Dynamic response of biological materials.
Effect of varying strain rate on physical properties of bone and muscle tissue, measuring load and time displacement with constant-velocity compression test machine
STRAIN RATE↗
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High-performance molded composites using additively manufactured preforms with controlled fiber and pore morphology
Here, large-scale multimaterial preforms produced by additive manufacturing (AM) underwent compression molding (CM) to produce high-performance thermoplastic composites reinforced with short carbon fibers. AM and CM techniques were integrated to control the fiber orientation (microstructure) and to reduce void content for the improved mechanical performance of the composite. The new integrated manufacturing technique is termed “additive manufacturing-compression molding” (AM-CM). For the present study, the most common materials were used for large-scale printing, i.e., acrylonitrile butadiene styrene (ABS), carbon fiber (CF)–filled ABS (CF/ABS) and glass fiber (GF)–filled ABS (GF/ABS). Three different manufacturing processes; (a) AM (b) extrusion compression molding (ECM), and (c) AM-CM were used to prepare four different panel configurations: (1) neat ABS, (2) CF/ABS, (3) overmold (CF/ABS over neat ABS), and (4) sandwich (neat ABS between two CF/ABS layers). The mechanical properties (tensile and flexural strength and modulus, and Izod impact energy) of samples prepared via all three manufacturing processes were compared. X-ray microcomputer tomography was employed to evaluate the fiber orientation distribution and the volumetric porosity content. The preform maintained high fiber alignment (≈ 82% of fibers within the range of 0–20° in the deposition direction), and the volumetric porosity was reduced by 50% from 3.79% to 1.91% after compression. The alignment of long pores along the deposition direction was also observed. The mechanical properties are discussed with correlation to the fiber alignment and void content in the samples. CF/ABS samples prepared by AM-CM showed significant improvement of 11.15%, 35.27%, 28.6%, and 74.3% in the tensile strength, tensile modulus, flexural strength, and flexural modulus, respectively, when compared with samples prepared by ECM. Unique aspects of this study are the demonstration of large-scale multimaterial AM and the use of multimaterials as preforms to make high-performance composites.
36 MATERIALS SCIENCE↗
Sizing comingled CF/PA 6 fibers with cellulose nanofibrils for enhanced performance properties
Compatibility between the reinforcing phase and the polymer matrix is critical to achieving the desired mechanical and thermal performance of composite materials. Several mechanisms can enhance this interfacial interaction, including surface treatments (e.g., oxidation, plasma, or irradiation), in-situ nanoparticle deposition, and fiber sizing. Here, in this study, cellulose nanofibrils (CNF) were employed as a sustainable sizing agent to modify the interface in commingled carbon fiber (CF)/polyamide 6 (PA 6) yarns, in which CF and PA6 filaments are intimately blended to enable simultaneous consolidation. A 0.25 wt% CNF aqueous suspension was applied under bath sonication to ensure uniform dispersion and minimize agglomeration. CNF-sized and unsized yarns were used to fabricate unidirectional composite plates via filament winding on a flat mandrel, followed by compression molding. Scanning electron microscopy confirmed CNF presence on both CF and PA6 filaments. CNF-sized composites exhibited increments in interlaminar shear strength (ILSS) by 50%, flexural strength by 11%, and tensile strength by 2.5% compared to unsized composites. Thermal analysis showed minimal changes in degradation temperature and crystallinity. These findings demonstrate that CNF sizing enhances interfacial bonding and mechanical performance, offering a scalable and environmentally friendly strategy for thermoplastic composite manufacturing along with yarn/tow handleability.
Cellulose nanofibrils (CNF)↗
Effects on the geomagnetic tail at 60 earth radii of the geomagnetic storm of April 9, 1971.
A geomagnetic storm beginning with an sc occurred on Apr. 9, 1971. During the storm the charged particle lunar environment experiment at the Apollo 14 site, the solar wind spectrometer experiment at the Apollo 12 site, and the Ames magnetometers on Explorer 35 took data in the magnetosheath, at the magnetopause, in the plasma sheet, and in the high-latitude geomagnetic tail. The MIT Faraday cup and Ames magnetometers on board Explorer 33 monitored the solar wind. The data show that the storm was caused by a corotating tangential discontinuity in the solar wind, the magnetopause position is strongly dependent on the attack angle of the solar wind, and the tail field strength was indirectly measured to increase from 10 to 14 gamma after the sc. During the main phase the field strength in the tail was observed to increase to between 28 and 34 gamma. This increase is consistent with a thermal and magnetic compression of the tail radius from about 26 to about 16 earth radii.
Burke, W. J.↗
Steady supersonic Navier-Stokes solutions of a 75 deg delta wing
Steady solutions about a slender sharp edged delta wing in a supersonic freestream for moderate and high angles of attack are obtained numerically by time integration of the unsteady compressible three dimensional laminar Navier-Stokes equations. The main features of the flow, including primary and secondary separation, and vortex position and strength, are adequately simulated in the numerical solutions. Improved resolution of the computational grid in the leading edge region from a previous solution had considerable effect on the accuracy of the solutions. Good agreement between numerical solutions and experimental data was obtained for two cases. A local timestepping procedure is used to speed convergence by approximately a factor of two.
Buter, T. A.↗
Process For Autoclaving HMW PMR-II Composites
Parts made of graphite-reinforced, high-molecular-weight (HMW) PMR-II polyimide easy to fabricate by autoclaving. Study showed autoclaved HMW PMR-II parts equal in quality to those made by compression molding. Well suited to use at temperatures up to 700 degrees F (371 degrees C). In aircraft engines, they offer advantages of strength and light weight.
Vannucci, Raymond D.↗
Interactive calculation procedures for mixed compression inlets
The proper design of engine nacelle installations for supersonic aircraft depends on a sophisticated understanding of the interactions between the boundary layers and the bounding external flows. The successful operation of mixed external-internal compression inlets depends significantly on the ability to closely control the operation of the internal compression portion of the inlet. This portion of the inlet is one where compression is achieved by multiple reflection of oblique shock waves and weak compression waves in a converging internal flow passage. However weak these shocks and waves may seem gas-dynamically, they are of sufficient strength to separate a laminar boundary layer and generally even strong enough for separation or incipient separation of the turbulent boundary layers. An understanding was developed of the viscous-inviscid interactions and of the shock wave boundary layer interactions and reflections.
Reshotko, Eli↗
Defect sensitivity of filament-wound structures in compression
Compression testing of 12-ply graphite/bismaleimide laminated plates with induced and natural defects is discussed, and emphasis is placed on resultant changes in strength and stiffness. Ply drops, ply cuts, and fiber crossovers are studied by comparison with a quasi-isotropic control group. It is observed that, as expected, failure initiates at the defects and progresses via delamination, sublaminate buckling, angle-ply cracking, and longitudinal ply failure. The ultimate stress is reduced by approximately 40 percent for all types of defects except the unsymmetrical cut-ply specimens which averages a 54-percent reduction. The average stiffness reduction of 10 percent is observed for specimens with induced defects. Fiber crossovers are found to reduce the laminate strength and stiffness significantly.
Jensen, David W.↗
Behavior of compacted lunar simulants using new vacuum triaxial device
The objectives of this study are to create a lunar simulant locally from a basaltic rock and to design and develop a vacuum triaxial test device that can permit testing of compacted lunar simulant under cyclic loading with different levels of initial vacuum. Triaxial testing is performed in the device itself without removing the compacted specimen. Preliminary constrained compression and triaxial shear tests are performed to identify effects of initial confinements and vacuums. The results are used to define deformation and strength parameters. At this time, vacuum levels up to 0.0001 are possible. The research can aid in the development of compacted materials for various construction applications.
Desai, Chandra S.↗
Increasing the Strength of Aluminum-alloy Columns by Prestressing
A series of tests was made in which the column strength of 17ST tubing was increased as much as 50 percent by prestressing the tubing to 40,000 pounds per square inch in compression under conditions of support that prevented column failure at this stress. This prestressing achieves it's beneficial effects entirely by improving the compressive properties of the material, principally the proportional limit.
Holt, M↗
Understanding the X-ray Flaring from Eta Carinae
We quantify the rapid variations in X-ray brightness ("flares") from the extremely massive colliding wind binary Eta Carinae seen during the past three orbital cycles by RXTE. The observed flares tend to be shorter in duration and more frequent as periastron is approached, although the largest ones tend to be roughly constant in strength at all phases. Plausible scenarios include (1) the largest of multi-scale stochastic wind clumps from the LBV component entering and compressing the hard X-ray emitting wind-wind collision (WWC) zone, (2) large-scale corotating interacting regions in the LBV wind sweeping across the WWC zone, or (3) instabilities intrinsic to the WWC zone. The first one appears to be most consistent with the observations, requiring homologously expanding clumps as they propagate outward in the LBV wind and a turbulence-like powerlaw distribution of clumps, decreasing in number towards larger sizes, as seen in Wolf-Rayet winds.
Moffat, A.F.J.↗
Urethane/Silicone Adhesives for Bonding Flexing Metal Parts
Adhesives that are blends of commercially available urethane and silicone adhesives have been found to be useful for bonding metal parts that flex somewhat during use. These urethane/silicone adhesives are formulated for the specific metal parts to be bonded. The bonds formed by these adhesives have peel and shear strengths greater than those of bonds formed by double-sided tapes and by other adhesives, including epoxies and neat silicones. In addition, unlike the bonds formed by epoxies, the bonds formed by these adhesives retain flexibility. In the initial application for which the urethane/silicone adhesives were devised, there was a need to bond spring rings, which provide longitudinal rigidity for inflatable satellite booms, with the blades that provide the booms axial strength. The problem was to make the bonds withstand the stresses, associated with differences in curvature between the bonded parts, that arose when the booms were deflated and the springs were compressed. In experiments using single adhesives (that is, not the urethane/ silicone blends), the bonds were broken and, in each experiment, it was found that the adhesive bonded well with either the ring or with the blade, but not both. After numerous experiments, the adhesive that bonded best with the rings and the adhesive that bonded best with the blades were identified. These adhesives were then blended and, as expected, the blend bonded well with both the rings and the blades. The two adhesives are Kalex (or equivalent) high-shear-strength urethane and Dow Corning 732 (or equivalent) silicone. The nominal mixture ratio is 5 volume parts of the urethane per 1 volume part of the silicone. Increasing the proportion of silicone makes the bond weaker but more flexible, and decreasing the proportion of silicone makes the bond stronger but more brittle. The urethane/silicone blend must be prepared and used quickly because of the limited working time of the urethane: The precursor of the urethane adhesive is supplied in a two-part form, comprising a resin and a hardener that must be mixed. The resulting urethane adhesive has a working time of 3 to 5 minutes. To prepare the urethane/silicone blend, one must quickly add the silicone to the urethane adhesive and mix it in thoroughly within the working time of the urethane. Once the urethane/silicone blend has been mixed and applied to the bond surfaces, it takes about 2 hours for the adhesive to cure under pressure. However, it takes about 24 hours for the adhesive to reach full strength.
Edwards, Paul D.↗
Verification Studies for the Noh Problem using Non-ideal Equations of State and Finite Strength Shocks
We present that the Noh verification test problem is extended beyond the commonly studied ideal gamma-law gas to more realistic equations of state (EOSs) including the stiff gas, the Noble-Abel gas, and the Carnahan-Starling EOS for hard-sphere fluids. Self-similarity methods are used to solve the Euler compressible flow equations, which in combination with the Rankine-Hugoniot jump conditions provide a tractable general solution. This solution can be applied to fluids with EOSs that meet criterion such as it being a convex function and having a corresponding bulk modulus. For the planar case the solution can be applied to shocks of arbitrary strength, but for cylindrical and spherical geometries it is required that the analysis be restricted to strong shocks. Finally, the exact solutions are used to perform a variety of quantitative code verification studies of the Los Alamos National Laboratory Lagrangian hydrocode FLAG.
42 ENGINEERING↗
Laboratory Evaluation of the Thermal Breakout Method for Maximum Horizontal Stress Measurement
Measuring in situ stress is essential for many problems in geomechanics, and the maximum horizontal stress is the most difficult to constrain. We are developing an extension of the breakout method to measure maximum horizontal stress in regions where natural breakouts do not occur. In the novel thermal breakout method, additional compression which leads to breakout development is induced by heating the borehole wall. In the present study, we validated the method experimentally in a true-triaxial apparatus on samples with predrilled boreholes. Two rocks were selected for laboratory testing: high-porosity Berea sandstone and low-porosity Niagaran dolomite. Prior to main true-triaxial tests, we carried out standard testing to characterize the strength, elasticity and thermal properties. The true-triaxial experiments consisted of: (1) room-temperature tests where samples were first loaded mechanically until the breakout formed, and (2) elevated-temperature tests where samples were loaded mechanically within the elastic range with additional compression induced thermally. Breakout initiation was monitored by acoustic emission sensors mounted on the pistons that applied horizontal stresses. Furthermore, the magnitude of induced thermal stress was calculated from temperature measurements around the borehole wall. In both rock types, we created thermally induced breakouts and examined analytical expressions to constrain maximum horizontal stress based on strength, elastic and thermal properties of the rocks.
58 GEOSCIENCES↗
Thermal Effects on the Bearing Behavior of Composite Joints
Thermal effects on the pin-bearing behavior of an IM7/PET15 composite laminate are studied comprehensively. A hypothesis presents factors influencing a change in pin-bearing strength with a change in temperature for a given joint design. The factors include the change in the state of residual cure stress, the material properties, and the fastener fit with a change in temperature. Experiments are conducted to determine necessary lamina and laminate material property data for the IM7/PET15 being utilized in this study. Lamina material properties are determined between the assumed stress free temperature of 460 F down to -200 F. Laminate strength properties are determined for several lay-ups at the operating temperatures of 350 F, 70 F, and -200 F. A three-dimensional finite element analysis model of a composite laminate subject to compressive loading is developed. Both the resin rich layer located between lamina and the thermal residual stresses present in the laminate due to curing are determined to influence the state of stress significantly. Pin-bearing tests of several lay-ups were conducted to develop an understanding on the effect of temperature changes on the pin-bearing behavior of the material. A computational study investigating the factors influencing pin-bearing strength was performed. A finite element model was developed and used to determine the residual thermal cure stresses in the laminate containing a hole. Very high interlaminar stress concentrations were observed two elements away from the hole boundary at all three operating temperatures. The pin-bearing problem was modeled assuming a rigid frictionless pin and restraining only radial displacements at the hole boundary. A uniform negative pressure load was then applied to the straight end of the model. A solution, where thermal residual stresses were combined with the state of stress due to pin-bearing loads was evaluated. The presence of thermal residual stresses intensified the interlaminar stresses predicted at the hole boundary in the pin-bearing problem. This dissertation shows that changes in material properties drives pin-bearing strength degradation with increasing temperature.
Walker, Sandra Polesky↗
Sensitivity of the strength and toughness of concrete to the properties of the interfacial transition zone
We report Civil infrastructure is made primarily of concrete structures or components and therefore understanding durability and fracture behavior of concrete is of utmost importance. Concrete contains an interfacial transition zone (ITZ), a porous region surrounding the aggregates, that is often considered to be the weakest region in the concrete. The ITZ is poorly characterized and property estimates for the ITZ differ considerably. In this simulation study, representative concrete mesostructures are produced by packing coarse aggregates with realistic geometries into a mortar matrix. A meshless numerical method, peridynamics, is utilized to simulate the mechanical response including fracture under uniaxial compression and tension. The sensitivity of the stiffness and fracture toughness of the samples to the ITZ properties is computed, showing strong relationships between the ITZ properties and the effective modulus and effective yield strength of the concrete. These results provides insight into the influence of the poorly characterized ITZ on the stiffness and strength of concrete. This work showcases the applicability of peridynamics to concrete systems, matching experimental strength and modulus values. Additionally, relationships between the ITZ’s mechanical properties and the overall concrete strength and stiffness are presented to enable future design decisions.
36 MATERIALS SCIENCE↗
A limit to strong shock behavior in the dynamic response of matter at pressure
Solids under high pressures experience a series of regimes, where their microstructure adapts to the applied compression and these key transitions are discussed in this paper. As strain increases, new forces emerge at extreme pressures. A previous study introduced the concept of the weak shock limit (WSL), at which the ambient theoretical shear strength is overcome. Above the WSL, further deformation under strong shock conditions results in electrons occupying higher energy levels as strain increases. As pressure rises further, shock melting occurs in the material and at around three times this melting pressure, the strong shock limit is reached where the driving physics under pressure switches, with electrons forced into higher energy states. This leads to significant reduction in their compressibility due to changes in electronic structure and developing electron degeneracy pressures. A derivation for conditions at this state is presented, which indicates that a dependence of the threshold pressure on the free electron number density defines the limit observed. This correlation suggests that ambient material moduli govern material compression up to nearly 50% strain. These observations show that models should account for different behaviors as dominant physics changes in each regime accessed as shock pressure increases.
36 MATERIALS SCIENCE↗
Dynamic strength of iron under pressure-temperature conditions of Earth’s inner core
Iron (Fe) is a primary constituent of terrestrial planetary cores, yet its rheological properties under extreme conditions remain uncertain. Here we present direct measurements of Fe strength at 310-430 GPa pressures and 3700-5800 K temperatures, obtained using Rayleigh-Taylor (RT) instability experiments at the National Ignition Facility. Single-crystal α-Fe samples with [001] and [111] orientations are shock-ramp compressed past the α-ε transition along paths approaching Earth’s inner core conditions. We find that ε-Fe derived from [001] α-Fe is consistently stronger (11-20 GPa) than that from [111] α-Fe (8-18 GPa), contrary to the trend at ambient conditions. Large-scale molecular dynamics simulations reproduce this atypical strength anisotropy and attribute it to microstructural evolution during the phase transition and subsequent ε-phase plasticity. Ripple growth analysis further constrains viscosities of 100-170 Pa·s under the driven conditions. Our results provide experimental benchmarks for Fe rheology at inner-core conditions, with implications for seismic anisotropy and the geodynamo.
Condensed-matter physics↗