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At least 19 records

Mode I tensile fracture behavior of adhesively-bonded metal–metal, metal–CFRP, and CFRP–CFRP bi-material combinations analyzed by size effect method

Understanding the adhesive and interfacial fracture is important for developing and achieving better adhesive jointing in bi-materials, the location which becomes less vulnerable in engineered structure components. Still, to characterize the fracturing behavior of various adhesively-bonded materials, it was shown in this work that the Mode I fracture energies estimated from conventional methods (e.g., work-of-fracture, (modified) compliance calibration method, (modified) beam theory, etc.) can be strongly affected by adherent thickness, adhesive bond length, and material type. Consequently, this hindered the proper understanding of fracturing in adhesive jointing of bi-materials since the estimated fracture energies can exhibit unreasonable difference among various material combinations, thus leading to the confusion in the literature due to the unfair comparison on these non-objective results estimated by leveraging conventional methods on the specimens with different geometries. This work compared size effect method with conventional methods on the calculation of the Mode I fracture energies of metal-metal, metal-CFRP, and CFRP-CFRP material combinations via Double Cantilever Beam (DCB) tests. The results showed that the estimated fracture energies of various material combinations are not dependent on the specimen geometries. This aspect allowed the fair comparison particularly on the interfacial fracturing between metal/adhesive and CFRP/adhesive, and the difference was further explained and correlated with the damage morphology on the material surface after failure identified through three-dimensional profilometer.

36 MATERIALS SCIENCE↗

A study of adhesive bonding in metal–metal, metal–CFRP, and CFRP–CFRP material combinations under shear deformation: Fracture morphologies and damage mechanisms

Safe design of adhesive joining in multi-materials in engineered structures requires the accumulation of numerous experimental data on the failure behavior of various adhesively-bonded material combinations under different loading conditions. The deep understanding of mechanical performance, fracturing morphologies, and main damage mechanisms is also quintessential for accelerating the development of proper physics-based and multi-scale models for assisting the design. Towards this goal, this work presents a comprehensive characterization of the failure behavior of adhesively-bonded metal–metal, metal–CFRP, and CFRP–CFRP material combinations under global shear deformation via single lap shear testing. Thanks to a synergistic combination of measurement methods by using Digital Imaging Correlation (DIC) and 3D optical profilometry, adhesive features on the adherend after failure were quantified and the main progressive damage mechanisms were identified. The characterization performed in this work provides quantitative data that contributes to a better understanding of shear failure in adhesive bonding across different bi-material combinations. Finally, the obtained results have practical implications, including the potential to enhance adhesive bonding design, identify failure causes in adhesive joints, and develop or validate computational models capable of capturing the observed behavior in various adhesively-bonded materials under global shear deformation.

36 MATERIALS SCIENCE↗

Development of NDE/NDT Tools for High-Volume & High-Speed Inspection of CFRP Structures in Automotive Manufacturing

Main advantages of the air-coupled ultrasound testing (ACUT) and electromagnetic testing (EMT) techniques for NDE of CFRP composites were non-contact sensing, scalability for high-speed inspection, cost-effectiveness, and non-hazardous operation. Despite these advantages, no systems that would satisfy the project requirements were commercially available. Hence, one of the major efforts of the Michigan State University (MSU) team at the initial stage of the project was to close this technological gap by developing, optimizing, and validating array sensors that would provide sufficient sensitivity, spatial coverage, and resolution for robust defect detection. Optimization of the ACUT and EMT sensor designs was performed using experimentally validated finite element models. Initial experiments using array probes were conducted on relatively flat CFRP samples. In parallel, the MSU team designed and assembled a portable platform with two robotic arms. The robots were equipped with newly designed sensors that enabled high-speed NDE of curved CFRP parts. Presently, the developed robotic platform can be used as a demo/template NDE system, which is easily adaptable to manufacturing environments and in-line NDE. The ACUT NDE system developed by the MSU team used a high-power 4-channel pulser receiver for parallel data acquisition. The array probes were designed by stacking commercially available ACUT transducers, which operated in the frequency range between 100 kHz and 500 kHz. MSU optimized the excitation procedure and developed wave focusing cones so as to reduce the crosstalk between the transducers and to provide higher pulse repletion frequency (PRF). The through-transmission (TT) and single-side access (SSA) inspection modes were successfully implemented. In the TT-ACUT, structural defects in CFRP were detected by passing ultrasonic waves through the test part. Hence, the ACUT transmitters and receivers needed to be placed on the opposite sides of the test part. In the SSA-ACUT, guided waves (GW) were excited in the test part using the transmitters and were sensed by the receivers from the same side. Multi-channel TT-ACUT and SSA-ACUT provided high-speed NDE, and were successfully validated on CFRP test samples with interlaminar delaminations and other embedded defects The EM techniques developed by the MSU team included: 1) eddy current testing (ECT), 2) capacitive imaging (CI) and hybrid dual-mode imaging. In ECT, structural damage was detected in CFRP using coils sensor arrays. In ECT, the excitation magnetic field is generated by passing an alternating current through a coil, which is placed above the test sample. The excitation field penetrates the conductive sample and induces the eddy currents in its transect. In turn, the eddy currents generate the reaction field, which affects the total field sensed by a coil. Hence, the presence of structural flaws will alter the eddy current flow and the picked-up signal. ECT is mostly sensitive to local changes of the electric conductivity of the test sample, and CFRPs are mostly conductive in the direction of carbon fibers. Hence, ECT was well suited for the detection of fiber damage/fiber irregularities. The MSU team developed printed circuit boards (PCB) with coil sensor arrays optimized for NDE of CFRP. Unlike most commercial probes designed for ECT of metallic structures, the MSU array probes were designed for operation in [1-10] MHz frequency range, which was optimal for low-conductive CFRP. Multiple sensing topologies (coil groups excitation/sensing arrangements) were implemented and successfully validated. Capacitive Imaging (CI) technique developed by MSU was complementary to ECT. In contrast to ECT, which was sensitive to local changes of the electrical conductivity, the CI was sensitive to local changes of the dielectric constant. Therefore, CI could provide information about matrix damage/matrix irregularities in CFRP. The MSU CI sensor arrays were made of multiple circular or rectangular open-plate capacitors printed on PCB. Sensors of this type are not commercially available. In addition to ECT and CI, the MSU team developed a hybrid (dual-mode) inductive/capacitive measurement technique that synergistically combined the benefits of inductive and capacitive sensing for rapid NDE of fiber reinforced polymer (FRP) composite structures. Fiber damage and fiber irregularities in FRPs were detected by configuring hybrid sensors as coil sensors. Similarly, matrix damage, matrix irregularities and interlaminar delaminations were detected by configuring hybrid sensors as capacitive sensors. ECT and CI were performed sequentially by means of electronic switching. Hence, eliminating the need for mounting two separate sensor arrays on the probe. Portable robotic platform was developed by MSU for multi-technique high-speed NDE of CFRP test parts. The platform had two 6-axis robots, which enabled inspection of curved parts in approximately a 6×6×6 ft 3 active scan area. On the software side, the MSU team integrated scripts for NDE hardware control with scripts for robot motion control. MSU also implemented automated path planning for the robots, reconstruction of part’s surfaces via stereovision, 3D rendering of inspection data, and image processing algorithms for enhanced defect detection. Automotive composite parts manufactured by Plasan Composites from Phase I were used to validate the ACUT and EMT techniques on representative testbeds. Among those parts were three X-braces for a Dodge Viper, one composite calibration plaque with known defects at known locations, and four other test sections, including sections from a front splitter, a corner section from a composite hood, and a high-pressure RTM panel made using non crimp fabric. Other test samples included CFRP and GFRP calibration plates with fiber/matrix defects fabricated at MSU/CVRC.

36 MATERIALS SCIENCE↗

Multiscale Modeling of Carbon Fiber Reinforced Polymer (CFRP) for Integrated Computational Materials Engineering Process

In this work, a multiscale modeling framework for CFRP is introduced to study hierarchical structure of CFRP. Four distinct scales are defined: nanoscale, microscale, mesoscale, and macroscale. Information at lower scales can be passed to higher scale, which is beneficial for studying effect of constituents on macroscale part’s mechanical property. This bottom-up modeling approach enables better understanding of CFRP from finest details. Current study focuses on microscale and mesoscale. Representative volume element is used at microscale and mesoscale to model material’s properties. At microscale, unidirection CFRP (UD) RVE is used to study properties of UD. The UD RVE can be modeled with different volumetric fraction to encounter non-uniform fiber distribution in CFRP part. Such consideration is important in modeling uncertainties at microscale level. Currently, we identified volumetric fraction as the only uncertainty parameters in UD RVE. To measure effective material properties of UD RVE, periodic boundary conditions (PBC) are applied to UD RVE to ensure convergence of obtained properties. Properties of UD is directly used at mesoscale woven RVE modeling, where each yarn is assumed to have same properties as UD. Within woven RVE, there can be many potential uncertainties parameters to consider for a physical modeling of CFRP. Currently, we will consider fiber misalignment within yarn and angle between wrap and weft yarns. PBC is applied to woven RVE to calculate its effective material properties. The effect of uncertainties are investigated quantitatively by Gaussian process. Preliminary results of UD and Woven study are analyzed for efficacy of the RVE modeling. This work is considered as the foundation for future multiscale modeling framework development for ICME project.

Composite, ICME, Multiscale Modeling↗

Evaluating the Lightning Strike Damage Tolerance for CFRP Composite Laminates Containing Conductive Nanofillers

Conductive nanofillers, such as carbon nanotube, graphene nanoplatelets, and carbon black particles (with diameters in nanometers) have been shown to enhance the electrical conductivity of fiber reinforced polymer matrix composites in many existing studies. The motivation is primarily for lightning strike protection, electromagnetic interference shielding, de-icing, and the manufacturing of lightweight electronic components. Here, we evaluate the lightning strike damage tolerance of carbon fiber reinforced polymer (CFRP) matrix composite laminates containing conductive nanofillers with varying weight fractions, including carbon black (CB), carbon nanotubes (CNT), and a mix of CB and CNT, through simulated lightning strike tests, followed by both non-destructive ultrasonic inspection and destructive sectioning to characterize the damage inflicted by the simulated lightning strike. Three-point flexural tests are performed to evaluate the residual strength retained by all CFRP specimens. Results show that lightning strike damage experienced varying levels of reduction for CFRP composite specimens containing conductive fillers in comparison to the baseline specimen without fillers. Notably, the delamination only penetrated to the interface between the 1st and 2nd layer for the specimen with 0.25 wt.% CNT in comparison to the baseline CFRP specimen for which the delamination penetrated to the interface between the 5th and 6th layer. Moreover, the retention of the flexural modulus increased from 26.5% to a maximum of 95.0% for the specimen with 0.25 wt.% hybrid CB and CNT. Yet, we show that using our chosen conductive fillers cannot fully eliminate lightning strike damage. Additionally, adding conductive fillers could compromise the flexural properties. We provide discussions on future recommendations on using conductive fillers for the lightning strike protection of CFRP composites.

36 MATERIALS SCIENCE↗

Reaction Kinetics of CFRP Degradation in Supercritical Fluids

The reaction kinetics models of carbon fiber-reinforced plastic (CFRP) degradation in supercritical fluids were established by analyzing the chain scission reaction of a cross-linked network in CFRP. The effect of reaction time and temperature on the residual resin content from the recycled carbon fiber was investigated. The reaction order of CFRP degradation was estimated, and the reaction rate constant was calculated at different reaction temperatures. Reaction kinetics equations of CFRP degradation in different supercritical fluids were also proposed. Results indicated that CFRP degradation was mainly due to the scission of the C–C, C–O, and –O– bonds in the linear chain segment and of the C–N bond in the cross-linked segment of an epoxy resin cure system. The reaction order was 2 or 2.5. The monofilament tensile strength of recycled carbon fiber in supercritical n-butanol and n-propanol, which had higher degradation reaction rates, decreased by about 2% compared with that of the original carbon fiber.

36 MATERIALS SCIENCE↗

A micro-scale cutting model for UD CFRP composites with thermo-mechanical coupling

Cutting a unidirectional carbon fiber-reinforced polymer (UD CFRP) structure is the basic unit for CFRP machining, which is a complex thermal-mechanically coupled process. To reveal the deformation mechanism and predict cutting force in UD CFRP micro cutting, a micro-scale fracture model for UD CFRP cutting with thermal-mechanical coupling is demonstrated in this paper, which captures the failure modes for fibers, matrix and the interface based on a micro-level RVE using a relatively simple damage based fracture method. The thermal-mechanical coupling model at the micro scale is developed on the basis of the plastic energy dissipation and frictional heating during cutting. Failure models for the fiber, matrix and interface region are applied depending on the material properties of each of these three phases. Numerical simulations based on the above model with different fiber orientations were performed to predict the deformation and forces of different components in UD CFRP. Cutting experiments with the same fiber orientations as considered in the simulations were carried out to validate the force and deformation results. The predicted force and deformation patterns match well with evidence from our experiments. In general, the cutting force is larger than the thrust force regardless of fiber orientation. The cutting force reaches a maximum as the fiber orientation approaches 90 , but thrust forces do not vary substantially across cases. When the fiber orientation is acute, the deformation of fibers is much smaller than when the cutting angle is obtuse. Surface roughness follows the same trend with cutting angle as fiber deformation.

42 ENGINEERING↗

Study on shear strengthening of RC continuous T-beams using different layers of CFRP strips

Carbon fiber reinforced polymer (CFRP) laminates are externally bonded to reinforced concrete (RC) members to provide additional strength such as flexural, shear, etc. However, this paper presents the results of an experimental investigation for enhancing the shear capacity of reinforced concrete (RC) continuous T- beams using different layers of CFRP wrapping schemes. A total of three concrete beams were tested and various sheet configurations and layouts were studied to determine their effects on ultimate shear strength and shear capacity of the beams. One beam was kept as control beams, while other beams were strengthened with externally bonded CFRP strips with three side bonding and one or two layers of CFRP strips. From the test results, it was found that all schemes were found to be effective in enhancing the shear strength of RC beams. It was observed that the strength increases with the number of sheet layers provided the most effective strengthening for RC continuous T- beam. Beam strengthened using this scheme showed 23.21% increase in shear capacity as compared to the control beam. Two prediction models available in literature were used for computing the contribution of CFRP strips and compared with the experimental results.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

Electrically conductive carbon fiber layers as lightning strike protection for non-conductive epoxy-based CFRP substrate

A large amount of electrically conductive fillers is needed to enhance a Carbon Fiber Reinforced Plastics (CFRP) electrical conductivity enough to withstand lightning strikes of peak currents. However, such large alien constituents hamper the inherent good mechanical properties of CFRP structures. In this work, a solution has been proposed to retain both desired properties in a CFRP laminate. Layer-wise hybrid laminate has been demonstrated as a solution for lightning strike protection of Carbon Fiber Reinforced Plastics (CFRP). Top few layers of a hybrid laminate are prepared using electrically conductive polymer-based resin (CF/C-POLY) to provide effective dissipation of lightning current while epoxy-based CFRP substrate (CF/Epoxy) provides the main structural strength. An insulating adhesive layer is used to bond CF/C-POLY and CF/Epoxy to prepare the laminate. The hybrid laminates were tested for their effectiveness against lightning strikes. Laminates were struck by modified lightning waveform of component A with peak current of -14 kA and -40 kA. The performance of the laminates against lightning strike were evaluated using high speed camera, high-speed and thermal camera. It is found that CF/C-POLY layer successfully defended the main structural component i.e. CF/Epoxy from lightning direct damage.

36 MATERIALS SCIENCE↗

Simulated lightning strike investigation of CFRP comprising a novel Polyaniline/Phenol based electrically conductive resin matrix

Traditional carbon fiber reinforced plastics (CFRPs) have been reported to exhibit lower electrical conductivity in the through-thickness direction, and have since paved the path for developing new resin systems to improve the through-thickness electrical conductivity and functionality of CFRP laminates. This work designs and investigates a novel Polyaniline (PANI)/Phenol resin, which possesses high electrical conductivity and mechanical strength. The CFRP manufactured by this PANI/Phenol resin with an addition of up to (~23.30%) phenol resulted in 0.6 S/cm through-thickness conductivity and demonstrated flexural strength and modulus values of 477 MPa and 59.2 GPa, respectively. We further evaluate the effectiveness of lightning strike protection of PANI/Phenol-based conductive CFRP laminates with a simulated lightning strike test. In essence, this research reports on PANI/Phenol-based CFRP's effectiveness as a material for lightning suppression without applying traditional metal-based lightning strike protection (LSP) systems.

36 MATERIALS SCIENCE↗

Corrosion Control in Carbon Fiber Reinforced Plastic (CFRP) Composite-Aluminum Closure Panel Hem Joints

This project targeted the implementation of CFRP/Al closure panels as a drop-in replacement for all-aluminum closures used in automobile production today. The project focused on the development of corrosion fundamentals involving CFRP materials and the use of those materials in mixed-material joints. Numerous studies were completed to benchmark current materials and test mixed metal joints. Good correlation was found between outdoor exposures and laboratory cyclic corrosion testing. The insights from the corrosion testing fundamentals and benchmarking phases informed the development of low-cure adhesive and electrocoats and conductive primers for the CFRP. Adhesive and electrocoat materials were successfully developed meeting low-cure targets for bake (150C/10min). These materials were scaled-up and used to produce 5 prototype liftgates to further evaluate CFRP/Al joints in a full-scale part. The lower cure materials enabled mitigation of CTE mismatch and reduced the required bake temperature, resulting in reduced part distortion. Corrosion testing of the liftgates revealed unexpected increases in corrosion relative to the standard bake materials. While rigorous evaluation of the parts was not possible due to numerous complexities associated with prototype testing, the results provided significant insights into the material behavior of CFRP/Al joints. Key learnings from the project included a better understanding of the system complexity (interplay of substrate/primer conductivity, production of full-scale prototypes), advances in coating/adhesive design for low-cure applications involving CFRP, and advancement of corrosion test protocols for CFRP.

36 MATERIALS SCIENCE↗

Application of IR Thermography with Thermal Diffusivity Analysis for Detection of Plies Displacement in CFRP Composites

This paper presents an efficient nondestructive testing (NDT) method for detection of plies displacement in carbon fiber reinforced plastic (CFRP) composites using the active thermography technique. To assess the capability of the proposed technique for detection of plies displacement, the CFRP composite specimens with simulated fault were designed and manufactured. The IR thermography measurements were conducted using two-sided experimental arrangement. From recorded sequences of thermal images, the temperature variations versus time plots were extracted to obtain the maximum thermal contrasts. For quantitative interpretation of the results, the thermal diffusivity values for each composite material were determined and related to the fiber volume fraction. The experimental results showed that the thermal diffusivity increases with an increase of fiber volume fraction; further, the values of thermal diffusivity are specimen thickness dependent. The obtained values of thermal diffusivity varied from 1.5 × 10{sup −7} m{sup 2}/s (for 3.2 mm composite with 8.5 vol.% carbon fiber) to 2.6 × 10{sup −7} m{sup 2}/s (for 7.7 mm composite with 34.1 vol.% carbon fiber). On the basis of these results, it was concluded that the active thermography combined with thermal diffusivity analysis can be considered as a reliable NDT technique for detection of plies displacement in CFRP composites.

36 MATERIALS SCIENCE↗

Statistical Characterization of Fracture in CFRP-Concrete Interfaces Due to Wet-Dry Cycling

The experimental fracture mechanics Single Contoured-Cantilever Beam (SCCB) specimen was implemented to evaluate environmentally conditioned concrete-CFRP interfaces. Fracture studies were conducted on specimens having undergone 10, 20 and 30 cycles of alternate wetting and drying. Half of the 24 conditioned specimens studied were placed in a 10% sodium sulfate solution (pH = 6.2–6.5) and half were soaked in sodium hydroxide (pH = 12) to simulate naturally occurring acidic and alkaline field exposure-conditions, respectively. At the end of each target age, SCCB fracture testing was conducted. Two approaches were used in determining the fracture toughness of the CFRP-concrete interface bond that depend on the proper identification of loads reaching a critical state, P{sub c}. In the first, the topmost, or “head”, −initiation and -arrestment loads were averaged, and in the second, the mean of the entire “set” of -initiation and -arrestment loads was taken. This raw-data was then reduced by a statistical-based method from which a range of permissible critical loads was designated. The final G{sub Ic} values cited are based on an averaging of this refined data. Considerable degradation of the CFRP-concrete interface bond resulted especially for cases of latter-stage cycling in the aggressive sodium-sulfate and -hydroxide solutions.

36 MATERIALS SCIENCE↗

Scanning tone burst eddy-current thermography (S-TBET) for NDT of carbon fiber reinforced plastic (CFRP) components

Tone Burst Eddy Current technique uses eddy current to apply transient heating inside a component and uses a conventional IR camera for visualization of the response to the transient heating. This technique has been earliest demonstrated for metallic components made of AL, Steel, Stainless Steel, etc., and for detection of cracks, corrosion and adhesive dis-bonds. Although, not nearly as conducting as metals, the Carbon Fibre Reinforced Plastic (CFRP) material absorbs measurable electromagnetic radiation in the frequency range above 10 kHz. When the surface temperature is observed on the surface that is being heated (defined as the surface just beneath and slightly to one side of the heating coil), the surface temperature increases with increasing frequency because the internal heating increases with frequency. A 2-D anisotropic transient Eddy current heating and thermal conduction model has been developed that provides a reasonable description of the processes described above. The inherent anisotropy of CFRP laminates is included in this model by calculating the heating due to three superimposed, tightly coupled isotropic layers having a specified ply-layup. The experimental apparatus consists of an induction heating coil and an IR camera with low NETD and high frame rates. The coil is moved over the sample using a stepper motor controlled manipulator. The IR data recording is synchronized with the motion control to provide a movie of the surface temperature over time. Several components were evaluated for detection of impact damage, location of stiffeners, etc. on CFRP components.

42 ENGINEERING↗

Quantitative impact characterization of aeronautical CFRP materials with non-destructive testing methods

In recent years, an increasing number of safety-relevant structures are designed and manufactured from carbon fiber reinforced polymers (CFRP) in order to reduce weight of airplanes by taking the advantage of their specific strength into account. Non-destructive testing (NDT) methods for quantitative defect analysis of damages are liquid- or air-coupled ultrasonic testing (UT), phased array ultrasonic techniques, and active thermography (IR). The advantage of these testing methods is the applicability on large areas. However, their quantitative information is often limited on impact localization and size. In addition to these techniques, Airbus Group Innovations operates a micro x-ray computed tomography (μ-XCT) system, which was developed for CFRP characterization. It is an open system which allows different kinds of acquisition, reconstruction, and data evaluation. One main advantage of this μ-XCT system is its high resolution with 3-dimensional analysis and visualization opportunities, which enables to gain important quantitative information for composite part design and stress analysis. Within this study, different NDT methods will be compared at CFRP samples with specified artificial impact damages. The results can be used to select the most suitable NDT-method for specific application cases. Furthermore, novel evaluation and visualization methods for impact analyzes are developed and will be presented.

42 ENGINEERING↗

Upcycling of CFRP Waste: Viable Eco-friendly Chemical Recycling and Manufacturing of Novel Repairable and Recyclable Composites

The rapid growth of the carbon fiber-reinforced polymer (CFRP) composite market has driven researchers to find value-added applications for outdated prepregs, manufacturing scraps, and end-of-life components. Currently, most CFRP waste is incinerated or landfilled, which squanders its residual value and burdens the environment. Various mechanical, thermal, and chemical approaches have been attempted to recover the carbon fiber, polymer matrix, or both. However, these current practices are often costly, energy-intensive, and generate secondary waste and pollution. To address these shortcomings, this project aims to develop a viable and sustainable chemical recycling technology for CFRP waste that can efficiently and cost-effectively decompose the polymer matrix and manufacture new recyclable composites from both the recovered carbon fiber (rCF) and decomposed matrix polymer (DMP).

36 MATERIALS SCIENCE↗

NDE of Novel Materials (CFRP) [Slides]

CFRP composites have not been used for nuclear safety-related applications until recently. In 2019, the ASME Boiler and Pressure Vessel Code Committee approved a new Code Case N-871 for internal repairs of Class 2 and 3 safety-related piping using CFRP for Service Levels A, B, C, and D for a service life of 50 years. The NRC did not review N-871 for inclusion in the Code Case Regulatory Guides. This project focuses on evaluating the capabilities and limitations of Nondestructive Evaluation (NDE) methods for examining the Carbon Fiber Reinforced Polymer (CFRP) repairs in commercial nuclear power plants (NPPs). This Report summarizes the work done on this project until the end of FY24.

36 MATERIALS SCIENCE↗

Friction Stir Scribe Joining of Carbon Fiber Reinforced Polymer (CFRP) to Aluminum

The purpose of this project was to develop the critical process technology, models, and tools necessary to advance the Friction Stir Scribe, FSS, joining method through experimentation, validation at the laboratory scale, and integration into a production-like robotic environment. Implementation of FSS technology for joining polymer composites to metals will enable greater use of lightweight materials by providing technology capable of joining linear configurations without the use of adhesives or other third-body fasteners by creating an in-situ joint from the parent materials. As FSS technology provides the capability to join multi-material structures on robotic platforms using linear configurations, the development of this technology for use on the BIW will impact a great diversity of CFRP joints within the vehicle; thus, allowing a greater reduction in vehicle mass through more specifically designed structures. The FSS process has been developed to include integration of the FSS tool with a stationary shoulder, which has been shown to be required to achieve the desired surface quality (i.e., crown flash level). However, the targeted joint strength has not been achieved because the resulting stirred CFRP microstructure does not provide similar performance as the as-molded composite leading to low fracture strengths despite our efforts investigating various unique alternative approaches. In support of the experimental work, a process-structure model was developed and validated for the FSS joining (FSSJ) process using surrogate materials (steel and Al). The cyclic corrosion testing of the FSS joints and self-piercing riveted (SPR) joints revealed different modes of galvanic corrosion in the two types of joints. The SPR samples exhibited a greater amount of corrosion on the external surfaces. The presence of steel rivets in these joints exacerbated the situation, with the rivets getting preferentially corroded. The FSSJ samples despite exhibiting less surface corrosion, exhibited severe corrosion under the joint overlap area.

36 MATERIALS SCIENCE↗