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NASA NTRS1984

The accuracy of altimetric surfaces

Estimates of the shape of the sea surface as determined from satellite altimeters have become of increasing importance in geophysics, geodesy and physical oceanography. The most effective error reduction procedures used in producing these surfaces have been some version of a crossing-arc analysis. The problem with this procedure is the absence of an easy means of evaluating the noise structure of the final result. By recasting the problem as one of objective mapping (optimal estimation) the error reduction is optimized and an explicit estimate is obtained of the wave-number structure of the final altimetric surface. Examples, suitable to a small computer, have been generated to show that the error reduction along the sub-satellite tracks is very great, with most of the residual lying in long wavelengths.

Wunsch, C.↗

NASA NTRS1993

Design of a surface deformation measuring instrument for the Surface Tension Driven Convection Experiment (STDCE-2)

This final technical report covers the work accomplished (under NAG3-1300) from 1 October 1991 to 1 October 1993. The grant is a direct result of Dr. H. Philip Stahl's (of Rose-Hulman Institute of Technology) participation in the NASA/ASEE Summer Faculty Fellowship Program at NASA Lewis Research Center sponsored by Case Western Reserve University and the Ohio Aerospace Institute. The Surface Tension Driven Convection Experiment (STDCE) is a fundamental fluid physics experiment designed to provide quantitative data on the thermocapillary flow of fluid under the influence of an increased localized surface temperature. STDCE flew on the Space Shuttle Columbia in the First United States Microgravity Laboratory (USML-1) in June 1992. The second flight of this experiment (STDCE-2) is scheduled for 1995. The specific science objectives of STDCE-2 are to determine the extent and nature of thermocapillary flows, the effect of heating mode and level, the effect of the liquid free-surface shape, and the onset conditions for and nature of oscillatory flows. In order to satisfy one of these objectives, an instrument for measuring the shape of an air/oil free surface must be developed.

Stahl, H. Philip↗

DOE OSTI2023

Revealing a 3D Fermi Surface Pocket and Electron-Hole Tunneling in UTe 2 with Quantum Oscillations

Spin triplet superconductor UTe 2 is widely believed to host a quasi-two-dimensional Fermi surface, revealed by first-principles calculations, photoemission and quantum oscillation measurements. An outstanding question still remains as to the existence of a three-dimensional Fermi surface pocket, which is crucial for our understanding of the exotic superconducting and topological properties of UTe 2 . This 3D Fermi surface pocket appears in various theoretical models with different physics origins, but has not been unambiguously detected in experiment. Here, in this study, for the first time we provide concrete evidence for a relatively isotropic, small Fermi surface pocket of UTe 2 via quantum oscillation measurements. In addition, we observed high frequency quantum oscillations corresponding to electron-hole tunneling between adjacent electron and hole pockets. The coexistence of 2D and 3D Fermi surface pockets, as well as the breakdown orbits, provides a test bed for theoretical models and aid the realization of a unified understanding of superconducting state of UTe 2 from the first-principles approach.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

NASA NTRS1987

Parameterization of radiative flux profiles within layer clouds

This paper presents simple formulations for the vertical structure of solar and infrared radiative fluxes within a layer cloud overlying a partially reflective surface. The parameterized profile shapes are analytic, with governing parameters derived from bulk radiative properties and more physically based radiative transfer models. The bulk cloud, subcloud layer, and surface radiative properties are assumed to be known. The parameterizations are based on exponential functions of height, with decay scales related to cloud liquid water content. Although the results presented here are based on very simple assumptions about the cloud structure in the vertical, the method used is applicable to more general cases as well as to various other analytic and/or numerical radiative transfer calculations.

Hanson, Howard P.↗

DOE OSTI2018

Investigating the role of anhydrous oxidative weathering on sedimentary rocks in the Transantarctic Mountains and implications for the modern weathering of sedimentary lithologies on Mars

We present that alteration of the uppermost surfaces of geologic materials is a pervasive process on planetary surfaces that is dependent upon factors including parent composition and the environment under which alteration is occurring. While rapid and pervasive in hot and humid climates on Earth, chemical weathering of rock surfaces has also been found to dominate in some of Earth's coldest and driest landscapes as well. Specifically, surfaces dominated by resistant fine-grained igneous rocks in the Antarctic preserve evidence of oxidative weathering processes, which represent the initial immature surface alteration processes that stagnate due to the lack of available water and kinetics necessary for the production of more mature alteration phases. In this study, we test the hypothesis that oxidative weathering also dominates the surfaces of sedimentary rocks throughout the Antarctic. We investigated the chemistry and mineralogy of a suite of sedimentary rocks from the Transantarctic Mountains ranging from fine-grained tuffs to coarse-grained sandstones and conglomerates. Additionally, our results show that, like the previously studied fine-grained igneous rocks in the Antarctic, sedimentary rocks generally showed only minor chemical weathering signatures at their surfaces relative to their interiors. However, unlike the igneous rocks in this earlier study, the sedimentary rocks exhibited a wide variety of non-systematic differences between surface and interior compositions. This variability of surface weathering signatures is equally as complex as the physical properties and compositions inherently present within these different sedimentary lithologies. Based on these analyses, it is apparent that oxidative weathering products do not dominate the surfaces of sedimentary rocks throughout the Transantarctic Mountains, which instead exhibit a wide array of weathering signatures that are likely dependent on both lithological and environmental factors. Considering that sedimentary lithologies are widespread across a significant fraction of the martian surface, our results suggest that observed alteration signatures limited to the surfaces of martian sedimentary rocks are most likely to be minor and to vary as a result of the lithological properties of the specific rock unit and not as a result of the widespread influences of the modern cold and dry climatic conditions.

58 GEOSCIENCES↗

DOE OSTI2016

Observation of Fermi arc and its connection with bulk states in the candidate type-II Weyl semimetal WTe2

A kind of topological material, the type-II Weyl semimetal, was proposed recently where the Weyl points emerge at the contact points of the electron and hole pockets, resulting in a highly tilted Weyl cone. In type-II Weyl semimetals, the Lorentz invariance is violated and a different type of Weyl fermion is generated that leads to intriguing physical properties. WTe 2 is interesting because it is predicted to be a good candidate for realizing type-II Weyl semimetals. By utilizing laser-based angle-resolved photoemission spectroscopy with high energy and momentum resolutions, we have revealed a full picture of the electronic structure of WTe 2 . A clear surface state has been identified and its connection with the bulk electronic states in the momentum and energy space shows good agreement with band structure calculations. Our results provide electronic signatures that are consistent with type-II Weyl states in WTe 2 . They lay a foundation for further investigations on the topological nature of WTe 2 and the exploration of unique phenomena and physical properties in type-II Weyl semimetals.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

NASA NTRS1972

A numerical study of electromagnetic scattering from ocean like surfaces

The integral equations describing electromagnetic scattering from one dimensional conducting surfaces are formulated and numerical results are presented. The results are compared with those obtained using approximate methods such as physical optics, geometrical optics, and perturbation theory. The integral equation solutions show that the surface radius of curvature must be greater than 2.5 wavelengths for either the physical optics or geometric optics to give satisfactory results. It has also been shown that perturbation theory agrees with the exact fields as long as the root mean square surface roughness is less than one-tenth of a wavelength.

Lentz, R. R.↗

NASA NTRS1974

A numerical study of electromagnetic scattering from ocean-like surfaces

The integral equations describing electromagnetic scattering from cylindrical, perfectly conducting surfaces are formulated and numerical results are presented. The results are compared with those obtained using approximate methods such as physical optics, geometrical optics, and perturbation theory. The integral equation solutions show that the surface radius of curvature must be greater than 2.5 wavelengths for either the physical optics or geometrical optics to give satisfactory results. It has also been shown that perturbation theory agrees with the exact fields as long as the root-mean-square surface roughness is less than one tenth of a wavelength.

Lentz, R. R.↗

DOE OSTI2022

An E and B gyrokinetic simulation model for kinetic Alfvén waves in tokamak plasmas

The gyrokinetic particle simulation is a powerful tool for studies of transport, nonlinear phenomenon, and energetic particle physics in tokamak plasmas. While most gyrokinetic simulations make use of the scalar and vector potentials, a new model (GK-E&B) has been developed by using the E and B field in a general form and has been implemented in simulating kinetic Alfvén waves in uniform plasma. In our work, the Chen et al. GK-E&B model has been expressed, in general, tokamak geometry using the local orthogonal coordinates and general tokamak coordinates. Its reduction for uniform plasma is verified, and the numerical results show good agreement with the original work. The theoretical dispersion relation and numerical results in the local model in screw pinch geometry are also in excellent agreement. Numerical results show excellent performance in a realistic parameter regime of burning plasmas with high values of β/(M e k$^{2}_{⊥}$ρ$^{2}_{i}$), which is a challenge for traditional methods due to the “cancellation” problem. As one application, the GK-E&B model is implemented with kinetic electrons in the local single flux surface limit. With the matched International Tokamak Physics Activity-Toroidicity-induced Alfvén Eigenmodes parameters adopted, numerical results show the capability of the GK-E&B in treating the parallel electron Landau damping for realistic tokamak plasma parameters. As another application, the global GK-E&B model has been implemented with the dominant electron contribution in the cold electron limit. Its capability in simulating the finite E || due to the finite electron mass is demonstrated.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

DOE OSTI2017

Time-Domain Modeling of RF Antennas and Plasma-Surface Interactions

Recent advances in finite-difference time-domain (FDTD) modeling techniques allow plasma-surface interactions such as sheath formation and sputtering to be modeled concurrently with the physics of antenna near- and far-field behavior and ICRF power flow. Although typical sheath length scales (micrometers) are much smaller than the wavelengths of fast (tens of cm) and slow (millimeter) waves excited by the antenna, sheath behavior near plasma-facing antenna components can be represented by a sub-grid kinetic sheath boundary condition, from which RF-rectified sheath potential variation over the surface is computed as a function of current flow and local plasma parameters near the wall. These local time-varying sheath potentials can then be used, in tandem with particle-in-cell (PIC) models of the edge plasma, to study sputtering effects. Particle strike energies at the wall can be computed more accurately, consistent with their passage through the known potential of the sheath, such that correspondingly increased accuracy of sputtering yields and heat/particle fluxes to antenna surfaces is obtained. The new simulation capabilities enable time-domain modeling of plasma-surface interactions and ICRF physics in realistic experimental configurations at unprecedented spatial resolution. We will present results/animations from high-performance (10k-100k core) FDTD/PIC simulations of Alcator C-Mod antenna operation.

47 OTHER INSTRUMENTATION↗

NASA NTRS1995

Elliptic surface grid generation on minimal and parametrized surfaces

An elliptic grid generation method, which generates boundary conforming grids in a two dimensional physical space, is presented. The method is based on the composition of an algebraic and elliptic transformation. The composite mapping obeys the Poisson grid generation system with control functions specified by the algebraic transformation. It is shown that the grid generation on a minimal surface in a three dimensional space is equivalent to the grid generation in a two dimensional domain in physical space. A second elliptic grid generation method, which generates boundary conforming grids on smooth surfaces, is presented. Concerning surface modeling, it is shown that bicubic Hermit interpolation is an excellent method to generate a smooth surface crossing a discrete set of control points.

Spekreijse, S. P.↗

DOE OSTI2016

Characterizing DNA Corona Rigidity in DNA-Directed Gold Nanoparticle Crystalline Structures

DNA-linked gold nanoparticle systems have become an adaptable self-assembly tool for programming various crystalline orders. The programmability lies in the DNA corona, a highly dense outer shell of DNA linkers that binds the nanoparticles together. Various self-assembled structures can be formed by changing the properties of the DNA corona, particularly the size ratio. However, uncertainty still remains as to the actual behavior and structural rigidity of the DNA itself, impeding advances in structural diversification. Specifically, the DNA could adopt an A-form structure after crystallization, or a more flexible DNA corona could be generated if B-form DNA persists but becomes physically bent and adsorbed to the nanoparticle surface in crystal formations. To understand the rigidity of the DNA corona, we devised a method to stretch the DNA between two nanoparticles by simultaneously using short and long linkers. This linker combination flexibly acts as a single linker, rather than two separate linkers that create two ranges of interactions. By measuring the edge-to-edge distance between the two nanoparticles using both linkers in small-angle X-ray scattering (SAXS) experiments, we recorded the first per-base contribution that is consistent with the B-form DNA rise of 3.4 Å. Here, the elucidation of DNA behavior within nanoparticle crystals is essential for understanding the programmability of DNA-linked nanoparticle systems.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

NASA NTRS1984

Wind abrasion on Venus: A means for experimental investigations

A study to determine the feasibility of conducting experiments to simulate the aeolian environment on Venus as related to wind abrasion was completed. Ideally, such experiments should involve complete investigation of weathering, in which mechanical, thermal, and chemical parameters are taken into account. This is particularly important for Venus, where atmospheric temperatures and pressures at the surface produce an environment which is equivalent to low or medium grade metamorphic conditions on Earth. Details that describe the Venus Aeolian Abrasion Device (VAAD) are included. The VAAD device would enable experiments to be conducted with the same chemistry, temperature, pressure, and other physical properties of the Venus atmosphere near the surface. The proposed device enables the important aeolian parameters to be controlled and monitored, including particle size, velocity, impact-angle and flux, atmospheric pressure, temperature, and gas composition.

Greeley, R.↗

DOE OSTI2020

Interactions of Oxide Surfaces with Water Revealed with Solid-State NMR Spectroscopy

Hydrous materials are ubiquitous in the natural environment and efforts have previously been made to investigate the structures and dynamics of hydrated surfaces for their key roles in various chemical and physical applications, with the help of theoretical modeling and microscopy techniques. However, an overall atomic-scale understanding of the water–solid interface, including the effect of water on surface ions, is still lacking. Herein, we employ ceria nanorods with different amounts of water as an example and demonstrate a new approach to explore the water–surface interactions by using solid-state NMR in combination with density functional theory. NMR shifts and relaxation time analysis provide detailed information on the local structure of oxygen ions and the nature of water motion on the surface: the amount of molecularly adsorbed water decreases rapidly with increasing temperature (from room temperature to 150 °C), whereas hydroxyl groups are stable up to 150 °C, and dynamic water molecules are found to instantaneously coordinate to the surface oxygen ions. Additionally, the applicability of dynamic nuclear polarization for selective detection of surface oxygen species is also compared to conventional NMR with surface selective isotopic-labeling: the optimal method depends on the feasibility of enrichment and the concentration of protons in the sample. These results provide new insight into the interfacial structure of hydrated oxide nanostructures, which is important to improve performance for various applications.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

NASA NTRS2001

Sedimentary Parameters Controlling Occurrence and Preservation of Microbial Mats in Siliciclastic Depositional Systems

Shallow-marine, siliciclastic depositional systems are governed by physical sedimentary processes. Mineral precipitation or penecontemporaneous cementation play minor roles. Today, coastal siliciclastic environments may be colonized by a variety of epibenthic, mat-forming cyanobacteria. Studies on microbial mats showed that they are not randomly distributed in modern tidal environments. Distribution and abundancy is mainly function of a particular sedimentary facies. Fine-grained sands composed of "clear" (translucent) quartz particles constitute preferred substrates for cyanobacteria. Mat-builders also favor sites characterized by moderate hydrodynamic flow regimes, which permit biomass enrichment and construction of mat fabrics without lethal burial of mat populations by fine sediments. A comparable facies relationship can be observed in ancient siliciclastic shelf successions from the terminal Neoproterozoic Nama Group, Namibia. Wrinkle structures that record microbial mats are present but sparsely distributed in mid- to inner shelf sandstones of the Nudaus Formation. The sporadic distribution of these structures reflects both the narrow ecological window that governs mat development and the distinctive taphonomic conditions needed to preserve the structures. These observations caution that statements about changing mat abundance across the Proterozoic-Cambrian boundary must be firmly rooted in paleoenvironmental and taphonomic analysis. Understanding the factors that influence the formation and preservation of microbial structures in siliciclastic regimes can facilitate exploration for biological signatures in Earth's oldest rocks. Moreover, insofar as these structures can be preserved on bedding surfaces and are not easily mimicked by physical processes, they constitute a set of biological markers that can be searched for on Mars by remotely controlled rovers.

Noffke, Nora↗

DOE OSTI2021

Dynamic deuterium retention properties of tungsten measured using laser-induced breakdown spectroscopy

Dynamic deuterium (D) retention properties of tungsten (W) are investigated under steady-state D plasma exposure in the PISCES-A linear plasma device. In contrast to static retention, dynamic retention is quickly released from the material at the termination of the incident plasma flux, and thus in-operando laser-induced breakdown spectroscopy (LIBS) measurements have been conducted during steady-state D plasma exposure. A procedure is, first, established to extract the dynamic retention component from the in-operando LIBS D I 656.1 nm line intensity, which can contain contributions from dynamic and static retention as well as background D/D 2 gas, excited by both steady-state and laser-induced plasmas. Using the developed procedure, the dynamic D retention in W is systematically examined while scanning the following plasma exposure parameters: incident ion energy, E i , sample temperature, T s , incident ion flux, Γ i . No clear E i dependence is seen in the range of E i ~ 45–175 eV, as expected from a small variation in the average implantation depth (~3-6 nm) of D in W. The dynamic retention is found to monotonously decrease with increasing T s from 348 to 573 K, while the total static retention is reported to peak at T s ~ 500–600 K. It is revealed that the dynamic retention linearly increases with increasing Γ i , and then saturates at Γ i ≥ 0.75 × 10 21 m –2 s –1 . Possible physical mechanisms for the observed dependence of the dynamic retention on T s and Γ i are discussed. Furthermore, sequential pure He, followed by pure D, plasma exposures show that the dynamic D retention is not strongly affected by He bubbles in the near-surface region.

super-saturated surface layer↗

DOE OSTI2026

Self-Assembly Driven Microlithography via Near-Infrared Light Activation

Current vat photopolymerization (VP) relies on UV or visible light to start the rapid crosslinking of liquid photocurable resins into 3D-printed structures. Here, we develop a self-assembly-driven photopatterning approach to photothermally generate polymeric solids by combining thermoplasmonic nanoparticles and thermoresponsive polymers, in which near-infrared (NIR) light activates thermoplasmonic heating of nanoparticles, triggering the irreversible self-assembly of thermoresponsive polymers into insoluble mesoglobules. A small amount of thermal initiator and crosslinker leads to irreversible self-assembly of polymer nanocomposites. NIR light offers deeper penetration and reduced scattering compared to UV, enabling more uniform curing of thicker or filled materials and expanded process control for composites or opaque systems. Thermoplasmonic heat generation is achieved using surface-modified gold nanorods (AuNRs) with a longitudinal localized surface plasmon resonance peak in the NIR region. Key variables such as polymer composition, molecular weight, physical interactions at the nanoparticle–polymer interface, which can be tuned by surface functionalization, AuNR concentration, and pH can be used to tailor the assembly behavior of these systems, including photothermal effect, flocculation, and cloud point temperature, and the mechanical properties of the final structures. Collectively, these results highlight a platform for photothermally-driven microlithography of polymer solids with diverse, tunable macroscopic properties, enabled by low-energy NIR light-activated self-assembly.

36 MATERIALS SCIENCE↗

NASA NTRS1986

Electrically conductive, black thermal control coatings for space craft application. II - Silicone matrix formulation

Five black electrically conductive thermal-control coatings have been formulated and tested for application on the Galileo spacecraft. The coatings consisted of organic and inorganic systems applied on titanium and aluminum surfaces. The coatings were tested under simulated space environment conditions. Coated specimens were subjected to thermal radiation and convective and conductive heating from -196 to 538 C. Mechanical, physical, thermal, electrical, and optical characteristics, formulation, mixing, application, surface preparation of substrates, and a method of determining electrical resistance are presented for the silicone matrix formulation designated as GF-580.

Hribar, V. F.↗