Search NASA⌕ Search

SEARCH · Search NASA

Results for “Fracture instability”

Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

Quote a phrase for an exact phrase match. Source license links do not imply unrestricted reuse.

At least 19 records
All sourcesNASA NTRSDOE OSTI
DOE OSTI2022

Integrated simulation, machine learning, and experimental approach to characterizing fracture instability in indentation pillar-splitting of materials

Measuring fracture toughness of materials at small scales remains challenging due to limited experimental testing configurations. A recently developed indentation pillar-splitting method has shown promise of improved flexibility in fracture toughness measurements at the microscale, partly due to the occurrence of an unusual fracture instability, i.e., a transition from stable to unstable crack propagation. In spite of growing interest in this method, the underlying mechanism of this phenomenon is yet to be elucidated. Furthermore, we provide a comprehensive description of fracture instability in indentation pillar-splitting by combining in situ experiments with high-fidelity simulations based on cohesive zone and J-integral methods. In addition, a machine-learning-based solution for predicting the critical indentation load of fracture instability is established through Gaussian processes regression for broad use of this method by the community.

36 MATERIALS SCIENCE↗
DOE OSTI2026

Phase instability-coupled fracture behavior in garnet LLZO solid electrolytes: a machine learning-enabled atomistic study

Fracture in the garnet-type solid electrolyte Li 7 La 3 Zr 2 O 12 (LLZO) poses a critical threat to both the performance and safety of solid-state batteries. To unravel the coupled chemomechanical processes that govern fracture in LLZO under external loading, we carry out large-scale molecular-dynamics simulations with a validated machine-learning force field. Our results demonstrate that triaxial stresses at crack flanks trigger a localized cubic-to-tetragonal phase transformation, which is accompanied by Li-ion rearrangement. The emergent tetragonal domains feature lattice contraction normal to the fracture plane, imposing coherent misfit strains that provide an additional driving force for further crack propagation. Crucially, introducing Li deficiencies stabilizes the cubic phase, postponing the phase transition and thereby delaying fracture initiation. These findings highlight the role of intrinsic phase instability in dictating LLZO's fracture resistance and its critical connection to local Li concentration. This chemomechanical coupling points toward targeted strategies to enhance the mechanical robustness of garnet electrolytes, including tuning Li content, ensuring dopant homogeneity, and refining processing protocols.

Materials science↗
NASA NTRS1972

Correcting for nonlinear effects in fracture toughness testing.

Expressions for fracture toughness, which include nonlinear effects due to crack front plastic yield and possible small crack extension prior to fracture instability, are obtained for several test specimen configurations. Inclusion of such effects is based on a simple compliance type determination of the total energy rate at onset of fast fracture.

Liebowitz, H.↗
DOE OSTI2024

Crack Growth Rate and Fracture Toughness of Stainless Steel Welds in Light Water Reactor Environment

Austenitic stainless steel welds play a crucial role in maintaining the structural integrity of light water reactors. Within the reactor core, stainless steel welds endure a harsh service environment including elevated temperature, corrosive coolant, and intense neutron irradiation. Long-term exposure to such a severe service environment could lead to performance degradation. To ensure the safe and economic operation of light water reactors, this study performed crack growth rate and fracture toughness tests on irradiated and thermally aged weld samples harvested from decommissioned reactor components. In a low-corrosion-potential environment, stainless steel welds showed resistance to stress corrosion cracking, and the measured crack propagation rates were comparable to those of wrought stainless steels under similar test conditions. However, a marked decline in fracture toughness was observed in weld samples, particularly in irradiated samples. Fracture instability was observed at ~0.8 dpa, significantly lower than those observed in wrought stainless steels. Further research at higher doses is needed to evaluate the dose dependence of irradiation-induced embrittlement, and to understand the interplay between thermal aging and neutron irradiation in stainless steel welds.

22 GENERAL STUDIES OF NUCLEAR REACTORS↗
NASA NTRS1979

Long term storage test of titanium material with liquid fluorine propellant

The compatibility of 6AL-4V Ti with propellant grade GF2 and LF2 at 77 K for up to 3 years was investigated. Titanium double coupons, annealed or heat treated, with 16 or 64 RMS finishes, were immersed in F2 in individual Pyrex capsules and stored under LN2 for 29 and 39 months. Pre and post immersion tests were performed on the propellant and coupons. Chemical analysis of the propellant did not reveal any significant changes due to titanium corrosion. Gravimetric, visual, microscopic, and metallurgical examination with pitting analysis did not reveal gross corrosion of the titanium although pitting appears to be greater after 39 months exposure. The increase in pit size and number raises the possibility of unpredictable crack propagation instability. Fracture toughness tests are necessary to define this possibility.

Denson, J. R.↗
NASA NTRS1974

Application of critical COD and plastic instability concepts to fracture of shells

The paper deals with the initiation, growth, and possible arrest of fracture in shell structures containing initial defects which may be approximated by an isolated part-through crack. The main study is restricted to the structures in which the net section of the shell wall around the defect zone is fully yielded. The problem is solved by using an 8th order shallow shell theory with a conventional plastic strip model to account for the plastic deformations. Using the critical COD or the plastic instability as fracture criterion, the results are applied to the fracture propagation and arrest in shells. The calculated results are then compared with those obtained from the experiments on zircaloy, aluminum, and steel pipes.

Erdogan, F.↗
NASA NTRS2014

A Multi-Parameter Approach for Calculating Crack Instability

An accurate fracture control analysis of spacecraft pressure systems, boosters, rocket hardware and other critical low-cycle fatigue cases where the fracture toughness highly impacts cycles to failure requires accurate knowledge of the material fracture toughness. However, applicability of the measured fracture toughness values using standard specimens and transferability of the values to crack instability analysis of the realistically complex structures is refutable. The commonly used single parameter Linear Elastic Fracture Mechanics (LEFM) approach which relies on the key assumption that the fracture toughness is a material property would result in inaccurate crack instability predictions. In the past years extensive studies have been conducted to improve the single parameter (K-controlled) LEFM by introducing parameters accounting for the geometry or in-plane constraint effects]. Despite the importance of the thickness (out-of-plane constraint) effects in fracture control problems, the literature is mainly limited to some empirical equations for scaling the fracture toughness data] and only few theoretically based developments can be found. In aerospace hardware where the structure might have only one life cycle and weight reduction is crucial, reducing the design margin of safety by decreasing the uncertainty involved in fracture toughness evaluations would result in lighter hardware. In such conditions LEFM would not suffice and an elastic-plastic analysis would be vital. Multi-parameter elastic plastic crack tip field quantifying developments combined with statistical methods] have been shown to have the potential to be used as a powerful tool for tackling such problems. However, these approaches have not been comprehensively scrutinized using experimental tests. Therefore, in this paper a multi-parameter elastic-plastic approach has been used to study the crack instability problem and the transferability issue by considering the effects of geometrical constraints as well as the thickness. The feasibility of the approach has been examined using a wide range of specimen geometries and thicknesses manufactured from 7075-T7351 aluminum alloy.

Zanganeh, M.↗
NASA NTRS2015

Crack Instability Predictions Using a Multi-Term Approach

Present crack instability analysis for fracture critical flight hardware is normally performed using a single parameter, K(sub C), fracture toughness value obtained from standard ASTM 2D geometry test specimens made from the appropriate material. These specimens do not sufficiently match the boundary conditions and the elastic‐plastic constraint characteristics of the hardware component, and also, the crack instability of most commonly used aircraft and aerospace structural materials have some amount of stable crack growth before fracture which makes the normal use of a K(sub C) single parameter toughness value highly approximate. In the past, extensive studies have been conducted to improve the single parameter (K or J controlled) approaches by introducing parameters accounting for the geometry or in‐plane constraint effects. Using 'J‐integral' and 'A' parameter as a measure of constraint is one of the most accurate elastic‐plastic crack solutions currently available. In this work the feasibility of the J‐A approach for prediction of the crack instability was investigated first by ignoring the effects of stable crack growth i.e. using a critical J and A and second by considering the effects of stable crack growth using the corrected J‐delta a using the 'A' parameter. A broad range of initial crack lengths and a wide range of specimen geometries including C(T), M(T), ESE(T), SE(T), Double Edge Crack (DEC), Three‐Hole‐Tension (THT) and NC (crack from a notch) manufactured from Al7075 were studied. Improvements in crack instability predictions were observed compared to the other methods available in the literature.

Zanganeh, Mohammad↗
NASA NTRS1994

Significant issues in proof testing: A critical appraisal

Issues which impact on the interpretation and quantification of proof test benefits are reviewed. The importance of each issue in contributing to the extra quality assurance conferred by proof testing components is discussed, particularly with respect to the application of advanced fracture mechanics concepts to enhance the flaw screening capability of a proof test analysis. Items covered include the role in proof testing of elastic-plastic fracture mechanics, ductile instability analysis, deterministic versus probabilistic analysis, single versus multiple cycle proof testing, and non-destructive examination (NDE). The effects of proof testing on subsequent service life are reviewed, particularly with regard to stress redistribution and changes in fracture behavior resulting from the overload. The importance of proof test conditions are also addressed, covering aspects related to test temperature, simulation of service environments, test media and the application of real-time NDE. The role of each issue in a proof test methodology is assessed with respect to its ability to: promote proof test practice to a state-of-the-art; aid optimization of proof test design; and increase awareness and understanding of outstanding issues.

Chell, G. G.↗
DOE OSTI2020

EXPERIMENTAL EVALUATION OF ULTRASONIC VELOCITIES AND ANISOTROPY IN THE TUSCALOOSA MARINE SHALE FORMATION

Tuscaloosa Marine Shale (TMS) formation is a clay- and organic-rich emerging shale play with a considerable amount of hydrocarbon resources. Despite the substantial potential, there have been only a few wells drilled and produced in the formation over the recent years. The analyzed TMS samples contain an average of 50 wt% total clay, 27 wt% quartz and 14 wt% calcite and the mineralogy varies considerably over the small intervals. The high amount of clay leads to pronounced anisotropy and the frequent changes in mineralogy result in the heterogeneity of the formation. We studied the compressional (V P ) and shear-wave (V S ) velocities to evaluate the degree of anisotropy and heterogeneity, which impact hydraulic fracture growth, borehole instabilities, and subsurface imaging. The ultrasonic measurements of P- and S-wave velocities from five TMS wells are the best fit to the linear relationship with R 2 = 0.84 in the least-squares criteria. We observed that TMS S-wave velocities are relatively lower when compared to the established velocity relationships. Most of the velocity data in bedding-normal direction lie outside constant V P /V S lines of 1.6–1.8, a region typical of most organic-rich shale plays. For all of the studied TMS samples, the S-wave velocity anisotropy exhibits higher values than P-wave velocity anisotropy. In the samples in which the composition is dominated by either calcite or quartz minerals, mineralogy controls the velocities and V P /V S ratios to a great extent. Additionally, the organic content and maturity account for the velocity behavior in the samples in which the mineralogical composition fails to do so. The results provide further insights into TMS Formation evaluation and contribute to a better understanding of the heterogeneity and anisotropy of the play.

Geochemistry & Geophysics↗
DOE OSTI2022

Graphene coating on silicon anodes enabled by thermal surface modification for high-energy lithium-ion batteries

Silicon is a high-energy density anode material for lithium-ion batteries, but it possesses shortcomings such as poor electronic conductivity, interfacial instability and mechanical fracturing that hinder its battery cycling. Carbon coating has been an important strategy for stabilizing silicon anodes, but the effects of the silicon surface properties on carbon coating morphology and the consequent silicon cycling stability have not been clearly elucidated. Herein, we find that thermal oxidation of the silicon anodes followed by chemical vapor deposition of carbonaceous precursors leads to a well-ordered graphene coating, whereas disordered graphite coating is formed on the native silicon surface. Graphene-coated silicon exhibits superior cycling performance, retaining a discharge capacity of ~1300 mAh g -1 after 300 cycles, whereas the disordered graphite-coated silicon suffers continuous degradation, retaining only~600 mAh g -1 after 300 cycles. Cryogenic electron microscopy reveals the mechanism behind the difference in cycling stabilities; graphene coated silicon is able to withstand the large mechanical strains induced during extended cycling, whereas disordered graphite coating is ruptured, exposing silicon surfaces to the electrolyte, leading to extensive buildup of SEI and poor cycling performance. Characterization of the silicon surface reveals that thermal treatment yields an oxygen-rich surface layer, which is hypothesized to play a decisive role in dictating the carbon coating. This work highlights the effect of silicon surface properties on carbon coating microstructure, and presents thermal treatment as a facile avenue to attain graphene coating on silicon anodes.

25 ENERGY STORAGE↗
NASA NTRS1974

Design, fracture control, fabrication, and testing of pressurized space-vehicle structures

The relationship between analysis, design, fabrication, and testing of thin shells is illustrated by Saturn S-IVB, Thor, Delta, and other single-use and reusable large-size cryogenic aluminum tankage. The analyses and design to meet the design requirements are reviewed and include consideration of fracture control, general instability, and other failure modes. The effect of research and development testing on the structure is indicated. It is shown how fabrication and nondestructive and acceptance testing constrain the design. Finally, qualification testing is reviewed to illustrate the extent of testing used to develop the Saturn S-IVB.

Babel, H. W.↗
NASA NTRS1987

Initial dynamic load estimates during configuration design

This analysis includes the structural response to shock and vibration and evaluates the maximum deflections and material stresses and the potential for the occurrence of elastic instability, fatigue and fracture. The required computations are often performed by means of finite element analysis (FEA) computer programs in which the structure is simulated by a finite element model which may contain thousands of elements. The formulation of a finite element model can be time consuming, and substantial additional modeling effort may be necessary if the structure requires significant changes after initial analysis. Rapid methods for obtaining rough estimates of the structural response to shock and vibration are presented for the purpose of providing guidance during the initial mechanical design configuration stage.

Schiff, Daniel↗
NASA NTRS2015

Damage Instability and Transition From Quasi-Static to Dynamic Fracture

In a typical mechanical test, the loading phase is intended to be a quasi-static process, while the failure and collapse is usually a dynamic event. The structural strength and modes of damage can seldom be predicted without accounting for these two aspects of the response. For a proper prediction, it is therefore essential to use tools and methodologies that are capable of addressing both aspects of responses. In some cases, implicit quasi-static models have been shown to be able to predict the entire response of a structure, including the unstable path that leads to fracture. However, is it acceptable to ignore the effect of inertial forces in the formation of damage? In this presentation we examine aspects of the damage processes that must be simulated for an accurate prediction of structural strength and modes of failure.

Davila, Carlos G.↗
DOE OSTI2023

A study of adhesive bonding in metal–metal, metal–CFRP, and CFRP–CFRP material combinations under shear deformation: Fracture morphologies and damage mechanisms

Safe design of adhesive joining in multi-materials in engineered structures requires the accumulation of numerous experimental data on the failure behavior of various adhesively-bonded material combinations under different loading conditions. The deep understanding of mechanical performance, fracturing morphologies, and main damage mechanisms is also quintessential for accelerating the development of proper physics-based and multi-scale models for assisting the design. Towards this goal, this work presents a comprehensive characterization of the failure behavior of adhesively-bonded metal–metal, metal–CFRP, and CFRP–CFRP material combinations under global shear deformation via single lap shear testing. Thanks to a synergistic combination of measurement methods by using Digital Imaging Correlation (DIC) and 3D optical profilometry, adhesive features on the adherend after failure were quantified and the main progressive damage mechanisms were identified. The characterization performed in this work provides quantitative data that contributes to a better understanding of shear failure in adhesive bonding across different bi-material combinations. Finally, the obtained results have practical implications, including the potential to enhance adhesive bonding design, identify failure causes in adhesive joints, and develop or validate computational models capable of capturing the observed behavior in various adhesively-bonded materials under global shear deformation.

36 MATERIALS SCIENCE↗
NASA NTRS1985

Elastic-plastic fracture mechanics technology

Among the topics discussed are: fracture analysis methods evaluation; instability prediction using the K sub R-curve approach; and the deformation failure assessment diagram. Consideration is also given to: instability prediction based on the modified J, J sub M-resistance curve approach; and stable crack growth and instability prediction on the V by means of the V sub R-curve method.

Newman, J. C., Jr.↗
NASA NTRS1989

A probabilistic approach to crack instability

A probabilistic model of brittle fracture is examined with reference to two-dimensional problems. The model is illustrated by using experimental data obtained for 25 macroscopically identical specimens made of short-fiber-reinforced composites. It is shown that the model proposed here provides a predictive formalism for the probability distributions of critical crack depth, critical loads, and crack arrest depths. It also provides similarity criteria for small-scale testing.

Chudnovsky, A.↗