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The selection of structural alloys, composite materials, solder alloys, and filler materials for use in cryogenic models is discussed. In particular, materials testing programs conducted at Langley are described.
A study investigating the physical properties and use of the SiAl composite Controlled Expansion 7 (CE7) for the packaging of silicon bolometric detectors for millimeter-wave astrophysical applications at cryogenic temperatures is presented. The existing interfaces to such detectors are typically made of either ductile metals or micro-machined silicon. As a composite of Si and Al, we find that CE7 exhibits properties of both in ways that may be advantageous for this application. This exploration of the physical properties of CE7 reveals: (a) superconductivity below a critical transition temperature, T_c ∼ 1.2 K; (b) a thermal contraction profile much closer to Si than metal substrates; (c) the relatively low thermal conductivity anticipated for a superconductor, which can be improved by Au-plating; and (d) the feasibility of machining mechanical features with tolerances of ∼25 µm. We further discuss the use of CE7 in the cosmology large angular scale surveyor telescope array, which deployed CE7 in several of its detector focal planes.
Cryogenically worked materials during strain hardening
Cryogenic radiation tests on structural alloys for NERVA Program, discussing test environment effects
Cryogenic fluid insulating material, ceramic-gold reflective coating and ceramic thermal insulation
Summary of material behavior at cryogenic temperatures
Electromechanical materials can be used in smart sensor and actuator devices. Yet none performing at low temperatures are available. To meet this need, Pb((MgNi)(1/3)Ta(2/3))03 was synthesized as an electrostrictive ceramic for applications in cryogenic environments. Employing the columbite precursor route, samples with 0% to 100% Ni substitution for Mg were prepared, but only samples with Ni-substitutions less than or equal to 20% yielded primarily the desired perovskite phase. For these compositions the temperature of highest permittivity decreased linearly with increasing Ni content to yield a minimum value of -124 C for 20% Ni-substitution. This composition showed good relaxor dielectric behavior with a maximum relative permittivity of 5890 at 1 kHz. Additionally, in samples with excess MgO, the magnitude of permittivity doubled. In this effort, Pb((MgNi)(1/3)Ta(2/3))03 (PMNiTa) was fabricated to lower its transition temperature by substituting Ni for Mg successively.
Aerogel blanket materials for use in thermal insulation systems are now commercially available and implemented by industry. Prototype aerogel blanket materials were presented at the Cryogenic Engineering Conference in 1997 and by 2004 had progressed to full commercial production by Aspen Aerogels. Today, this new technology material is providing superior energy efficiencies and enabling new design approaches for more cost effective cryogenic systems. Aerogel processing technology and methods are continuing to improve, offering a tailor-able array of product formulations for many different thermal and environmental requirements. Many different varieties and combinations of aerogel blankets have been characterized using insulation test cryostats at the Cryogenics Test Laboratory of NASA Kennedy Space Center. Detailed thermal conductivity data for a select group of materials are presented for engineering use. Heat transfer evaluations for the entire vacuum pressure range, including ambient conditions, are given. Examples of current cryogenic applications of aerogel blanket insulation are also given. KEYWORDS: Cryogenic tanks, thermal insulation, composite materials, aerogel, thermal conductivity, liquid nitrogen boil-off
Effect of nuclear radiation on materials at cryogenic temperature
The effects of cryogenic temperatures on the mechanical and physical properties of materials are summarized. Heat capacity and thermal conductivity are considered in the context of conservation of liquid nitrogen, thermal stability of the gas stream, and the response time for changes in operating temperature. Particular attention is given to the effects of differential expansion and failure due to thermal fatigue. Factors affecting safety are discussed, including hazards created due to the inadvertent production of liquid oxygen and the physiological effects of exposure to liquid and gaseous nitrogen, such as cold burns and asphyxiation. The preference for using f.c.c. metals at low temperatures is explained in terms of their superior toughness. The limitations on the use of ferritic steels is also considered. Nonmetallic materials are discussed, mainly in the context of their LOX compatibility and their use in the form of foams and fibers as insulatants, seals, and fiber reinforced composites.
Nuclear radiation effect on materials at cryogenic temperatures
Nuclear radiation effect on materials at cryogenic temperatures
Many different aerogel-based materials are now being used in thermal insulation systems for cryogenic applications. These materials include flexible composite blankets, bulk-fill particles, and polymer composites in both evacuated and non-evacuated environments. In ambient environments, aerogels provide superior thermal performance compared to conventional polymeric foam and cellular glass insulations while offering unique advantages in avoiding problems with weathering, moisture, and mechanical damage. Aerogels are also used as spacer materials in multilayer insulation systems. These layered systems provide combined structural-thermal capability for cryogenic systems in either vacuum-jacketed or externally-applied insulation designs. Test data (effective thermal conductivity) include a wide range of both commercial and experimental aerogel materials. Testing was performed using laboratory cryostats and standard methods including full range vacuum (from ambient pressure to high vacuum) and boundary temperatures 293 K and 78 K. Examples of aerogel-based insulation systems are given for both evacuated and non-evacuated applications.
Effect of nuclear radiation on materials at cryogenic temperatures
Many different aerogel-based materials are now being used in thermal insulation systems for cryogenic applications. These materials include flexible composite blankets, bulk-fill particles, and polymer composites in both evacuated and non-evacuated environments. In ambient environments, aerogels provide superior thermal performance compared to conventional polymeric foam and cellular glass insulations while offering unique advantages in solving problems with weathering, moisture, and mechanical damage. Aerogels are also used as spacer materials in multilayer insulation systems. These layered systems provide combined structural-thermal capability for cryogenic systems in either vacuum-jacketed or externally-applied insulation designs. Test data (effective thermal conductivity) include a wide range of both commercial and experimental aerogel materials. Testing was performed using laboratory cryostats and standard methods including full range vacuum (from ambient pressure to high vacuum) and boundary temperatures 293 K and 78 K. Examples of aerogel-based insulation systems are given for both evacuated and non-evacuated applications.
Physical and thermal properties of structural reinforced plastic materials at cryogenic temperatures
Structural reinforced plastic materials at cryogenic temperatures
Nuclear radiation effect on materials at cryogenic temperatures