegetation ranged from −37.11 to −11.77‰, and from −4.25 to −0.08‰, respectively. This may result from high evaporation rates in this season with the lowest atmospheric humidity. Groundwater fluxes were calculated by mass transfer and isotope mass balance approaches, suggesting that the water sources of the Caohai Wetland were mainly from groundwater in the high-flow season, while the groundwater has a smaller contribution to wetland water during the low-flow season.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2019

Color optimization of red OLEDs via periodic and gradient deposition rate of fluorescent dopants

We have investigated a method to enhance the light emission efficiency and color tuning for mixture of dyes with varying the growth parameters, during Alq{sub 3}:Nile Red deposition. We used solvent bath and green laser (532 nm) for improvement of the performance of devices. This paper presents two kind of evaporation method, periodic and gradient. We observed that periodic emission layers can greatly improve the device performances such as electroluminescence, chromaticity coordinates, luminance, and reduced the turn on voltage. The periodic 3 structure with evaporation rate of (0.1 → 3 → 2 → 3 → 2 → 0.1 A°/s) has a luminance of 3000 cd/m{sup 2} and maximum efficiency of 1.8 cd/A at 18 V which are the highest values among devices.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

DOE OSTI2018

Magnesium Loss in Nd:YAG Pulsed Laser Welding of Aluminum Alloys

In the current investigation, the loss of magnesium (Mg) in Nd:YAG pulsed laser welding of a number of aluminum (Al) alloys was studied both experimentally and numerically. The experimental results showed that at a fixed average laser power, with the increasing pulse frequency, Mg concentration of the weld metals decreased. A numerical model was developed for the calculation of Mg evaporation from the weld pool. The model predicted a trend in the changes of Mg concentration of the weld pool, working best for alloys containing the higher levels of Mg. The calculations showed that with the increasing pulse frequency from 15 to 40 Hz, due to a decrease in the average temperature of the weld pool, Mg loss in terms of mass per unit area of the weld spot actually decreased from 230 × 10{sup −5} to 120 × 10{sup −5} kg/m{sup 2}. However, due to a decrease in the weld penetration/volume, the effective Mg loss of the weld metal in terms of concentration increased from 110 × 10{sup −1} to 260 × 10{sup −1} kg/m{sup 3}. It was shown that due to interactions between Mg and other main alloying elements, the activity coefficient of Mg had to be modified for the model to accurately predict Mg evaporation of the weld pool.

36 MATERIALS SCIENCE↗