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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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DOE OSTI2020

The exit-wave power-cepstrum transform for scanning nanobeam electron diffraction: robust strain mapping at subnanometer resolution and subpicometer precision

Scanning nanobeam electron diffraction (NBED) with fast pixelated detectors is a valuable technique for rapid, spatially resolved mapping of lattice structure over a wide range of length scales. However, intensity variations caused by dynamical diffraction and sample mistilts can hinder the measurement of diffracted disk centers as necessary for quantification. Robust data processing techniques are needed to provide accurate and precise measurements for complex samples and non-ideal conditions. Here we present an approach to address these challenges using a transform, called the exit wave power cepstrum (EWPC), inspired by cepstral analysis in audio signal processing. The EWPC transforms NBED patterns into real-space patterns with sharp peaks corresponding to inter-atomic spacings. We describe a simple analytical model for interpretation of these patterns that cleanly decouples lattice information from the intensity variations in NBED patterns caused by tilt and thickness. With tracking the inter-atomic spacing peaks in EWPC patterns, strain mapping is demonstrated for two practical applications: mapping of ferroelectric domains in epitaxially strained PbTiO 3 films and mapping of strain profiles in arbitrarily oriented core-shell Pt-Co nanoparticle fuel-cell catalysts. The EWPC transform enables lattice structure measurement at sub-pm precision and sub-nm resolution that is robust to small sample mistilts and random orientations.

42 ENGINEERING↗

DOE OSTI2017

Optimal Bandwidth for Multitaper Spectrum Estimation

A systematic method for bandwidth parameter selection is desired for Thomson multitaper spectrum estimation. We give a method for determining the optimal bandwidth based on a mean squared error (MSE) criterion. When the true spectrum has a second-order Taylor series expansion, one can express quadratic local bias as a function of the curvature of the spectrum, which can be estimated by using a simple spline approximation. This is combined with a variance estimate, obtained by jackknifing over individual spectrum estimates, to produce an estimated MSE for the log spectrum estimate for each choice of time-bandwidth product. The bandwidth that minimizes the estimated MSE then gives the desired spectrum estimate. Additionally, the bandwidth obtained using our method is also optimal for cepstrum estimates. We give an example of a damped oscillatory (Lorentzian) process in which the approximate optimal bandwidth can be written as a function of the damping parameter. Furthermore, the true optimal bandwidth agrees well with that given by minimizing estimated the MSE in these examples.

97 MATHEMATICS AND COMPUTING↗

DOE OSTI2017

Multiobjective Optimization of Regional and Teleseismic Data to Constrain the Source of the 12 September 2016 Mw 5.4 Earthquake in South Korea

In this paper, we propose a new approach for source inversion with automatic criteria for the station selection process and using a multiobjective optimization scheme combining teleseismic body-wave and regional surface-wave observations. To illustrate the approach, we determine the source parameters of the 12 September 2016 M w 5.4 South Korea earthquake, as well as its foreshock (same day) and its main aftershock on 19 September 2016. Available teleseismic (short period and broadband) and regional (broadband) seismograms from the Incorporated Research Institutions for Seismology International–Federation of Digital Seismograph Networks (IRIS-FDSN) webservice are selected (see Data and Resources). First, all teleseismic data with signal-to-noise ratio (SNR) above 2 in the 0.3–1.5 Hz frequency band are selected and a cepstrum function is blindly applied to help detect reflected wave arrivals inside a P coda. This method allows the identification of records with weak P-coda and clear depth phase (pP, sP) arrivals and can be used to select an optimal set of teleseismic seismograms to be used for the inversion. Second, regional seismograms are selected according to the fit between their observed and theoretical dispersion curves extracted from local 1D velocity model. Depending on the epicentral distance, two frequency bands are proposed for regional data: 15–50 s for epicentral distances smaller than 2° and 30–80 s otherwise. Finally, we explore the space parameters from exhaustive grid searches for the two objective functions Tf and Rf for teleseismic and regional data, respectively. We show that the seismic moment parameters can be exclusively derived from Rf and can be fixed for Tf. However, the depth parameter is not sensitive to Rf and can be simultaneously inverted from both. The selection of the optimal solution satisfying both cost functions uses the optimum Pareto front that allows a decrease in epistemic uncertainty. Lastly, we discuss the advantage of this approach for improving the characterization of moderate earthquake sources in areas with limited regional instrumentation.

58 GEOSCIENCES↗

DOE OSTI2023

Fluctuation cepstral scanning transmission electron microscopy of mixed-phase amorphous materials

Four-dimensional scanning transmission electron microscopy (4D-STEM) is a versatile analytical tool for characterizing materials structural properties. However, extending such analysis to disordered materials is challenging, especially in technologically important samples with mixed ordered and disordered phases. Here, in this work, we present a new 4D-STEM method, called fluctuation cepstral STEM (FC-STEM), based on the fluctuation analysis of cepstral transform of diffraction patterns. The peaks in the associated transformation relate to inter-atomic distances in a thin sample. By varying the real-space range over which fluctuations are calculated, distinct ordered and disordered phases can be mapped in a diffractive image reconstruction. We demonstrate the principles of FC-STEM by characterizing a silicon anode, harvested from a cycled lithium-ion battery. A mixture of amorphous and nanocrystalline silicon, graphitic carbon, and electrolyte by-products is identified and mapped. Comparisons with conventional electron imaging and energy-dispersive X-ray spectroscopy show that FC-STEM is highly effective for the structure determination of mixed-phase amorphous materials.

36 MATERIALS SCIENCE↗