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DOE OSTI2014

On the sol-gel synthesis of strontium-titanate thin films and the prospects of their use in electronics

Strontium-titanate films obtained by the sol-gel technique are deposited onto silicon and silicon/oxide titanium/platinum substrates. The strontium-titanate phase is detected by the method of X-ray diffraction analysis after heat treatment at temperatures of 750 and 800°C. The thickness of the films obtained by the spin-on method increases from 50 to 250 nm as the number of deposited layers is increased and is accompanied with an increase in the grain size in the films. Prospects of the development of the sol-gel technique for the formation of film components of electronic devices based on SrTiO{sub 3} xerogels are discussed.

36 MATERIALS SCIENCE↗

NASA NTRS2015

Mapping the Region in the Nearest Star System to Search for Habitable Planets

Circumstellar planets within the alpha Centauri AB star system have been suggested through formation models and recent observations, and ACESat (Belikov et al. AAS Meeting #225, #311.01, 2015) is a proposed space mission designed to directly image Earth-sized planets in the habitable zones of both of these stars. The alpha Centauri system is billions of years old, so planets are only expected to be found in regions where their orbits are long-lived. We evaluate the extent of the regions within the alpha Centauri AB star system where small planets are able to orbit for billion-year timescales and we map the positions in the sky plane where planets on stable orbits about either stellar component may appear. We confirm the qualitative results of Wiegert & Holman (Astron. J. 113, 1445, 1997) regarding the approximate size of the regions of stable orbits, which are larger for retrograde orbits relative to the binary than for prograde orbits. Additionally, we find that mean motion resonances with the binary orbit leave an imprint on the limits of orbital stability, and the effects of the Lidov-Kozai mechanism are also readily apparent. Overall, orbits in the habitable zones near the plane of the binary are stable, whereas high-inclination orbits are short-lived.

alpha Centauri AB star system↗

NASA NTRS2014

Looking for a Source of Water in Martian Basltic Breccia NWA 7034

The recently described martian meteorite NWA 7034 has high water content compared to other SNC meteorites. Deuterium to hydrogen isotope ratio measurements indicates that there are two distinct delta-D components in NWA 7034, a low temperature (150-500degC) light component around -100per mille and a high temperature (300-1000degC) heavy component around +300per mille. NWA 7034 contains iron-rich phases that are likely secondary aqueous alteration products. They are commonly found as spheroidal objects of various sizes that are often rich in Fe-Ti oxides and possibly iron hydroxides. Iron oxides and oxyhydroxides are very common in weathered rocks and soils on Earth and Mars and they are important components of terrestrial and Martian dust. In NWA 7034 iron-rich phases are found throughout the fine-grained basaltic groundmass of the meteorite. The total amount of martian H2O in NWA 7034 is reported to be 6000 ppm, and in this study we attempt to determine the phase distribution of this H2O by texturally describing and characterizing hydrous phases in NWA 7034, using Fourier transform infrared spectrometry (FTIR) and transmission electron microscopy (TEM).

Muttik, N.↗

NASA NTRSDate not supplied

Theoretical and Simulated Capacity of Urban Air Mobility Airspace Characteristics

As interest in urban air mobility grows, as are the optimistic predictions for potentially hundreds of simultaneous operations within a given metropolitan airspace. This high density of traffic poses a challenge for safe, efficient, and timely operations, particularly when realistic airspace restrictions, fleet sizes, and fluctuating demand are considered. Routes for urban air mobility aircraft, similar to automotive roadways more than other types of airways, are one proposed solution for traffic management. This paper identifies several potential components of urban air mobility routes and compares their numerically predicted maximum capacity with what is achieved in a realistic simulation that includes airspace restrictions, parking limitations, fleet sizes, and uneven demand.

Urban Air Mobility↗

NASA NTRSDate not supplied

Theoretical and Simulated Capacity of Urban Air Mobility Airspace Characteristics

Urban Air Mobility↗

NASA NTRS2001

Status of the Direct Data Distribution (D(exp 3)) Experiment

NASA Glenn Research Center's Direct Data Distribution (D3) project will demonstrate an advanced, high-performance communications system that transmits information from an advanced technology payload carried by a NASA spacecraft in low Earth orbit (LEO) to a small receiving terminal on Earth. The space-based communications package will utilize a solid-state, K-band phased-array antenna that electronically steers the radiated energy beam toward a low-cost, tracking ground terminal, thereby providing agile, vibration-free, electronic steering at reduced size and weight with increased reliability. The array-based link will also demonstrate new digital processing technology that will allow the transmission of substantially increased amounts of latency-tolerant data collected from the LEO spacecraft directly to NASA field centers, principal investigators, or into the commercial terrestrial communications network. The technologies demonstrated by D3 will facilitate NASA's transition from using Government-owned communication assets to using commercial communication services. The hardware for D3 will incorporate advanced technology components developed under the High Rate Data Delivery (HRDD) Thrust Area of NASA's Office of Aerospace Technology Space Base Program at Glenn's Communications Technology Division. The flight segment components will include the electrically steerable phased-array antenna, which is being built by the Raytheon System Corporation and utilizes monolithic microwave integrated circuit (MMIC) technology operating at 19.05 GHz; and the digital encoder/modulator chipset, which uses four-channel orthogonal frequency division multiplexing (OFDM). The encoder/modulator will use a chipset developed by SICOM, Inc., which is both bandwidth and power efficient. The ground segment components will include a low-cost, open-loop tracking ground terminal incorporating a cryoreceiver to minimize terminal size without compromising receiver capability. The project is planning to hold a critical design review in the second quarter of fiscal year 2002.

Wald, Lawrence↗

DOE OSTI2022

Computational studies of structural, energetic, and electronic properties of pure Pt and Mo and mixed Pt/Mo clusters: Comparative analysis of characteristics and trends

The added technological potential of bimetallic clusters and nanoparticles, as compared to their pure (i.e., one-component) counterparts, stems from the ability to further fine-tune their properties and, consequently, functionalities through a simultaneous use of the “knobs” of size and composition. The practical realization of this potential can be greatly advanced by the knowledge of the correlations and relationships between the various characteristics of bimetallic nanosystems on the one hand and those of their pure counterparts as well as pure constituent components on the other hand. Here, in this study, we present results of a density functional theory based study of pure Pt n and Mo n clusters aimed at revisiting and exploring further their structural, electronic, and energetic properties. These are then used as a basis for analysis and characterization of the results of calculations on two-component Pt n-m Mo m clusters. The analysis also includes establishing relationships between the properties of the Pt n-m Mo m clusters and those of their Pt n-m and Mo m components. One of the particularly intriguing findings suggested by the calculated data is a linear dependence of the average binding energy per atom in sets of Pt n-m Mo m clusters that have the same fixed number m of Mo atoms and different number n-m of Pt atoms on the fractional content (n-m)/n of Pt atoms. We derive an analytical model that establishes the fundamental basis for this linearity and expresses its parameters—the m-dependent slope and intercept—in terms of characteristic properties of the constituent components, such as the average binding energy per atom of Mo m and the average per-atom adsorption energy of the Pt atoms on Mo m . The conditions of validity and degree of robustness of this model and of the linear relationship predicted by it are discussed.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

NASA NTRS1994

Residual strength of thin panels with cracks

The previous design philosophies involving safe life, fail-safe and damage tolerance concepts become inadequate for assuring the safety of aging aircraft structures. For example, the failure mechanism for the Aloha Airline accident involved the coalescence of undetected small cracks at the rivet holes causing a section of the fuselage to peel open during flight. Therefore, the fuselage structure should be designed to have sufficient residual strength under worst case crack configurations and in-flight load conditions. Residual strength is interpreted as the maximum load carrying capacity prior to unstable crack growth. Internal pressure and bending moment constitute the two major components of the external loads on the fuselage section during flight. Although the stiffeners in the form of stringers, frames and tear straps sustain part of the external loads, the significant portion of the load is taken up by the skin. In the presence of a large crack in the skin, the crack lips bulge out with considerable yielding; thus, the geometric and material nonlinearities must be included in the analysis for predicting residual strength. Also, these nonlinearities do not permit the decoupling of in-plane and out-of-plane bending deformations. The failure criterion combining the concepts of absorbed specific energy and strain energy density addresses the aforementioned concerns. The critical absorbed specific energy (local toughness) for the material is determined from the global specimen response and deformation geometry based on the uniaxial tensile test data and detailed finite element modeling of the specimen response. The use of the local toughness and stress-strain response at the continuum level eliminates the size effect. With this critical parameter and stress-strain response, the finite element analysis of the component by using STAGS along with the application of this failure criterion provides the stable crack growth calculations for residual strength predictions.

Madenci, Erdogan↗

DOE OSTI2015

Study of an unrefined humate solution as a possible remediation method for groundwater contamination - 15698

Savannah River Site (SRS) was one of the major nuclear processing facilities in the U.S. where plutonium was produced during the Cold War. Approximately 1.8 billion gallons of low level acidic waste solution containing radionuclides and dissolved metals were discharged to a series of unlined seepage basins at the F/H Area. Uranium is a key contaminant of concern in the basin's groundwater. It is migrating into the groundwater creating an acidic plume with a pH between 3-5.5. Groundwater Actions: The pump-and-treat water treatment unit was designed and built in 1997 to remove metals and radionuclides. In 2004 a hybrid funnel-and-gate system was constructed to create a treatment zone in which the acidic nature of the contaminated sediments could be reversed. Huma-K is an organic fertilizer that comes from the alkaline extraction of leonardite (a low-rank coal). Huma-K has a high content of humic substances which consist of complex organic compounds formed by the decomposition of plant and animal tissue. The objective of this study is to determine if a low cost unrefined humate solution (Huma-K) can be used to facilitate uranium adsorption to control its mobility in acidic groundwater. This study can assist in evaluating whether Huma-K can be used as an in situ amendment for the remediation of groundwater contaminated with uranium. Sediments from FAW-1 70-90 ft were used in this experiment. Sediments were disaggregated and sieved to a particle size of . 2 mm. Concentrations in the range 10-500 ppm were tested. Once all the components were added, pH was adjusted to 4. Samples were vortex mixed and placed on a shaker table at 100 RPM for a period of 24 hours in order to reach the adsorption equilibrium. Once the adsorption equilibrate was reached, samples were centrifuged at 2700 RPM to separate the liquid and the solid phase. The liquid fraction was analyzed using a Thermo Scientific Genesys 10S UV-Vis spectrophotometer. The same experimental design was used as explained above. A known concentration of Huma-K was used to study the pH effect on the sorption process. pH values were measured at the beginning and at the end of the experiment. Spectra of Huma-K show a featureless character. Absorbance of light increases as the wavelength is decreased. Measurements were done at 254 nm due to the presence of aromatic rings. Apparently there are two sorption processes. The first one follows the same trend as the Langmuir isotherm up to 250 ppm. The second sorption process occurs after all the binding sites in the sediments have been occupied. Precipitation decreases as the pH is increased. Based on the sorption isotherm, humic substances apparently bind first to the binding sites of the sediments particles. Once all the binding sites have been occupied, other sorption processes may start to dominate. Sorption is affected by pH. Higher sorption is seen at low pH values. Increased precipitation at low pH values is probably due to the neutralization of surface charges of humic molecules making them agglomerate.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

DOE OSTI2021

Compositional Control on Shale Pore Structure Characteristics across a Maturation Gradient: Insights from the Devonian New Albany Shale and Marcellus Shale in the Eastern United States

The pore structure characteristics of shales are controlled by their mineralogical and organic matter (OM) composition. However, the contributions by different components in shales at varying thermal maturities remain poorly understood. In this study, Devonian New Albany Shale and Marcellus Shale samples spanning a thermal maturity from marginally mature (vitrinite reflectance R o 0.55%) to post-mature (R o 2.41 %) were selected to study the control of composition on the pore structure properties of shales at different stages of thermal maturation. Scanning electron microscope (SEM) imaging was used to examine pore types in shales, and low-pressure N 2 and CO 2 adsorption analyses were used to quantitatively characterize the mesopore and micropore characteristics of bulk shales and major components in shales. The results show that matrix-associated pores including interparticle pores between silt-sized mineral grains, phyllosilicate framework pores, and intraparticle pores within mineral grains exist in all samples but become less common with increasing maturity, which is likely caused by elevated compaction, cementation, and occlusion with bitumen. Secondary organic pores were not observed under SEM at marginal maturity but were detected in the condensate–wet gas and dry gas windows, with more organic pores in the dry gas window. At marginal maturity, OM has large amounts of mesopores and micropores as demonstrated by low-pressure N 2 and CO 2 adsorption analyses of OM isolated from shales, even though no OM-hosted pores were observed under SEM. With increasing thermal maturity, the mesopore and micropore specific surface area of OM increase and make greater contributions to the pore structure properties of bulk shales. The mesopore and micropore properties of shales are controlled by OM content and maturity as well as by clay mineral type and content, and they can be estimated from the contribution of each component at different stages of thermal maturation. In conclusion, accurate evaluation of the pore volume and SSA of shales will have important implications for assessing gas adsorption and transport in shales.

03 NATURAL GAS↗

DOE OSTI2017

Fabrication, microstructure, and wear performance of WC-Fe composite/metal coating fabricated by resistance seam welding

Highlights: • WC-Fe/metal coating consisted of WC-Fe layer and metal interlayer was fabricated by resistance seam welding. • The microstructure, hardness and wear performance of coatings with different WC particles size were analyzed. • The wear mechanism of coatings showed huge difference following various sliding distance. - Abstract: WC-Fe composite/metal coatings consisting of a WC-Fe composite layer and a metal interlayer were successfully fabricated on an Al 6061 substrate by resistance seam welding. The microstructures and phase compositions of the WC-Fe composite/metal coatings with different WC particle sizes (nano, fine, and coarse) were investigated. The WC-Fe composite layer consisted of WC particles and a Fe-C-Si super hard alloy (SHA) component, whereas the metal interlayer was composed of SHA, FeAl{sub 3}, Fe{sub 2}Al{sub 5}, and Al 6061. The surface microhardness of the WC-Fe composite/metal coating increased with increasing WC particle size. The wear performance of the coatings tested with different sliding distances is discussed in detail. Coating-C (coarse) showed the best wear resistance. The wear rates of both coating-N (nano) and coating-C decreased as the sliding distance increased, while coating-F (fine) demonstrated the opposite behavior. The wear mechanisms of the coatings were drastically different owing to the significantly different WC particle behavior at various sliding distances.

36 MATERIALS SCIENCE↗

NASA NTRS1991

Neural network architecture for crossbar switch control

A Hopfield neural network architecture for the real-time control of a crossbar switch for switching packets at maximum throughput is proposed. The network performance and processing time are derived from a numerical simulation of the transitions of the neural network. A method is proposed to optimize electronic component parameters and synaptic connections, and it is fully illustrated by the computer simulation of a VLSI implementation of 4 x 4 neural net controller. The extension to larger size crossbars is demonstrated through the simulation of an 8 x 8 crossbar switch controller, where the performance of the neural computation is discussed in relation to electronic noise and inhomogeneities of network components.

Troudet, Terry P.↗

NASA NTRS2006

G2 Flywheel Module Design

Design of a flywheel module, designated the G2 module, is described. The G2 flywheel is a 60,000 RPM, 525 W-hr, 1 kW system designed for a laboratory environment; it will be used for component testing and system demonstrations, with the goal of applying flywheels to aerospace energy storage and integrated power and attitude control (IPACS) applications. G2 has a modular design, which allows for new motors, magnetic bearings, touchdown bearings, and rotors to be installed without a complete redesign of the system. This design process involves several engineering disciplines, and requirements are developed for the speed, energy storage, power level, and operating environment. The G2 rotor system consists of a multilayer carbon fiber rim with a titanium hub on which the other components mount, and rotordynamics analysis is conducted to ensure rigid and flexible rotor modes are controllable or outside of the operating speed range. Magnetic bearings are sized using 1-D magnetic circuit analysis and refined using 3-D finite element analysis. The G2 magnetic bearing system was designed by Texas A&M and has redundancy which allows derated operation after the loss of some components, and an existing liquid cooled two pole permanent magnet motor/generator is used. The touchdown bearing system is designed with a squeeze film damper system allowing spin down from full operating speed in case of a magnetic bearing failure. The G2 flywheel will enable module level demonstrations of component technology, and will be a key building block in system level attitude control and IPACS demonstrations.

Jensen, Ralph H.↗

DOE OSTI2018

Size Effect in the Phase Separation of Cr–W Solid Solutions

Size effects in phase transformations of nanoscale systems show up as significant changes in their phase diagram. Here, using a thermodynamic approach we demonstrate how the immiscibility region of Cr–W solid solutions is influenced by their particle size. For 40- and 70-nm-diameter particles, we consider two thermodynamically stable states with a core–shell configuration, differing in the composition of the core phase. It is shown that, in the nanometer range, one of these states becomes metastable and that the phase diagrams of the stable and metastable states differ significantly. Reducing the particle size leads to a decrease in the upper critical dissolution temperature (UCDP) by 300–400 K and marked changes in the mutual solubility of the components at temperatures comparable to the UCDP.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

NASA NTRS2011

Miniature Laser Magnetometer

A conceptual design has been developed for a miniature laser magnetometer (MLM) that will measure the scalar magnitude and vector components of near-Earth magnetic fields. The MLM incorporates a number of technical innovations to achieve high-accuracy and high-resolution performance while significantly reducing the size of the laser-pumped helium magnetometer for use on small satellites and unmanned aerial vehicles (UAVs). and electronics sections that has the capability of measuring both the scalar magnetic field magnitude and the vector magnetic field components. Further more, the high-accuracy scalar measurements are used to calibrate and correct the vector component measurements in order to achieve superior vector accuracy and stability. The correction algorithm applied to the vector components for calibration and the same cell for vector and scalar measurements are major innovations. The separate sensor and electronics section of the MLM instrument allow the sensor to be installed on a boom or otherwise located away from electronics and other noisy magnetic components. The MLM s miniaturization will be accomplished through the use of advanced miniaturized components and packaging methods for the MLM sensor and electronics. The MLM conceptual design includes three key innovations. The first is a new non-magnetic laser package that will allow the placement of the laser pump source near the helium cell sensing elements. The second innovation is the design of compact, nested, triaxial Braunbek coils used in the vector measurements that reduce the coil size by a factor of two compared to existing Helmholtz coils with similar field-generation performance. The third innovation is a compact sensor design that reduces the sensor volume by a factor of eight compared to MLM s predecessor.

Slocum, Robert↗

DOE OSTI2018

Locally coupled open subsystems: A formalism for affordable electronic structure calculations featuring fractional charges and size consistency

This manuscript introduces a methodology (within the Born-Oppenheimer picture) to compute electronic ground-state properties of molecules and solids/surfaces with fractionally occupied components. Given a user-defined division of the molecule into subsystems, our theory uses an auxiliary global Hamiltonian that is defined as the sum of subsystem Hamiltonians, plus the spatial integral of a second-quantized local operator that allows the electrons to be transferred between subsystems. This electron transfer operator depends on a local potential that can be determined using density functional approximations and/or other techniques such as machine learning. The present framework employs superpositions of tensor-product wave functions, which can satisfy size consistency and avoid spurious fractional charges at large bond distances. The electronic population of each subsystem is in general a positive real number and is obtained from wave-function amplitudes, which are calculated by means of ground-state matrix diagonalization (or matrix propagation in the time-dependent case). Furthermore, our method can provide pathways to explore charge-transfer effects in environments where dividing the molecule into subsystems is convenient and to develop computationally affordable electronic structure algorithms.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

NASA NTRS1987

Supersonic throughflow fans for high-speed aircraft

Increased need for more efficient long-range supersonic flight has revived interest in the supersonic throughflow fan as a possible component for advanced high-speed propulsion systems. A fan that can operate with supersonic inlet axial Mach numbers would reduce the inlet losses incurred in diffusing the flow from supersonic Mach numbers to a subsonic one at the fan face. In addition, the size and weight of an all-supersonic inlet will be substantially lower than those of a conventional inlet. However, the data base for components of this type is practically nonexistent. Therefore, in order to furnish the required information for assessing the potential for this type of fan, the NASA Lewis Research Center has begun a program to design, analyze, build, and test a fan stage that is capable of operating with supersonic axial velocities from inlet to exit. The objectives are to demonstrate the feasibility and potential of supersonic throughflow fans, to gain a fundamental understanding of the flow physics associated with such systems, and to develop an experimental data base for design and analysis code validation. A brief overview of past supersonic throughflow fan activities are provided; the technology needs discussed; the design of a supersonic throughflow fan stage, a facility inlet, and a downstream diffuser described; and the results from the analysis codes used in executing the design are presented. Also presented is an engine concept intended to permit establishing supersonic throughflow within the fan on the runway and maintaining the supersonic throughflow condition within the fan throughout the flight envelope.

Ball, Calvin L.↗

DOE OSTI2026

Innovative laser-based methods for monitoring fuel retention in ITER

This paper addresses the challenge of tritium inventory management in ITER and future fusion reactors, highlighting the importance of accurate tritium measurement and its spatial distribution within the vacuum vessel. Given ITER’s operational constraints, especially the limit on tritium retention, precise measurement is essential for both safety and regulatory compliance. To tackle these questions, the paper presents the T-monitor diagnostic system developed by Forschungszentrum Jülich, which uses Laser-Induced Desorption (LID) in combination with Diagnostic Residual Gas Analysis (DRGA) to measure hydrogen isotope concentrations on the surface of divertor tiles. The system integrates a high-power laser, advanced optical components, and a Fast Scanning Mirror Unit (FSMU) for accurate laser spot positioning with rapid response. Designed to measure in situ tritium retention, the diagnostic provides high-resolution spatial mapping, vital for evaluating detritiation strategies. The laser heating process increases the divertor surface temperature to 1600 K within the laser spot, promoting hydrogen isotope desorption. Accurate measurements require the precise control of laser parameters, including pulse duration and spot size, with a target relative accuracy of 20%. The optical design includes both in-vessel and ex-vessel components, such as durable high-reflectivity mirrors made of gold and copper, selected not only for their infrared performance but also for their transmission of visible wavelengths for observation purposes. To protect optical components from contamination, a pneumatic shutter is used.

Hydrogen isotopes↗