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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 1,711 records · Page 95

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DOE OSTI2017

Effect of quenching rate on the microstructure and mechanical behavior of Ce75Al21Ga4 glassy alloy

Highlights: • Structural and microstructural changes with respect to quenching rate have been reported. • Ribbons synthesized at slow cooling rate shows higher hardness and yield strength. • Study is focused on the correlation between quenching rate and mechanical behavior. • Metallic glass synthesized at faster quenching rate contains the highest shear band density. - Abstract: The present study deals with the structural and microstructural changes with respect to the quenching rate and their correlation with mechanical behavior of melt-spun Ce{sub 75}Al{sub 21}Ga{sub 4} glassy alloys. The ribbons of the alloy have been synthesized at different quenching rates obtained through different wheel speeds (44, 36, 29, 22 and 15 m/s). The glass forming indicators and mechanical properties have been investigated at different quenching rates. The higher quenching rate obtained through high wheel speed (44, 36 and 29 m/s) has led to phase separation giving rise to nano-amorphous domains in a glassy matrix while the lower quenching rate obtained through lower wheel speed (22 and 15 m/s) produces nano-crystalline grains with size ranges from 25 ± 1 to 120 ± 1 nm. It has been found that the size of the nano-amorphous domains decreases with decrease in wheel speed. The mechanical behavior has been studied using micro-indentation technique. The indentation test indicates that with the same chemical composition, the ribbons synthesized at slow quenching rate exhibits higher hardness and yield strength than those synthesized at faster quenching rate. The ribbons synthesized at 44 m/s contains the large free volume and has the highest shear band density.

36 MATERIALS SCIENCE↗

DOE OSTI2019

Quantifying the hydration structure of sodium and potassium ions: taking additional steps on Jacob's Ladder

The ability to reproduce the experimental structure of water around the sodium and potassium ions is a key test of the quality of interaction potentials due to the central importance of these ions in a wide range of important phenomena. In this study, we simulate the Na + and K + ions in bulk water using three density functional theory functionals: (1) the generalized gradient approximation (GGA) based dispersion corrected revised Perdew, Burke, and Ernzerhof functional (revPBE-D3) (2) the recently developed strongly constrained and appropriately normed (SCAN) functional (3) the random phase approximation (RPA) functional for potassium. We compare with experimental X-ray diffraction (XRD) and X-ray absorption fine structure (EXAFS) measurements to demonstrate that SCAN accurately reproduces key structural details of the hydration structure around the sodium and potassium cations, whereas revPBE-D3 fails to do so. However, we show that SCAN provides a worse description of pure water in comparison with revPBE-D3. RPA also shows an improvement for K + , but slow convergence prevents rigorous comparison. Finally, we analyse cluster energetics to show SCAN and RPA have smaller fluctuations of the mean error of ion–water cluster binding energies compared with revPBE-D3.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DOE OSTI2022

Integrated Capture and Conversion of CO 2 to Methanol (ICCCM) Process Technology - CRADA 449 (Final Report)

The goal of this project is to develop a prototype system that integrates the capture and catalytic hydrogenation of CO 2 into methanol in the same solvent. Ultimately, this integrated approach could provide a technology with projected reductions to capital and operating costs by at least 20% relative to a benchmark methanol synthesis via gas-phase CO 2 hydrogenation. There were five primary objectives for the project: 1. Optimize the selections of both the catalysts and the CO 2 capture solvents to achieve high conversion (>80%) and high selectivity (>90%) toward methanol in the targeted processing ranges (100-180°C, 1-60 bar). 2. Design a reactor system that provides a fixed catalyst surface area and high-efficiency heat exchange to assure compact modular processing. 3. Build and test a reactor system and demonstrate in a bench scale continuous flow system, and use the operating data to refine the comparison to existing conversion technologies. 4. Refine techno economic (TEA) and Tech-to-Market (TTM) analyses using the experimental data obtained from the bench-scale system. 5. Use the experimental data and TEA/TTM projections to develop a conceptual design for a pre-commercial system that targets a specific market opportunity.

09 BIOMASS FUELS↗

DOE OSTI2025

Sister Rod Destructive Examinations (FY23) Appendix B: Segmentation, Defueling, Metallographic Data and Total Cladding Hydrogen

As a part of the DOE-NE High Burnup Spent Fuel Data Project, Oak Ridge National Laboratory (ORNL) is performing destructive examinations (DEs) of high burnup (HBU) (>45 GWd/MTU) spent nuclear fuel (SNF) rods from the North Anna Nuclear Power Station operated by Dominion Energy. The SNF rods, called sister rods or sibling rods are all HBU and include four different kinds of fuel rod cladding: standard Zircaloy-4 (Zirc-4), low-tin (LT) Zirc-4, ZIRLO ® , and M5 ® . The DEs are being conducted to obtain a baseline of the HBU rod’s condition before dry storage and are focused on understanding overall SNF rod strength and durability. Both composite fuel and defueled cladding will be tested to derive material properties. Although the data generated can be used for multiple purposes, one primary goal for obtaining the post-irradiation examination data and associated measured mechanical properties is to support SNF dry storage licensing and relicensing activities by (1) addressing identified knowledge gaps and (2) enhancing the technical basis for post-storage transportation, handling, and subsequent disposition of the SNF. This report documents the status of the ORNL Phase 1 DE activities related to: Rough segmentation (RS), Defueling (DEF), DE.02 optical microscopy (MET), and DE.03, cladding total hydrogen measurements. It is a cumulative update to the FY22 status report.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

DOE OSTI2026

Testing Classical Properties from Quantum Data

Many properties of Boolean functions can be tested far more efficiently than the function itself can be learned. However, this dramatic advantage often disappears when testers are limited to random samples of ƒ instead of adaptively chosen queries to f. In this work we investigate the quantum version of this restriction: quantum algorithms that test properties of a Boolean function f solely from copies of either the function state |ƒ⟩ ∝ ∑ x |x, ƒ(x)⟩ or the phase state |(-1) ƒ ⟩ ∝ ∑ x (-1) ƒ(x) |x⟩. For monotonicity, symmetry, and triangle-freeness, we show passive quantum testers are unboundedly or super-polynomially better than their classical passive testing counterparts. They are competitive with classic query -based testers in each case. Our new testers use techniques beyond quantum Fourier sampling, and it turns out this is necessary: we show a certain class of bent functions can be tested from 𝒪(1) function states but has a sample complexity lower bound of 2 Ω(n) for any tester relying exclusively on Fourier and classical samples. Our passive quantum testers are competitive with classical query -based testers, but this isn't universal: we exhibit a testing problem that can be solved from 𝒪(1) classical queries but requires Ω(2 n/2 ) function state copies. The Forrelation problem provides a separation of the same magnitude in the opposite direction, so we conclude that quantum data and classical queries are "maximally incomparable" resources for testing. We also begin the study of lower bounds for testing from quantum data. For quantum monotonicity testing, we prove that the ensembles of [Goldreich et al., 2000; Black, 2024], which give exponential lower bounds for classical sample-based testing, do not yield any nontrivial lower bounds for testing from quantum data. New insights specific to quantum data will be required for proving copy complexity lower bounds for testing in this model.

Boolean Functions↗

NASA NTRS1972

Analytical design of sensors for measuring during terminal phase of atmospheric temperature planetary entry

An analytical study was conducted to develop a sensor for measuring the temperature of a planetary atmosphere from an entry vehicle traveling at supersonic speeds and having a detached shock. Such a sensor has been used in the Planetary Atmosphere Experiments Test Probe (PAET) mission and is planned for the Viking-Mars mission. The study specifically considered butt-welded thermocouple sensors stretched between two support posts; however, the factors considered are sufficiently general to apply to other sensors as well. This study included: (1) an investigation of the relation between sensor-measured temperature and free-stream conditions; (2) an evaluation of the effects of extraneous sources of heat; (3) the development of a computer program for evaluating sensor response during entry; and (4) a parametric study of sensor design characteristics.

Millard, J. P.↗

NASA NTRS1977

Results of phase change paint heat transfer test utilizing 0.040-scale 50% forebody models (no. 82-0) of the Rockwell International Space Shuttle Orbiter in AEDC VKF hypersonic tunnel B (test OH54B)

Aerodynamic heating phase change paint tests for the space shuttle orbiter are reported. The model was a 0.040 scale representation of the forward 50% of the orbiter. Surface roughness effects on boundary layer transition were investigated. The roughness was simulated by steel balls 0.020 and 0.025 inch in diameter and a 0.25 in. diameter hole simulating the forward ET attach socket. A nominal Mach number of was tested with unit Reynolds number varying from 0.75 x 1 million ft through 3.5x 1 million ft. Angle of attack was varied from 20 degrees to 40 degrees.

Dye, W. H.↗

NASA NTRS1985

X-ray satellite

The projected launch date has been delayed approx. 7 weeks from the planned launch date. The Engineering Model (EM) of the automatic measurement and control system (AMCS) is in the critical phase. The contract change no. 1 to the main contract has been signed. A new version of the welding seam location specifications for the wide field camera (WFC) was proposed by the WFC Consortium. The payload integration plan (PIP) has been signed. Production of the EM/QM prototype and ground station equipment has proceeded according to plan with the exception of some delays. Production of the EM equipment has begun. Preparations for the qualification tests of the EM/QM equipment and the integration of EM equipment has begun. The cause of the delay in the launch date include the combined effects of the postponement of the target date for the EM equipment, along with the fact that only a structural model is available.

Source record↗

NASA NTRS2004

Statistical Analysis of CMC Constituent and Processing Data

Ceramic Matrix Composites (CMCs) are the next "big thing" in high-temperature structural materials. In the case of jet engines, it is widely believed that the metallic superalloys currently being utilized for hot structures (combustors, shrouds, turbine vanes and blades) are nearing their potential limits of improvement. In order to allow for increased turbine temperatures to increase engine efficiency, material scientists have begun looking toward advanced CMCs and SiC/SiC composites in particular. Ceramic composites provide greater strength-to-weight ratios at higher temperatures than metallic alloys, but at the same time require greater challenges in micro-structural optimization that in turn increases the cost of the material as well as increases the risk of variability in the material s thermo-structural behavior. to model various potential CMC engine materials and examines the current variability in these properties due to variability in component processing conditions and constituent materials; then, to see how processing and constituent variations effect key strength, stiffness, and thermal properties of the finished components. Basically, this means trying to model variations in the component s behavior by knowing what went into creating it. inter-phase and manufactured by chemical vapor infiltration (CVI) and melt infiltration (MI) were considered. Examinations of: (1) the percent constituents by volume, (2) the inter-phase thickness, (3) variations in the total porosity, and (4) variations in the chemical composition of the Sic fiber are carried out and modeled using various codes used here at NASA-Glenn (PCGina, NASALife, CEMCAN, etc...). The effects of these variations and the ranking of their respective influences on the various thermo-mechanical material properties are studied and compared to available test data. The properties of the materials as well as minor changes to geometry are then made to the computer model and the detrimental effects observed using statistical analysis software. The ultimate purpose of this study is to determine what variations in material processing can lead to the most critical changes in the materials property. The work I have taken part in this summer explores, in general, the key properties needed In this study SiC/SiC composites of varying architectures, utilizing a boron-nitride (BN)

Fornuff, Jonathan↗

NASA NTRS2021

Phase Change Processes for Thermal Management Systems and Science Investigations

This white paper focuses on the scientific rationale and motivation for deploying phase change processes-based spacecraft thermal management systems for space missions [1,2]. Phase change processes need to be implemented in the design of various life support systems, sub-critical cryogenic and thermal control systems, taking advantage of the latent heat of phase change so as to significantly increase the heat transfer rate per unit fluid mass. Experimental data are critical to understanding gravitational effects on complex phase change processes using novel materials and working fluids. Experimental data can be acquired by either designing new testing platforms or performing experiments with simulant fluids on existing microgravity platforms. With the acquired data, theoretical flow physics models and numerical simulations can then be validated for use under long-duration microgravity conditions. The acquired data and validated models will enable the deployment of game-changing thermal management systems with remarkably improved efficiency and stability in heat acquisition, transport, and rejection for long-duration space missions.

Fluid mechanics↗

DOE OSTI2026

Study of the Protection Improvements for a Weak Grid Area With High Inverter-Based Resources (IBRs)

This project designs enhanced protection scheme for the real-world weak grid area with a high penetration of IBRs. As the existing protection schemes are originally designed for traditional synchronous machines, we first evaluate if the protection scheme will continue to operate reliably in systems with high levels of IBRs. Hardware relays are tested using a controller-hardware-in-the-loop setup. PSCAD electromagnetic transient simulation with IBR original equipment manufacturer black-box models is used to perform fault studies and generate COMTRADE data, which are replayed by a real-time digital simulator (RTDS) to feed input to the hardware relays. Three scenarios are analyzed: normal operation, an N-1 contingency, and an IBR-only scenario. The evaluation results reveal the following: 1) the protection scheme remains reliable under normal conditions and N-1 contingencies and 2) in IBR-only scenarios, differential protection (87L) continues to operate reliably, whereas local protection elements, such as distance and directional elements, fail because of the lack of regulated negative sequence current contributed by IBRs. Enhanced protection is designed to address the challenge of lack of negative sequence current from IBRs, including increased restraining factors a2 and k2 to block 32Q or using V instead QV ORDER for ground faults, enhanced mho distance element with voltage and phase angle supervision for L-L faults. The efficacy of enhanced protection logic is validated and proven to work reliably. Additionally, IEEE Std. 2800-2022 negative sequence current compliant GFL and GFM IBRs from another vendor are tested and proven to work reliably without need for enhanced logic. Therefore, this work provides valuable decision-making for utilities facing protection system challenges due to IBRs, either designing enhanced protection scheme or requesting their IBRs being IEEE Std. 2800-2022 compliant to produce regulated negative sequence current for protection relay to make correct decision.

24 POWER TRANSMISSION AND DISTRIBUTION↗

NASA NTRS1969

Test of sodium boiling in a single tube-in- shell heat exchanger over the range 1720 deg to 1980 deg F /1211 to 1355 K/

Sodium was boiled in a vertical, 1/2-inch (1.27-cm) inside diameter by 4-fOOt (1.22-m) long tube. The columbium alloy boiler operated at flow rates of 75 to 380 lbm/hr (9.4 to 48 g/sec) and up to 0.93 quality. Boiling performance depended on whether the inlet flow was two-phase or liquid. Two-phase momentum pressure drops were 1(1/2) times frictional drops. Qualities over 0.9 were obtained at some critical (burnout) boiling conditions. Liquid superheats up to 250° F (139 K) existed before initiation of boiling.

James P. Lewis↗

DOE OSTI2021

Testing the reliability of interpretable neural networks in geoscience using the Madden–Julian oscillation

Abstract. We test the reliability of two neural network interpretation techniques, backward optimization and layerwise relevance propagation, within geoscientific applications by applying them to a commonly studied geophysical phenomenon, the Madden–Julian oscillation. The Madden–Julian oscillation is a multi-scale pattern within the tropical atmosphere that has been extensively studied over the past decades, which makes it an ideal test case to ensure the interpretability methods can recover the current state of knowledge regarding its spatial structure. The neural networks can, indeed, reproduce the current state of knowledge and can also provide new insights into the seasonality of the Madden–Julian oscillation and its relationships with atmospheric state variables. The neural network identifies the phase of the Madden–Julian oscillation twice as accurately as a linear regression approach, which means that nonlinearities used by the neural network are important to the structure of the Madden–Julian oscillation. Interpretations of the neural network show that it accurately captures the spatial structures of the Madden–Julian oscillation, suggest that the nonlinearities of the Madden–Julian oscillation are manifested through the uniqueness of each event, and offer physically meaningful insights into its relationship with atmospheric state variables. We also use the interpretations to identify the seasonality of the Madden–Julian oscillation and find that the conventionally defined extended seasons should be shifted later by 1 month. More generally, this study suggests that neural networks can be reliably interpreted for geoscientific applications and may thereby serve as a dependable method for testing geoscientific hypotheses.

58 GEOSCIENCES↗

DOE OSTI2019

Extraction of Mercury Utilizing 3D Printed Media - Mercury Extraction Coalescer (MEC) (Revision 1)

The presence of mercury in environmental or industrial settings presents a number of issues from bio-accumulation to production of toxic by-products. The primary objective of this project was the development of a 3D printed component designed to act as a coalescing filter for the removal or segregation of elemental mercury from aqueous streams. The use of 3D printing allows for the design and integration of surface microstructures and internal geometries that could be difficult if not impossible to achieve through traditional manufacturing techniques. The initial phase of testing focused on the integration of 3D printed components into both environmental remediation testing (university subcontracted testing) and simulations of high-level nuclear waste processing (SRNL). Structures ranged from simple torturous paths that provided regions where the elemental mercury could settle out of the recirculation process to micro-structured frits that have increased surface area for aid in droplet coalescence and surface adsorption.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

NASA NTRS2008

Enabling and Enhancing Space Mission Success and Reduction of Risk through the Application of an Integrated Data Architecture

The engineering phases of design, development, test, and evaluation (DDT and E) and subsequent planning, preparation, and operation (Ops) of space vehicles in a complex and distributed environment requires massive and continuous flows of information across the enterprise and across temporal stages of the vehicle lifecycle. The resulting capabilities at each subsequent stage depend in part on the capture, preparation, storage, and subsequent provision of information from prior stages. The United States National Aeronautics and Space Administration (NASA) is currently designing a fleet of new vehicles that will replace the Space Shuttle and expand space operations and exploration capabilities. This includes the 2 stage human rated lift vehicle Ares 1 and its associated crew vehicle the Orion, and a service module; the heavy lift cargo vehicle, Ares 5, and an associated cargo stage known as the Earth Departure Stage; and a Lunar Lander vehicle that contains a descent stage, and ascent stage, and a habitation module. A variety of concurrent assorted ground operations infrastructure including software and facilities are also being developed, assorted technology and assembly designs and development for equipment such as EVA suits, life support systems, command and control technologies are also in the pipeline. The development is occurring in a distributed manner, with project deliverables being contributed by a large and diverse assortment of vendors and most space faring nations. Critical information about all of the components, software, and procedures must be shared during the DDT and E phases and then made readily available to the mission operations staff for access during the planning, preparation, and operations phases, and also need to be readily available for system to system interactions. The Constellation Data Systems Project (CxDS) is identifying the needs, and designing and deploying systems and processes to support these needs. This paper details the steps and processes that NASA is applying within the Constellation Program to manage this data and information, and to insure that the correct information is available, correctly annotated, and can be provisioned digitally to enhance response times, and support engineering analysis and anomaly resolution.

Brummett, Robert C.↗

DOE OSTI2017

Shock and Microstructural Characterization of the α-ω Phase Transition in Titanium Crystals

In this paper, a multicrystal comprised of a small number of large crystals of high-purity titanium and a [ 0001 ] oriented high-purity single crystal titanium sample were shock loaded using gas gun plate impact experiments. Tests were performed at stresses above the α − ω phase transition stress (for high-purity polycrystalline specimens) to observe the behavior of oriented crystals under similar conditions. Post-mortem characterization of the shocked microstructure was conducted on the single crystal sample to measure textures, and quantify phases and twinning. The apparent activation of plastic and transformation mechanisms was dependent upon crystal orientation. Specifically, the [ 0001 ] crystal showed a higher Hugoniot elastic limit than the [ 10 1 ¯ 0 ] or [ 3 1 ¯ 4 ¯ 4 ] orientations. The slope of velocity as a function of time was lower in the [ 0001 ] orientation than the other orientations during plastic deformation, indicating sluggish transformation kinetics for the α to ω phase transition for the [ 0001 ] oriented crystal. Finally, microtexture measurements of a recovered [ 0001 ] oriented single crystal revealed the presence of retained ω phase after unloading, with orientations of the constituent phase fractions indicative of the forward α→ω transition, rather than the reverse ω→α transition, suggesting that the material never achieved a state of 100% ω phase.

36 MATERIALS SCIENCE↗

DOE OSTI2022

Numerical modeling and parametric study of a dual purpose underground thermal battery

We report integrating thermal energy storage with building energy systems can enable flexible building electric demands at buildings to help mitigate the mismatch between electricity supply and demand. A novel building heating and cooling system that integrates a dual-source heat pump with hybrid thermal storage named dual-purpose underground thermal battery (DPUTB) has been developed for reshaping building electric demands. The proposed DPUTB integrated geothermal heat pump system is an original innovation that enables Grid-interactive Energy Efficient buildings. This paper focuses on the study of the novel DPUTB. The DPUTB works as both a thermal storage tank (an inner tank) and a ground heat exchanger (an outer tank separated from the inner tank by the insulation material). High fidelity and computationally effective models are needed to predict the performance of the novel DPUTB. This study has developed a simplified dynamic model for the DPUTB according to heat transfer and energy conservation principles and validated it by using experimental data obtained from testing a small-scale DPUTB apparatus. A parametric study was conducted to identify a design that can achieve the target thermal storage performance of load shift and energy efficiency. The parametric study results show that the inner tank shell thermal conductivity and the phase change material's melting point are the two most influencing factors on the performance of the DPUTB. One single full-size DPUTB with the identified design could provide 1-ton cooling (3.51 kW) with the supply temperature lower than 11 °C for 4 hours in summer after being fully charged in 8 hours. The inner tank filled with phase change material is for cooling thermal storage as a latent tank in the design. However, its capacity can be as high as 60 MJ as a sensible water tank for heating storage in winter. In the future study, the DPUTB model will be incorporated into the dual-source heat pump system for evaluating the overall system performance of demand side management in the long term.

25 ENERGY STORAGE↗

DOE OSTI2018

Central Appalachian Basin Unconventional (Coal/Organic Shale) Reservoir Small Scale CO 2 Injection Test

The Virginia Center for Coal and Energy Research (VCCER) project, “Injecting Carbon Dioxide into Unconventional Storage Reservoirs in the Central Appalachian Basin, with an Emphasis on Enhanced Coalbed Methane Recovery (ECBM), to Validate Prior Geological Characterization,” successfully completed two unique field projects: (1) a 510 ton scale ‘huff-and-puff’ carbon dioxide (CO 2 ) injection into a legacy horizontal Chattanooga Shale well in Morgan County, Tennessee and (2) a 13,263 ton CO 2 injection into 3 legacy coalbed methane (CBM) wells in Buchanan County, Virginia. The results from this Morgan County shale injection test confirm the injectivity and storage potential of CO 2 in organic shales formations while enhancing gas recovery. During the flowback phase, gas composition and flow rate were frequently monitored. Results indicated that there was a significant increase in gas flow rate during the first five months of the flowback phase and there was also a significant increase in gas quality, such that the percent composition of NGLs (natural gas liquids), including ethane, propane, and butane, increased. The primary objective of the research is to test the injectivity of CO 2 into unmineable coal seams and the potential for enhanced coalbed methane recovery (ECBM) by stressing the coals under continuous injection for a one-year period. The results from the Buchanan County ECBM test provided data to better understand the effect of matrix swelling, due to the adsorption of CO 2 on the coal surface, on injectivity and ECBM. During the greater than 13,000-ton injection, injectivity was maintained and coal swelling reduced by injecting into multiple wells at a moderate injection rate. Flowback has recently commenced and will be instrumental in determining the ECBM potential of central Appalachian coals and identifying commercialization opportunities.

03 NATURAL GAS↗