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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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NASA NTRSDate not supplied

The Marshall 100-Meter X-ray Beamline

The Marshall 100-Meter X-ray Beamline is a user facility for x-ray and EUV optics and instrumentation calibration, located at NASA’s Marshall Space Flight Center in Huntsville, Alabama. Also known as the Stray Light Test Facility, the Marshall-100 provides a range of focal plane detectors, x-ray sources, translation stages, cleanrooms, and high-vacuum level capability to the high-energy astrophysics community. Facility time is made available to Astronomy and Physics Research and Analysis (APRA) funded projects and is also available to the broader community upon request made to beamline management. The beamline has successfully been employed in the calibration of larger scope projects such as the Spectrum-Roentgen-Gamma Astronomical Roentgen Telescope X-ray Concentrator (ART-XC) telescope and the Small Explorer (SMEX) class Imaging X-ray Polarimetry Explorer (IXPE) Space Telescope. Additionally, the Marshall-100 is instrumental in supporting testing related to MSFC’s high-angular resolution optics development program.

X-ray Beamline, Test Facility, X-ray Calibration↗
NASA NTRS2002

MSFC ESL Facility and Beamline Studies

The poster presentation provides an overview of the MSFC ESL facility. The technical capabilities and accomplishments of the facility are summarized. Future plans including the development of a pressurized processing chamber and additional high-energy X-ray beamline studies are outlined.

Rogers, J. R.↗
NASA NTRS2005

Beamline Electrostatic Levitator (BESL) for in-situ High Energy K-Ray Diffraction Studies of Levitated Solids and Liquids at High Temperature

Determinations of the phase formation sequence, the crystal structures and the thermodynamic properties of materials at high temperatures are difficult because of contamination from the sample container and environment. Containerless processing techniques, such as electrostatic (ESL), electromagnetic (EML), aerodynamic, and acoustic levitation, are most suitable these studies. An adaptation of ESL for in-situ structural studies of a wide range of materials, including metals, semiconductors, insulators using high energy (125 keV) synchrotron x-rays is described here. This beamline ESL (BESL) allows the in-situ determination of the atomic structures of equilibrium solid and liquid phases, including undercooled liquids, as well as real-time studies of solid-solid and liquid-solid phase transformations. The use of image plate (MAR345) or GE-Angio detectors enables fast (30 ms - 1s) acquisition of complete diffraction patterns over a wide q-range (4 - 140/mm). The wide temperature range (300 - 2500 K), containerless processing under high vacuum (10(exp -7) - 10(exp -8) torr), and fast data acquisition, make BESL particularly suitable for phase diagram studies of high temperature materials. An additional, critically important, feature of BESL is the ability to also make simultaneous measurement of a host of thermo-physical properties, including the specific heat, enthalpy of transformation, solidus and liquidus temperatures, density, viscosity, and surface tension; all on the same sample and simultaneous with the structural measurements.

Gangopadhyay, A. K.↗
NASA NTRS2010

Radiation Beamline Testbeds for the Simulation of Planetary and Spacecraft Environments for Human and Robotic Mission Risk Assessment

The Center for Radiation Engineering and Science for Space Exploration (CRESSE) at Prairie View A&M University, Prairie View, Texas, USA, is establishing an integrated, multi-disciplinary research program on the scientific and engineering challenges faced by NASA and the international space community caused by space radiation. CRESSE focuses on space radiation research directly applicable to astronaut health and safety during future long term, deep space missions, including Martian, lunar, and other planetary body missions beyond low earth orbit. The research approach will consist of experimental and theoretical radiation modeling studies utilizing particle accelerator facilities including: 1. NASA Space Radiation Laboratory (NSRL) at Brookhaven National Laboratory; 2. Proton Synchrotron at Loma Linda University Medical Center; and 3. Los Alamos Neutron Science Center (LANSCE) at Los Alamos National Laboratory. Specifically, CRESSE investigators are designing, developing, and building experimental test beds that simulate the lunar and Martian radiation environments for experiments focused on risk assessment for astronauts and instrumentation. The testbeds have been designated the Bioastronautics Experimental Research Testbeds for Environmental Radiation Nostrum Investigations and Education (BERT and ERNIE). The designs of BERT and ERNIE will allow for a high degree of flexibility and adaptability to modify experimental configurations to simulate planetary surface environments, planetary habitats, and spacecraft interiors. In the nominal configuration, BERT and ERIE will consist of a set of experimental zones that will simulate the planetary atmosphere (Solid CO2 in the case of the Martian surface.), the planetary surface, and sub-surface regions. These experimental zones can be used for dosimetry, shielding, biological, and electronic effects radiation studies in support of space exploration missions. BERT and ERNIE are designed to be compatible with the experimental areas associated with the above facilities. CRESSE has broad expertise in space radiation in the areas of space radiation environment modeling, Monte-Carlo radiation transport modeling, space radiation instrumentation and dosimetry, radiation effects on electronics, and multi-functional composite shielding materials. The BERT and ERNIE testbeds will be utilized in individual and collaborative research incorporating this expertise. The research goal is to maximize the technical readiness level (TRL) of radiation instrumentation for human and robotic missions, optimizing the return value of CRESSE for NASA exploration and international co-operative missions. Outcomes and knowledge from research utilizing BERT and ERNIE will be applied to a variety of scientific and engineering disciplines vital for safe and reliable execution of future space exploration missions, which can be negatively impacted by the space radiation environment. The testbeds will be central to a variety of university educational activities and educational goals of NASA. Specifically, BERT and ERNIE will enhance educational opportunities in science, technology, engineering and mathematics (STEM) disciplines for engineering and science students at PVAMU, a historically black college/university. Preliminary data on prototype testbed configurations, including simulated lunar regolith (JSC-1A stimulant based on Apollo 11 samples), regolith/polyethylene composites, and dry ice, will be presented to demonstrate the usefulness of BERT and ERNIE in radiation beam line experiments.

Wilkins, Richard↗
NASA NTRS2017

Synthesis of Ti Oxides at Reducing Conditions: Implications for Beamline Standards and Cosmochemistry

These initial experiments demonstrate the great potential for synthesizing customized compounds for use as standards, or in buffering experiments at reducing conditions. We are also investigating Cr and V oxides, as well as compounds containing these elements such as FeV2O4 and FeCr2O4. Oxygen fugacity exerts a major control on mineral major element chemistry and elemental valence of minerals in any plane-tary compositional system [1]. For Earth, Fe is multivalent ranging from nearly Fe0 at low fO2 in the deep mantle to Fe2+ to Fe3+ at high low fO2. For solar nebular and meteoritic materials fO2 ranges from near IW to ~10 log fO2 units below the IW buffer [1]. Phases in CAIs, for example, contain no Fe2+, but may contain Ti4+, Ti3+, or Ti2+, and Cr3+ or Cr2+, and V3+ or V2+ [1,2,3]. De-tailed study of inclusions may reveal important differences in fO2 thus reflecting different environments in the solar nebula [4]. XANES, FEG-SEM, and TEM can reveal such variations in micro and nano samples such as Stardust and cosmic dust particles [5], but successful application to reduced conditions depends upon the availability of well characterized standards. Acquiring appropriate standards for reduced phases that contain Ti3+ or Ti2+, Cr3+ or Cr2+, and V3+ or V2+ can be a challenge. Here we report our preliminary results at synthesizing reduced Ti bearing standards, and focus on the preliminary characterization.

Righter, K.↗
NASA NTRS1994

Performance Report: A timeline for the synchrotron calibration of AXAF

Presented herein are the known elements of the timeline for synchrotron reflectance calibrations of HRMA witness samples (Section 2). In Section 3, lists of measurements to be done on each witness flat are developed. The elements are then arranged into timelines for the three beamlines we expect to employ in covering the full 50-12,000 eV energy range (Section 4). Although the required AXAF operational range is only 0.1-10 keV, we must calibrate the extent to which radiation just outside this band may contaminate our in-band response. In Section 5, we describe the working relationships which exist with each of the beamlines, and estimate the time available for AXAF measurements on each. From the timelines and the available time, we calculate the number of flats which could be measured in full detail over the duration of the program for each beamline. A suggestion is made regarding a minimum required baselines of witness flats from each element coating run or qualification run to be used in the calibration. We intend that this suggestion open discussion of the issue of witness flat deployment.

Tananbaum, H. D.↗
NASA NTRS1993

UV/VUV radiometric calibrations at SURF II

Since 1981 more than 150 instrument calibrations have been performed on the radiometric instrumentation calibration beamline at the Synchrotron Ultraviolet Radiation Facility (SURF II) at the National Institute of Standards and Technology (NIST) in Gaithersburg, Maryland. This 300 MeV electron storage ring operates routinely at electron currents greater than 250 mA. The spectrometer calibration beamline provides a continuum of radiation from 4 nm through the visual spectral region in the form of an intense beam with total angular divergence of 1.2 mrad. The probable uncertainty for the flux ranges from about 5 percent at 4 nm to less than 2 percent above 20 nm. The new system will radiometrically trace to SURF II, and thus is expected to reduce the calibration uncertainty for diodes in this region by a factor of five to the 1-2 percent level.

Furst, Mitchell L.↗
NASA NTRS1996

Trace Element Abundance Measurements on Cosmic Dust Particles

The X-Ray Microprobe on beamline X-26A at the National Synchrotron Light Source (NSLS) at Brookhaven National Laboratory was used to determine the abundances of elements from Cr through Sr in individual interplanetary dust particles (IDPs) collected from the Earth's stratosphere and the Scanning Transmission X-ray Microscope (STXM) on beamline X-1A at the NSLS was used to determine the carbon abundances and spatial distributions in IDPs. In addition, modeling was performed in an attempt to associate particular types of IDPs with specific types of parent bodies, and thus to infer the chemistry, mineralogy, and structural properties of those parent bodies.

Flynn, George↗
NASA NTRS2008

Role of Hf on Phase Formation in Ti45Zr(38-x)Hf(x)Ni17 Liquids and Solids

Hafnium and zirconium are very similar, with almost identical sizes and chemical bonding characteristics. However, they behave differently when alloyed with Ti and Ni. A sharp phase formation boundary near 18-21 at.% Hf is observed in rapidly-quenched and as-cast Ti45Zr38-xHfxNi17 alloys. Rapidly-quenched samples that contain less than 18 at.% Hf form the icosahedral quasicrystal phase, whiles samples containing more than 21 at.% form the 3/2 rational approximant phase. In cast alloys, a C14 structure is observed for alloys with Hf lower than the boundary concentration, while a large-cell (11.93 ) FCC Ti2Ni-type structure is found in alloys with Hf concentrations above the boundary. To better understand the role of Hf on phase formation, the structural evolution with supercooling and the solidification behavior of liquid Ti45Zr38-xHfxNi17 alloys (x=0, 12, 18, 21, 38) were studied using the Beamline Electrostatic Levitation (BESL) technique using 125keV x-rays on the 6ID-D beamline at the Advanced Photon Source, Argonne National Laboratory. For all liquids primary crystallization was to a BCC solid solution phase; interestly, an increase in Hf concentration leads to a decrease in the BCC lattice parameter in spite of the chemical similarity between Zr and Hf. A Reitveld analysis confirmed that as in the cast alloys, the secondary phase that formed was the C14 below the phase formation boundary and a Ti2Ni-type structure at higher Hf concentrations. Both the liquidus temperature and the reduced undercooling change sharply on traversing the phase formation boundary concentration, suggesting a change in the liquid structure. Structural information from a Honeycutt-Anderson index analysis of reverse Monte Carlo fits to the S(q) liquid data will be presented to address this issue.

Wessels, V.↗
NASA NTRS2012

Computational Transport Modeling of High-Energy Neutrons Found in the Space Environment

The high charge and high energy (HZE) particle radiation environment in space interacts with spacecraft materials and the human body to create a population of neutrons encompassing a broad kinetic energy spectrum. As an HZE ion penetrates matter, there is an increasing chance of fragmentation as penetration depth increases. When an ion fragments, secondary neutrons are released with velocities up to that of the primary ion, giving some neutrons very long penetration ranges. These secondary neutrons have a high relative biological effectiveness, are difficult to effectively shield, and can cause more biological damage than the primary ions in some scenarios. Ground-based irradiation experiments that simulate the space radiation environment must account for this spectrum of neutrons. Using the Particle and Heavy Ion Transport Code System (PHITS), it is possible to simulate a neutron environment that is characteristic of that found in spaceflight. Considering neutron dosimetry, the focus lies on the broad spectrum of recoil protons that are produced in biological targets. In a biological target, dose at a certain penetration depth is primarily dependent upon recoil proton tracks. The PHITS code can be used to simulate a broad-energy neutron spectrum traversing biological targets, and it account for the recoil particle population. This project focuses on modeling a neutron beamline irradiation scenario for determining dose at increasing depth in water targets. Energy-deposition events and particle fluence can be simulated by establishing cross-sectional scoring routines at different depths in a target. This type of model is useful for correlating theoretical data with actual beamline radiobiology experiments. Other work exposed human fibroblast cells to a high-energy neutron source to study micronuclei induction in cells at increasing depth behind water shielding. Those findings provide supporting data describing dose vs. depth across a water-equivalent medium. This poster presents PHITS data suggesting an increase in dose, up to roughly 10 cm depth, followed by a continual decrease as neutrons come to a stop in the target.

Cox, Brad↗
NASA NTRS2017

Effect of Tube-Based X-Ray Microtomography Imaging on the Amino Acid and Amine Content of the Murchison CM2 Chondrite

X-ray and synchrotron X-ray micro-computed tomography (micro-CT) are increasingly being used for three dimensional reconnaissance imaging of chondrites and returned extraterrestrial material prior to detailed chemical and mineralogical analyses. Although micro-CT imaging is generally considered to be a non-destructive technique since silicate and metallic minerals in chondrites are not affected by X-ray exposures at the intensities and wavelengths typically used, there are concerns that the use of micro-CT could be detrimental to the organics in carbonaceous chondrites. We recently conducted a synchrotron micro-CT experiment on a powdered sample of the Murchison CM2 carbonaceous chondrite exposed to a monochromatic high energy (approximately 48 kiloelectronvolts) total X-ray radiation dose of approximately 1 kilogray (kGy) using the Advanced Photon Source beamline 13-BMD (13-Bending Magnet-D Beamline) at Argonne National Laboratory and found that there were no detectable changes in the amino acid abundances or enantiomeric compositions in the chondrite after exposure relative to a Murchison control sample that was not exposed. However, lower energy bremsstrahlung X-rays could interact more with amino acids and other lower molecular weight amines in meteorites. To test for this possibility, three separate micro-CT imaging experiments of the Murchison meteorite using the GE Phoenix v/tome/x s 240 kilovolt microfocus high resolution tungsten target X-ray tube instrument at the American Museum of Natural History (AMNH) were conducted and the amino acid abundances and enantiomeric compositions were determined. We also investigated the abundances of the C1-C5 amines in Murchison which were not analyzed in the first study.

Microtomography Imaging↗
NASA NTRS2018

Ground-Based X-Ray Calibration of the Astro-H/Hitomi Soft X-Ray Telescopes

We present the summary of the on-ground calibration of two soft x-ray telescopes (SXT-I and SXT-S), developed by NASA's Goddard Space Flight Center (GSFC), onboard Astro-H/Hitomi. After the initial x-ray measurements with a diverging beam at the GSFC 100-meter beamline, we performed the full calibration of the x-ray performance, using the 30-meter x-ray beamline facility at the Institute of Space and Astronautical Science of Japan Aerospace Exploration Agency in Japan. We adopted a raster scan method with a narrow x-ray pencil beam with a divergence of approximately 15 arc secs. The on-axis effective area (EA), half-power diameter, and vignetting function were measured at several energies between 1.5 and 17.5 kiloelectronvolts. The detailed results appear in tables and figures in this paper. We measured and evaluated the performance of the SXT-S and the SXT-I with regard to the detector-limited field-of-view and the pixel size of the paired flight detector, i.e., SXS and the SXI, respectively. The primary items measured are the EA, image quality, and stray light for on-axis and off-axis sources. The accurate measurement of these parameters is vital to make the precise response function of the ASTRO-H SXTs. This paper presents the definitive results of the ground-based calibration of the ASTRO-H SXTs.

Iizuka, Ryo↗
NASA NTRS2018

Analysis of the NGXO Telescope X-Ray Hartmann Data

Next Generation X-Ray Optics (NGXO) team at the Goddard Space Flight Center (GSFC) has been developing a new silicon-based grazing incidence mirror technology for future high resolution x-ray astronomical missions. Recently, the GSFC team completed the construction of first few mirror modules that contain one pair of mirrors. One of the mirror pairs was tested in GSFC 600-m long beamline facility and Panter (Neuried, Germay) 120-m long x-ray beamline facility. Both full aperture x-ray tests, Hartmann tests, and focal plane sweeps were completed. In this paper we present the data analysis process and compare the results from our models to measured x-ray centroid data, x-ray performance data, and out of focus images of the mirror pair.

Spaceborne telescopes↗