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Results for “Coherent X-ray scattering”

Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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All sourcesNASA NTRSDOE OSTI
NASA NTRS1986

Measuring interstellar grains from the haloes of binary X-ray sources

Coherent forward scattering of X-rays by interstellar grains creates a halo around the X-ray image of a compact source. The fractional halo brightness at 2 keV is typically of order 10% moderately reddened galactic sources. The angular brightness distribution of the halo, which extends over several arcminutes, indicates the size distribution of the grains, and the spectrum of the halo indicates the composition of the grains. The halo will persist for several hours after the point source vanishes during an eclipse of a binary source; this provides a way to avoid systematic errors in measuring halo brightness due to an extended point response function of the X-ray telescope. Indeed, it is possilbe to infer the size distribution and composition of the grains without an imaging X-ray telescope by observing the time-dependence of the halo spectrum during eclipse.

Xu, Y.↗
NASA NTRS2005

Overview of Biomineralization and Nanobacteria

Biomineralization is a frequently used term in nanotechnology, astrobiology, geology, and medicine. In the process of biomineralization, a living organism provides a chemical environment that controls the nucleation and growth of unique mineral phases. Often these materials exhibit hierarchical structural order, leading to superior physical properties, not found either in their inorganic counterparts or in synthetic materials. Biomineralization is widespread in the biosphere and hundreds of different minerals are produced or assisted by a variety of organisms from bacteria to humans. Teeth, bones, kidney stones, and skeletons of algae, mussels, and magnetotactic bacteria are all examples of biomineralization. We do not fully understand the control mechanism of biomineralization either in primitive or in developed organisms. The presence of organic molecules, among other characteristics, can influence the coherence length for X-ray scattering in biogenic crystals. Control over biomineral properties can be accomplished at a myriad of levels, including the regulation of particle size, shape, crystal orientation, polymorphic structure, defect texture, and particle assembly. In the latter case, cellular processes enable control in both the spatial and temporal domain in such a way that hierarchical composite structures can be built which increase the toughness and durability of the material, which is invaluable for load-bearing materials such as bones, teeth, mollusk shells, etc. Durability of biominerals produces remarkably preserved bacterial and cyanobacterial microfossils from billions of years-old samples. The differentiation between microfossils and nonbiogenic artifacts has been a lively discussion subject in astrobiology especially in the last decade. Clearly, more detailed information on the mechanism of biomineralization, and the effect of organic matter on crystal formation/fossilization would help focus such discussions.

Ciftcioglu, N.↗
NASA NTRS2000

The Origin of the X-Ray and Ultraviolet Emission in NGC 7469

We present a spectral analysis of a approx 30 day, near-continuous observation of the Seyfert 1 galaxy NGC 7469 with RXTE. Daily integrations show strong spectral changes during the observation. Our main result is that we find the X-ray spectral index to be correlated with the UV flux. Furthermore, the broadband X-ray photon flux is also correlated with the UV continuum. These correlations point toward a model in which the X-rays originate via thermal Comptonization of UV seed photons. Furthermore, the UV is also correlated with the extrapolation of the X-ray power law into the soft X-ray/EUV region. Our data analysis therefore reopens the possibility that the UV photons and their variability arise from reprocessing, as long as the primary source of heating is photoelectric absorption in the re-processor, rather than Compton down-scattering. A coherent picture of the X-ray/UV variability can therefore be constructed whereby absorption and reprocessing of EUV/soft X-rays in a standard accretion disk produce a variable seed photon distribution, which is in turn up-scattered into the X-ray band. We also find a significant correlation between the 2-10 keV flux and the 6.4 keV iron K-alpha line, suggesting that at least some portion of the line originates within approx. 1 light day of the X-ray continuum source. Neither the power-law photon index nor the Compton reflection component are correlated with the 2-10 keV flux. The latter is not correlated with the iron K-alpha line flux either. We do find an apparent correlation between the X-ray spectral index and the strength of the Compton reflection component. In an Appendix we show, however, that this can be produced by a combination of statistical and systematic errors. We conclude that the apparent variations in the Compton reflection component may be an artifact of these effects.

Nandra, K.↗
NASA NTRS1986

Solar flare ionization in the mesosphere observed by coherent-scatter radar

The coherent-scatter technique, as used with the Urbana radar, is able to measure relative changes in electron density at one altitude during the progress of a solar flare when that altitude contains a statistically steady turbulent layer. This work describes the analysis of Urbana coherent-scatter data from the times of 13 solar flares in the period from 1978 to 1983. Previous methods of measuring electron density changes in the D-region are summarized. Models of X-ray spectra, photoionization rates, and ion-recombination reaction schemes are reviewed. The coherent-scatter technique is briefly described, and a model is developed which relates changes in scattered power to changes in electron density. An analysis technique is developed using X-ray flux data from geostationary satellites and coherent scatter data from the Urbana radar which empirically distinguishes between proposed D-region ion-chemical schemes, and estimates the nonflare ion-pair production rate.

Parker, J. W.↗
NASA NTRS1986

An analysis at mesospheric coherent-scatter power enhancements during solar flare events

Solar flares produce increases in coherent-scatter power from the mesosphere due to the increase in free electrons produced by X-ray photoionization. Thirteen such power enhancements were observed at Urbana. When such an enhancement occurs at an altitude containing a turbulence layer with constant strength, the relative enhancement of electon density is estimated from the enhancement in power. Such estimates of enchanced electron density are compared with estimates of the X-ray photoionization at that altitude, deduced from geostationary satellite measurements. It is found that possible types ion-chemical reaction scheme may be distinguished, and the nonflare ion-pair production function may be estimated. The type of ion-chemical scheme and the nonflare ion-production function are shown to depend on the solar zenith angle.

Parker, J.↗
NASA NTRS2007

Investigation of Synthetic Mg(1.3)V(1.7)O4 Spinel with MgO Inclusions: Case Study of a Spinel with an Apparently occupied Interstitial Site

A magnesium vanadate spinel crystal, ideally MgV2O4, synthesized at 1 bar, 1200 C and equilibrated under FMQ + 1.3 log f(sub o2) condition, was investigated using single-crystal X-ray diffraction, electron microprobe, and electron backscatter (EBSD). The initial X-ray structure refinements gave tetrahedral and octahedral site occupancies, along with the presence of 0.053 apfu Mg at an interstitial octahedral site . Back-scattered electron (BSE) images and electron microprobe analyses revealed the existence of an Mg-rich phase in the spinel matrix, which was too small (less than or equal to 3microns) for an accurate chemical determination. The EBSD analysis combined with X-ray energy dispersive spectroscop[y (XEDS) suggested that the Mg-rich inclusions are periclase oriented coherently with the spinel matrix. The final structure refinements were optimized by subtracting the X-ray intensity contributions (approx. 9%) of periclase reflections, which eliminated the interstitial Mg. This study provides insight into possible origins of refined interstitial cations reported in the the literature for spinel, and points to the difficulty of using only X-ray diffraction data to distinguish a spinel with interstitial cations from one with coherently oriented MgO inclusions.

Uchida, Hinako↗
NASA NTRS2019

Detection of Nonthermal Hard X-Ray Emission from the “Fermi Bubble” in an External Galaxy

We report new Chandra hard X-ray (>2 keV) and Jansky Very Large Array C-band observations of the nuclear super bubble of NGC 3079, an analog of the “Fermi bubble” in our Milky Way. We detect extended hard X-ray emission on the southwest (SW)side of the galactic nucleus with coherent multiwavelength features in radio, Hα, and soft X-ray. The hard X-ray feature has a cone shape with possibly a weak cap, forming a bubble-like structure with a diameter of∼1.1 kpc. A similar extended feature, however, is not detected on the northeast (NE)side, which is brighter in all other wavelengths such as radio, Hα, and soft X-ray. Scattered photons from the nuclear region or other nearby point-like X-ray bright sources, inverse Compton emission from cosmic-ray(CR)electrons via interaction with the cosmic microwave background, or any individually faint stellar X-ray source populations, cannot explain the extended hard X-ray emission on the SW side and the strongly NE/SW asymmetry. A synchrotron emission model, plus a thermal component accounting for the excess at∼1 keV, can well characterize the broadband radio/hard X-ray spectra. The broadband synchrotron spectra do not show any significant cutoff, and even possibly slightly flatten at higher energy. This rule out a loss-limited scenario in the acceleration of the CR electrons in or around this superbubble. As the first detection of kiloparsec-scale extended hard X-ray emission associated with a galactic nuclear superbubble, the spatial and spectral properties of the multiwavelength emissions indicate that the CR leptons responsible for the broadband synchrotron emission from the SW bubble must be accelerated in situ, instead of transported from the nuclear region of the galaxy.

Jiang-Tao Li↗
NASA NTRS2003

Phase Sensitive X-Ray Diffraction Imaging Study of Protein Crystals

The study of defects and growth of protein crystals is of importance in providing a fundamental understanding of this important category of systems and the rationale for crystallization of better ordered crystals for structural determination and drug design. Yet, as a result of the extremely weak scattering power of x-rays in protein and other biological macromolecular crystals, the extinction lengths for those crystals are extremely large and, roughly speaking, of the order of millimeters on average compared to the scale of micrometers for most small molecular crystals. This has significant implication for x-ray diffraction and imaging study of protein crystals, and presents an interesting challenge to currently available x-ray analytical techniques. We proposed that coherence-based phase sensitive x-ray diffraction imaging could provide a way to augment defect contrast in x-ray diffraction images of weakly diffracting biological macromolecular crystals. I shall examine the principles and ideas behind this approach and compare it to other available x-ray topography and diffraction methods. I shall then present some recent experimental results in two model protein systems-cubic apofemtin and tetragonal lysozyme crystals to demonstrate the capability of the coherence-based imaging method in mapping point defects, dislocations, and the degree of perfection of biological macromolecular crystals with extreme sensitivity. While further work is under way, it is intended to show that the observed new features have yielded important information on protein crystal perfection and nucleation and growth mechanism otherwise unobtainable.

Hu, Z. W.↗
NASA NTRS2005

A Comparative View of X-rays from the Solar System

With the advent of sophisticated X-ray observatories, viz., Chandra and XMM-Newton, the field of planetary X-ray astronomy is advancing at a faster pace. Several new solar system objects are now know to shine in X-rays at energies generally below 2 keV. Jupiter, Saturn, and Earth, all three magnetized planets, have been observed by Chandra and XMM-Newton. At Jupiter, both auroral and non-auroral disk X-ray emissions have been observed. The first soft X-ray observation of Earth's aurora by Chandra shows that it is highly variable. X-rays have been detected from Saturn's disk, but no convincing evidence of X-ray aurora has been seen. Several comets have been observed in X-rays by Chandra and XMM-Newton. Cometary X-rays are produced due to change exchange of solar wind ions with cold cometary neutrals. Soft X-rays have also been observed from Venus, Mars, Moon, Io, Europa, Io plasma torus, and heliosphere. The non-auroral X-ray emissions from Jupiter, Saturn, and Earth, and those from sunlit disk of Mars, Venus, and Moon are produced due to scattering of solar X-rays. The spectral characteristics of X-ray emission from comets, heliosphere, darkside of Moon, and Martian halo are quite similar, but they appear to be quite different from those of Jovian auroral X-rays. The X- ray aurora on Earth is generated by electron bremsstrahlung and on Jupiter by precipitation of highly-ionized energetic heavy ions. In this paper we will present a comparative overview of X-ray emission from different solar system objects and make an attempt to synthesize a coherent picture.

Bhardwaj, Anil↗
NASA NTRS1985

Effect of Scattering on Instabilities in Line-driven Stellar Winds

Line driven O-B stellar winds are unstable to perturbations of short spatial wavelength and the growth rates for such instabilities are very rapid. The nature of the nonlinear development of this instability is unknown, but might possibly be one of blobs of gas driven through ambient gas or a quasiregular train of outward moving shocks. In either case the resulting dissipation of mechanical energy might explain the observed anomalous heating n O-B stars as evidenced by their X-ray emission and high ionization state. It also might explain the observed fine structure of the absorption lines and their time variability. The driving due to the absorption of the stellar continuum flux was considered and the effects of the diffuse, scattered radiation field were neglected. It was shown that under certain special conditions the effect of scattering could reduce the instability growth rate to zero. A stability analysis that includes scattering, but that uses the more physically realistic assumption of complete redistribution instead of coherent scattering, and that includes the effects of transverse velocity gradients, which become important as the flow moves away from the stellar surface is presented. It is found that the instability is eliminated right at the base of the wind, but that as the flow moves outward the instability rate rapidly becomes equal to a substantial fraction of the calculated value, the fraction asymptotically reaching 80% at large radii. Since this still implies many e folds in a characteristic outflow time, the primary conclusion that these winds are highly unstable is unchanged.

Owocki, S. P.↗
NASA NTRS1984

Observations of solar-flare ionization in the mesosphere using coherent-scatter radar

Observations of solar-flare ionization in the mesosphere can be made using coherent-scatter radar systems. The scattered power profiles they measure in the 60-90 km altitude region is a function of the ion concentration gradient and the intensity of turbulent mixing at each altitude. By comparing the power profiles before, during and after a solar flare, it is possible to estimate the ion production rate during the flare as a function of altitude and time. This analysis is used to compare the ion production rates with generally accepted ion-chemical models. Comparisons are made with ion production rates estimated from the solar X-ray flux for the same flare made by geostationary satellites.

Parker, J. W.↗
NASA NTRS2015

Transmission X-ray Diffraction (XRD) Patterns Relevant to the MSL Chemin Amorphous Component: Sulfates And Silicates

The Mars Science Laboratory (MSL) CheMin instrument on the Curiosity rover is a transmission X-ray diffractometer (Co-Kalpha radiation source and a approx.5deg to approx.52deg 2theta range) where the analyzed powder samples are constrained to have discrete particle diameters <150 microns by a sieve. To date, diffraction patterns have been obtained for one basaltic soil (Rocknest (RN)) and four drill fines of coherent rock (John Klein (JK), Cumberland (CB), Windjana (WJ), and Confidence Hills (CH)). The CheMin instrument has detected and quantified the abundance of both primary igneous (e.g., feldspar, olivine, and pyroxene) and secondary (e.g., Ca-sulfates, hematite, akaganeite, and Fe-saponite) minerals. The diffraction patterns of all CheMin samples are also characterized by a broad diffraction band centered near 30deg 2theta and by increasing diffraction intensity (scattering continuum) from approx.15deg to approx.5deg, the 2theta minimum. Both the broad band and the scattering continuum are attributed to the presence of an XRD amorphous component. Estimates of amorphous component abundance, based on the XRD data itself and on mass-balance calculations using APXS data crystalline component chemistry derived from XRD data, martian meteorites, and/or stoichiometry [e.g., 6-9], range from approx.20 wt.% to approx.50 wt.% of bulk sample. The APXSbased calculations show that the amorphous component is rich in volatile elements (esp. SO3) and is not simply primary basaltic glass, which was used as a surrogate to model the broad band in the RN CheMin pattern. For RN, the entire volatile inventory (except minor anhydrite) is assigned to the amorphous component because no volatile-bearing crystalline phases were reported within detection limits [2]. For JK and CB, Fesaponite, basanite, and akaganeite are volatile-bearing crystalline components. Here we report transmission XRD patterns for sulfate and silicate phases relevant to interpretation of MSL-CheMin XRD amorphous components.

Morris, R. V.↗
NASA NTRS2009

Fabricating Radial Groove Gratings Using Projection Photolithography

Projection photolithography has been used as a fabrication method for radial grove gratings. Use of photolithographic method for diffraction grating fabrication represents the most significant breakthrough in grating technology in the last 60 years, since the introduction of holographic written gratings. Unlike traditional methods utilized for grating fabrication, this method has the advantage of producing complex diffractive groove contours that can be designed at pixel-by-pixel level, with pixel size currently at the level of 45 45 nm. Typical placement accuracy of the grating pixels is 10 nm over 30 nm. It is far superior to holographic, mechanically ruled or direct e-beam written gratings and results in high spatial coherence and low spectral cross-talk. Due to the smooth surface produced by reactive ion etch, such gratings have a low level of randomly scattered light. Also, due to high fidelity and good surface roughness, this method is ideally suited for fabrication of radial groove gratings. The projection mask is created using a laser writer. A single crystal silicon wafer is coated with photoresist, and then the projection mask, with its layer of photoresist, is exposed for patterning in a stepper or scanner. To develop the photoresist, the fabricator either removes the exposed areas (positive resist) of the unexposed areas (negative resist). Next, the patterned and developed photoresist silicon substrate is subjected to reactive ion etching. After this step, the substrate is cleaned. The projection mask is fabricated according to electronic design files that may be generated in GDS file format using any suitable CAD (computer-aided design) or other software program. Radial groove gratings in off-axis grazing angle of incidence mount are of special interest for x-ray spectroscopy, as they allow achieving higher spectral resolution for the same grating area and have lower alignment tolerances than traditional in-plane grating scheme. This is especially critical for NASA Constellation- X project that will utilize hundreds of gratings all of which need to be precisely aligned for x-ray observation of space.

Iazikov, Dmitri↗
NASA NTRS2017

Probing Large-Scale Coherence Between Spitzer IR and Chandra X-Ray Source-Subtracted Cosmic Backgrounds

We present new measurements of the large-scale clustering component of the cross-power spectra of the source-subtracted Spitzer-IRAC cosmic infrared background and Chandra-ACIS cosmic X-ray background surface brightness fluctuations. Our investigation uses data from the Chandra Deep Field South, Hubble Deep Field North, Extended Groth Strip/AEGIS (All-wavelength Extended Groth Strip International Survey) field, and UDS (Ultra-Deep Survey) / SXDF surveys, comprising 1160 Spitzer hours and approximately 12 megaseconds of Chandra data collected over a total area of 0.3 degrees squared. We report the first (greater than 5 sigma) detection of a cross-power signal on large angular scales greater than 20 arc seconds between [0.5-2] kiloelectronvolts and the 3.6 and 4.5 micron bands, at approximately 5 omega and 6.3 sigma significance, respectively. The correlation with harder X-ray bands is marginally significant. Comparing the new observations with existing models for the contribution of the known unmasked source population at redshift less than 7, we find an excess of about an order of magnitude at 5 sigma confidence. We discuss possible interpretations for the origin of this excess in terms of the contribution from accreting early black holes (BHs), including both direct collapse BHs and primordial BHs, as well as from scattering in the interstellar medium and intra-halo light.

Capelluti, N.↗
NASA NTRS2020

Timing of the Accreting Millisecond Pulsar IGR J17591-2342: Evidence of Spin-down during Accretion

We report on the phase-coherent timing analysis of the accreting millisecond X-ray pulsar IGR J17591–2342, using Neutron Star Interior Composition Explorer (NICER) data taken during the outburst of the source between 2018 August 15 and 2018 October 17. We obtain an updated orbital solution of the binary system. We investigate the evolution of the neutron star spin frequency during the outburst, reporting a refined estimate of the spin frequency and the first estimate of the spin frequency derivative ( ˙ν ∼ −7 × 10−14 Hz s−1), confirmed independently from the modelling of the fundamental frequency and its first harmonic. We further investigate the evolution of the X-ray pulse phases adopting a physical model that accounts for the accretion material torque as well as the magnetic threading of the accretion disc in regions where the Keplerian velocity is slower than the magnetosphere velocity. From this analysis we estimate the neutron star magnetic field Beq = 2.8(3) × 108 G. Finally, we investigate the pulse profile dependence on energy finding that the observed behaviour of the pulse fractional amplitude and lags as a function of energy is compatible with the down-scattering of hard X-ray photons in the disc or the neutron star surface.

A Sanna↗